Goldichite Graeber E J, Rosenzweig A American Mineralogist 56 (1971) 1917-1933 The crystal structures of yavapaiite, KFe(SO4)2, and goldichite, KFe(SO4)2.4H2O _database_code_amcsd 0000264 CELL PARAMETERS: 10.3870 10.4860 9.0860 90.000 101.680 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 969.138 Density (g/cm3): 2.520 MAX. ABS. INTENSITY / VOLUME**2: 5.745566645 RIR: 0.742 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.69 73.24 10.1719 1 0 0 2 12.12 100.00 7.3011 1 1 0 4 13.05 80.84 6.7845 0 1 1 4 14.53 14.81 6.0952 -1 1 1 4 16.91 5.97 5.2430 0 2 0 2 17.44 6.83 5.0860 2 0 0 2 19.04 34.46 4.6603 1 2 0 4 19.40 6.54 4.5761 2 1 0 4 20.10 3.65 4.4177 -1 0 2 2 20.14 2.18 4.4092 -2 1 1 4 20.68 31.25 4.2954 -1 2 1 4 21.70 2.48 4.0956 0 1 2 4 21.83 19.99 4.0711 -1 1 2 4 22.34 54.31 3.9794 1 2 1 4 23.39 6.53 3.8032 1 0 2 2 23.42 5.54 3.7978 2 1 1 4 24.38 20.93 3.6506 2 2 0 4 24.90 5.95 3.5753 1 1 2 4 24.98 12.34 3.5641 -2 2 1 4 25.25 20.10 3.5271 -2 1 2 4 26.27 29.73 3.3922 0 2 2 4 26.28 1.56 3.3906 3 0 0 2 26.38 13.92 3.3783 -1 2 2 4 26.97 5.18 3.3056 1 3 0 4 27.41 17.25 3.2533 0 3 1 4 27.53 27.07 3.2395 -3 1 1 4 27.65 5.66 3.2262 3 1 0 4 27.73 14.16 3.2172 2 2 1 4 28.17 7.50 3.1675 -1 3 1 4 29.00 28.27 3.0786 1 2 2 4 29.22 62.42 3.0560 2 0 2 2 29.31 32.36 3.0476 -2 2 2 4 29.44 5.57 3.0342 1 3 1 4 29.72 60.77 3.0060 -3 0 2 2 30.47 11.18 2.9339 2 1 2 4 30.85 2.40 2.8987 -1 1 3 4 30.95 1.46 2.8896 -3 1 2 4 31.05 17.28 2.8806 2 3 0 4 31.26 4.34 2.8615 3 1 1 4 31.32 1.89 2.8563 -3 2 1 4 31.34 26.34 2.8540 0 1 3 4 31.42 24.47 2.8471 3 2 0 4 31.53 8.48 2.8376 -2 3 1 4 32.58 11.79 2.7485 0 3 2 4 32.67 4.60 2.7411 -1 3 2 4 33.79 65.32 2.6529 2 3 1 4 33.95 1.60 2.6402 2 2 2 4 34.20 8.24 2.6215 0 4 0 2 34.39 4.12 2.6078 -3 2 2 4 34.67 6.16 2.5871 3 2 1 4 34.75 14.59 2.5815 0 2 3 4 34.86 2.59 2.5735 1 3 2 4 35.12 7.60 2.5554 -2 3 2 4 35.29 1.71 2.5430 4 0 0 2 35.71 3.32 2.5146 0 4 1 4 36.35 1.74 2.4713 4 1 0 4 36.42 1.72 2.4667 3 0 2 2 36.85 7.19 2.4394 -3 3 1 4 37.00 14.62 2.4298 -4 0 2 2 37.01 20.32 2.4290 -3 1 3 4 37.45 1.50 2.4012 3 1 2 4 38.81 11.58 2.3202 -4 2 1 4 39.68 12.03 2.2712 -1 0 4 2 40.55 1.45 2.2245 0 0 4 2 40.94 2.41 2.2046 2 4 1 4 40.94 3.88 2.2046 -4 2 2 4 41.10 1.81 2.1961 -2 3 3 4 41.85 3.71 2.1584 1 4 2 4 41.95 5.90 2.1539 2 2 3 4 42.26 7.71 2.1388 1 3 3 4 42.77 4.12 2.1142 -4 1 3 4 43.42 26.24 2.0841 -1 2 4 4 44.04 8.25 2.0563 4 3 0 4 44.09 5.74 2.0540 1 5 0 4 44.26 3.08 2.0466 1 1 4 4 44.47 2.32 2.0371 -5 1 1 4 44.51 1.31 2.0356 -2 2 4 4 44.88 7.06 2.0195 -1 5 1 4 44.98 12.78 2.0154 3 3 2 4 45.10 1.12 2.0104 -5 0 2 2 45.35 1.19 1.9999 3 1 3 4 45.35 5.83 1.9998 4 1 2 4 45.41 1.80 1.9971 5 1 0 4 45.46 4.73 1.9951 -4 3 2 4 45.59 1.53 1.9897 2 4 2 4 46.86 1.22 1.9388 1 2 4 4 47.39 4.83 1.9182 -3 2 4 4 47.76 1.07 1.9045 -1 3 4 4 47.90 4.52 1.8990 3 2 3 4 47.91 1.25 1.8989 4 2 2 4 47.96 9.48 1.8970 0 5 2 4 47.97 1.40 1.8966 5 2 0 4 48.02 4.36 1.8946 -1 5 2 4 48.50 1.16 1.8772 -5 2 2 4 48.51 2.62 1.8767 0 3 4 4 48.62 5.45 1.8727 -4 0 4 2 48.67 2.64 1.8708 5 1 1 4 48.84 1.37 1.8647 2 5 1 4 49.44 2.53 1.8435 -4 1 4 4 49.50 5.22 1.8415 -4 4 1 4 49.64 8.63 1.8365 1 5 2 4 49.83 2.53 1.8299 -2 5 2 4 50.83 2.79 1.7965 3 4 2 4 51.09 1.55 1.7877 2 2 4 4 51.16 13.22 1.7853 -5 3 1 4 51.22 2.65 1.7836 3 5 0 4 51.47 2.85 1.7754 -3 3 4 4 51.60 2.08 1.7711 -2 1 5 4 51.95 6.26 1.7602 3 3 3 4 51.95 1.23 1.7601 4 3 2 4 52.11 6.74 1.7553 -5 2 3 4 52.35 1.46 1.7477 0 6 0 2 52.51 2.23 1.7427 -5 3 2 4 52.67 1.29 1.7379 4 1 3 4 52.95 1.38 1.7292 2 5 2 4 53.43 2.72 1.7149 0 6 1 4 53.46 6.86 1.7140 3 5 1 4 53.51 1.66 1.7124 0 5 3 4 53.66 2.83 1.7081 3 0 4 2 53.83 4.47 1.7031 -3 1 5 4 53.83 2.56 1.7031 -6 0 2 2 54.07 3.36 1.6961 0 4 4 4 54.31 2.30 1.6892 -2 4 4 4 54.86 1.23 1.6736 6 1 0 4 54.97 3.44 1.6704 4 2 3 4 54.97 1.32 1.6704 2 3 4 4 55.45 1.73 1.6572 1 5 3 4 55.91 3.17 1.6446 -2 6 1 4 55.94 1.86 1.6438 -6 2 1 4 56.10 2.64 1.6395 -3 2 5 4 56.35 2.57 1.6326 1 4 4 4 56.68 1.64 1.6241 3 2 4 4 56.91 3.96 1.6180 4 5 0 4 57.09 2.15 1.6134 1 2 5 4 57.27 1.24 1.6087 3 4 3 4 57.27 5.55 1.6086 4 4 2 4 57.33 2.21 1.6072 5 4 0 4 57.61 3.84 1.6000 -5 2 4 4 57.70 1.20 1.5978 3 5 2 4 57.79 1.05 1.5953 -5 4 2 4 58.17 1.45 1.5859 0 3 5 4 58.67 4.27 1.5736 4 3 3 4 59.02 2.60 1.5651 2 1 5 4 59.44 1.38 1.5549 -3 6 1 4 59.51 2.84 1.5534 3 6 0 4 59.60 1.50 1.5512 -6 3 1 4 59.74 1.86 1.5480 -4 2 5 4 59.75 1.10 1.5476 -3 3 5 4 60.11 2.89 1.5393 2 4 4 4 60.25 4.52 1.5361 6 2 1 4 60.60 1.47 1.5280 4 0 4 2 60.71 3.07 1.5256 1 3 5 4 60.72 1.26 1.5254 6 3 0 4 61.16 1.58 1.5153 2 2 5 4 61.21 1.36 1.5143 -5 3 4 4 61.31 3.27 1.5120 4 1 4 4 61.66 3.02 1.5042 -4 5 3 4 61.72 2.41 1.5030 -6 0 4 2 62.19 1.73 1.4927 -2 1 6 4 62.51 1.82 1.4859 -2 6 3 4 62.92 1.89 1.4772 0 7 1 4 63.14 1.25 1.4726 -3 0 6 2 63.26 3.09 1.4700 -3 5 4 4 63.31 2.71 1.4689 -1 7 1 4 63.68 1.93 1.4613 3 5 3 4 63.73 1.50 1.4602 5 5 0 4 64.49 1.52 1.4450 3 1 5 4 64.49 1.03 1.4448 -6 2 4 4 64.77 3.22 1.4394 7 1 0 4 65.15 3.08 1.4318 -3 6 3 4 65.17 1.79 1.4315 -2 7 1 4 65.34 1.16 1.4282 -6 4 2 4 65.41 1.05 1.4267 -7 2 1 4 66.05 1.63 1.4146 -5 4 4 4 66.09 2.25 1.4138 1 1 6 4 66.21 1.65 1.4114 -4 0 6 2 66.36 1.79 1.4087 2 5 4 4 67.50 1.44 1.3876 -1 3 6 4 68.09 1.10 1.3770 -5 3 5 4 68.26 2.13 1.3740 -7 2 3 4 68.42 1.62 1.3712 -3 7 1 4 68.47 1.01 1.3702 3 7 0 4 68.50 2.72 1.3698 6 4 1 4 68.80 1.78 1.3646 -2 5 5 4 68.89 1.49 1.3629 -4 2 6 4 69.26 1.36 1.3567 -7 3 2 4 69.83 2.14 1.3469 6 1 3 4 70.14 1.45 1.3418 7 3 0 4 70.54 1.08 1.3350 -6 5 1 4 70.62 1.82 1.3338 -5 0 6 2 71.20 1.18 1.3244 3 5 4 4 72.02 3.67 1.3113 -5 5 4 4 72.39 1.06 1.3055 7 0 2 2 72.70 1.35 1.3007 -5 4 5 4 72.74 2.15 1.3000 1 8 0 4 73.17 1.21 1.2935 6 4 2 4 73.29 1.98 1.2917 7 3 1 4 73.32 1.36 1.2911 -1 8 1 4 73.35 1.23 1.2908 0 4 6 4 73.62 2.05 1.2867 5 6 1 4 73.78 1.38 1.2842 -1 1 7 4 73.81 1.38 1.2839 -3 4 6 4 74.38 1.19 1.2754 6 5 1 4 74.68 1.24 1.2709 7 4 0 4 75.31 2.31 1.2619 0 1 7 4 75.55 3.03 1.2586 3 1 6 4 75.55 1.87 1.2586 -2 2 7 4 76.07 1.46 1.2512 -7 4 3 4 76.68 1.13 1.2427 -4 4 6 4 76.94 2.28 1.2392 1 8 2 4 77.57 2.64 1.2307 -4 7 3 4 78.01 2.03 1.2249 6 1 4 4 78.91 1.49 1.2131 6 5 2 4 79.56 1.38 1.2049 -7 5 2 4 79.90 2.65 1.2006 -3 3 7 4 83.75 1.71 1.1549 8 1 2 4 84.41 1.47 1.1476 -8 3 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.