Biringuccite Corazza E, Menchetti S, Sabelli C American Mineralogist 59 (1974) 1005-1015 The crystal structure of biringuccite, Na4[B10O16(OH)2].2H2O CELL PARAMETERS: 11.1955 6.5607 20.7566 90.000 93.891 90.000 SPACE GROUP: P2_1/c X-RAY WAVELENGTH: 1.541838 MAX. ABS. INTENSITY / VOLUME**2: 1.801398333 2-THETA INTENSITY D-SPACING H K L 8.54 100.00 10.3544 0 0 2 11.25 10.79 7.8643 -1 0 2 12.04 5.77 7.3490 1 0 2 15.66 9.59 5.6570 1 1 0 15.87 1.96 5.5848 2 0 0 15.99 7.36 5.5419 0 1 2 16.38 5.67 5.4100 1 1 1 17.13 31.85 5.1772 0 0 4 17.52 2.00 5.0610 -2 0 2 17.60 64.00 5.0378 -1 1 2 18.13 33.21 4.8942 1 1 2 18.39 11.22 4.8237 -1 0 4 18.56 15.83 4.7817 2 0 2 19.38 2.70 4.5801 1 0 4 19.95 5.78 4.4511 -1 1 3 20.89 9.15 4.2527 2 1 0 21.11 17.81 4.2088 -2 1 1 21.87 4.62 4.0642 0 1 4 23.02 1.67 3.8643 2 1 2 23.69 8.70 3.7555 1 1 4 23.90 3.22 3.7232 3 0 0 24.00 2.12 3.7073 -2 1 3 24.22 5.89 3.6745 2 0 4 25.16 6.59 3.5400 2 1 3 25.81 79.62 3.4515 0 0 6 26.23 6.51 3.3980 -1 1 5 26.43 17.59 3.3727 -2 1 4 27.12 6.74 3.2884 1 1 5 27.18 5.02 3.2803 0 2 0 27.53 4.20 3.2400 0 2 1 27.55 3.68 3.2381 3 1 0 27.56 1.02 3.2363 1 0 6 28.36 13.62 3.1474 1 2 0 28.54 12.43 3.1272 0 2 2 29.31 93.93 3.0468 -2 1 5 29.49 46.85 3.0294 -2 0 6 29.50 10.08 3.0275 -1 2 2 29.86 6.19 2.9924 -1 1 6 30.16 30.63 2.9628 0 2 3 31.00 2.59 2.8847 -1 2 3 31.38 41.92 2.8508 2 0 6 31.46 1.70 2.8433 1 2 3 31.78 35.03 2.8155 -2 2 1 32.08 27.30 2.7897 2 2 1 32.31 3.55 2.7709 0 2 4 32.56 3.19 2.7503 -2 1 6 33.02 18.31 2.7125 -1 2 4 33.12 10.23 2.7050 2 2 2 33.22 5.02 2.6969 0 1 7 33.50 50.57 2.6753 3 1 4 33.70 3.04 2.6594 -1 1 7 33.81 10.16 2.6513 4 0 2 33.83 36.69 2.6495 -2 2 3 34.13 4.23 2.6274 -3 1 5 34.30 6.68 2.6146 2 1 6 34.65 41.11 2.5886 0 0 8 34.70 6.21 2.5853 1 1 7 34.89 1.25 2.5715 0 2 5 34.92 4.26 2.5695 -4 1 1 34.92 4.87 2.5694 4 1 0 35.05 1.84 2.5603 -1 0 8 35.47 5.76 2.5310 -4 1 2 35.47 16.73 2.5306 4 1 1 35.47 9.66 2.5305 -4 0 4 35.49 8.02 2.5294 -1 2 5 36.08 9.23 2.4896 -2 1 7 36.15 14.85 2.4849 1 0 8 36.17 2.94 2.4832 1 2 5 36.21 4.38 2.4810 3 1 5 36.51 15.26 2.4613 3 2 0 36.57 10.49 2.4571 -3 2 1 36.93 14.84 2.4343 -3 1 6 36.97 3.84 2.4314 3 2 1 37.28 6.80 2.4119 -2 0 8 37.34 1.85 2.4079 0 1 8 37.62 1.26 2.3909 4 0 4 37.84 1.69 2.3777 0 2 6 37.90 5.31 2.3741 -2 2 5 37.94 1.05 2.3718 2 1 7 38.12 3.84 2.3610 -4 1 4 38.13 12.69 2.3603 4 1 3 38.27 3.20 2.3520 -3 2 3 38.75 3.14 2.3238 1 1 8 39.10 8.98 2.3038 1 2 6 39.41 2.49 2.2861 3 2 3 39.82 1.53 2.2637 -2 1 8 39.84 3.36 2.2626 -3 2 4 40.05 1.28 2.2513 -3 1 7 40.13 6.33 2.2471 -4 1 5 40.14 2.36 2.2467 -4 0 6 40.14 4.39 2.2463 4 1 4 40.53 3.59 2.2255 -2 2 6 41.10 2.83 2.1964 -3 0 8 41.32 12.18 2.1852 3 2 4 41.52 2.54 2.1748 0 3 1 41.84 3.52 2.1589 -3 2 5 41.99 2.84 2.1518 2 2 6 42.24 7.93 2.1397 0 3 2 42.33 1.37 2.1354 1 2 7 42.40 5.42 2.1319 1 3 1 42.51 14.39 2.1264 -4 2 1 42.51 4.24 2.1263 4 2 0 42.55 1.27 2.1247 4 1 5 42.70 2.40 2.1176 -5 1 1 42.76 1.24 2.1147 5 1 0 42.93 1.18 2.1070 -1 3 2 42.94 2.90 2.1063 1 1 9 42.98 3.63 2.1044 -4 2 2 42.99 1.39 2.1037 -5 0 4 43.03 3.75 2.1023 4 0 6 43.11 9.50 2.0985 -5 1 2 43.40 1.82 2.0848 0 3 3 43.45 2.34 2.0828 -3 1 8 43.50 1.08 2.0805 -2 2 7 43.61 1.14 2.0754 3 2 5 43.71 1.08 2.0709 0 0 10 43.75 13.88 2.0690 -2 1 9 43.90 4.62 2.0623 -4 2 3 43.93 1.44 2.0609 3 0 8 43.97 5.69 2.0593 -5 1 3 44.26 4.83 2.0463 5 1 2 44.37 9.96 2.0419 1 3 3 44.91 1.96 2.0183 -1 2 8 45.00 6.67 2.0145 0 3 4 45.06 1.03 2.0119 1 0 10 45.17 2.44 2.0075 -2 3 2 45.26 4.66 2.0036 -4 2 4 45.27 5.48 2.0033 -5 1 4 45.27 14.97 2.0032 4 2 3 45.28 3.61 2.0028 -4 1 7 45.29 1.64 2.0023 5 0 4 45.61 7.81 1.9888 2 3 2 45.67 4.71 1.9865 5 1 3 45.68 5.21 1.9861 -2 0 10 45.81 1.28 1.9808 1 2 8 45.96 3.19 1.9748 0 1 10 46.16 2.27 1.9664 -2 3 3 46.17 1.06 1.9661 3 1 8 46.17 3.85 1.9661 -4 0 8 46.25 2.77 1.9628 3 2 6 46.83 2.35 1.9402 2 3 3 46.92 1.77 1.9363 -5 0 6 46.95 3.48 1.9353 -3 2 7 47.03 11.25 1.9321 4 2 4 47.26 7.67 1.9234 1 1 10 47.46 33.52 1.9158 -1 3 5 47.85 1.87 1.9009 -2 1 10 47.87 8.62 1.9001 2 0 10 48.00 3.84 1.8955 1 3 5 48.31 3.73 1.8838 0 2 9 48.33 6.54 1.8833 -4 1 8 48.35 10.00 1.8826 4 1 7 48.48 1.59 1.8777 2 2 8 48.63 8.06 1.8721 3 3 1 48.79 2.50 1.8665 -3 3 2 49.05 2.90 1.8571 -5 1 6 49.13 1.56 1.8543 -6 0 2 49.17 1.63 1.8531 4 2 5 49.30 4.59 1.8483 -5 2 1 49.38 1.11 1.8456 -2 3 5 49.52 1.15 1.8408 1 2 9 49.65 3.63 1.8362 5 1 5 49.67 1.31 1.8356 -5 2 2 49.96 2.19 1.8255 3 1 9 50.12 1.19 1.8199 5 0 6 50.25 2.65 1.8158 -2 2 9 50.39 7.82 1.8110 6 0 2 50.42 2.90 1.8098 2 3 5 50.43 11.82 1.8096 0 1 11 50.44 1.17 1.8092 -5 2 3 50.89 4.52 1.7943 -6 1 1 50.99 3.77 1.7909 -6 0 4 51.19 4.33 1.7844 -6 1 2 51.48 1.52 1.7752 -5 1 7 51.54 4.63 1.7732 -2 3 6 51.61 5.42 1.7709 -5 2 4 51.90 6.33 1.7617 -6 1 3 52.00 2.28 1.7586 0 3 7 52.09 1.90 1.7557 2 2 9 52.16 5.24 1.7537 5 1 6 52.34 1.30 1.7480 -1 3 7 52.76 6.98 1.7352 2 3 6 53.00 1.91 1.7277 -6 1 4 53.04 1.60 1.7265 1 3 7 53.07 11.11 1.7257 0 0 12 53.15 3.20 1.7232 -1 0 12 53.25 3.64 1.7202 -4 0 10 53.59 7.50 1.7100 -4 3 2 53.63 3.80 1.7091 5 2 4 54.22 1.38 1.6918 -5 1 8 54.30 2.80 1.6895 2 1 11 54.38 1.55 1.6872 -4 3 3 54.38 1.08 1.6870 -6 0 6 54.41 1.36 1.6864 -4 2 8 54.43 6.13 1.6858 4 2 7 54.58 1.91 1.6813 -2 0 12 54.66 1.80 1.6793 -3 3 6 54.96 2.95 1.6705 0 3 8 55.23 1.35 1.6633 4 1 9 55.24 2.11 1.6629 -1 3 8 55.91 2.36 1.6445 3 2 9 56.26 1.92 1.6350 1 1 12 56.47 1.62 1.6294 -1 2 11 56.50 3.66 1.6287 -2 1 12 56.80 1.25 1.6208 -3 2 10 56.90 1.04 1.6181 2 0 12 57.05 1.11 1.6142 -6 2 2 57.39 3.70 1.6056 -1 4 2 57.47 1.36 1.6035 -4 2 9 57.49 2.50 1.6030 4 2 8 57.58 1.23 1.6008 1 4 2 58.20 2.63 1.5852 0 3 9 58.34 1.29 1.5816 2 3 8 58.77 1.10 1.5710 2 1 12 59.16 1.23 1.5617 -3 1 12 59.26 3.62 1.5593 1 3 9 59.45 1.22 1.5549 -7 0 4 59.53 2.54 1.5528 5 3 1 59.77 3.00 1.5473 -1 1 13 60.08 1.42 1.5400 -5 3 3 60.60 1.37 1.5280 2 4 3 61.01 4.53 1.5188 7 1 2 61.05 1.54 1.5177 -2 1 13 61.69 1.39 1.5037 0 3 10 62.26 1.00 1.4913 -3 4 2 62.46 1.19 1.4870 3 1 12 62.81 1.81 1.4795 -1 0 14 63.02 1.48 1.4751 -3 4 3 63.73 4.09 1.4602 -6 1 9 63.89 2.16 1.4570 -6 2 7 64.01 1.55 1.4545 -2 0 14 64.12 1.80 1.4523 -3 4 4 64.57 1.28 1.4433 -1 1 14 65.02 1.36 1.4345 0 4 7 65.80 1.40 1.4193 -6 3 1 65.89 1.05 1.4176 6 3 0 66.06 2.67 1.4143 -4 4 1 66.26 1.63 1.4106 -6 2 8 66.98 1.15 1.3971 3 1 13 67.21 1.04 1.3929 4 1 12 67.69 2.51 1.3841 3 2 12 68.41 1.63 1.3714 8 0 2 68.45 1.36 1.3706 6 1 9 69.33 1.25 1.3555 5 3 7 69.49 1.06 1.3527 -4 4 5 69.92 1.39 1.3454 -4 0 14 71.12 1.11 1.3256 8 0 4 72.24 1.01 1.3077 -4 2 13 73.15 1.81 1.2937 -3 2 14 73.28 1.04 1.2917 1 5 2 73.48 1.43 1.2888 -7 2 8 73.58 1.37 1.2872 -8 2 1 73.90 1.47 1.2824 -1 5 3 74.08 1.20 1.2798 -7 3 3 74.62 1.56 1.2719 4 0 14 74.74 2.79 1.2701 -2 5 2 75.99 1.43 1.2524 -7 2 9 77.35 1.70 1.2337 3 5 1 77.52 2.13 1.2314 -3 4 10 77.98 2.41 1.2252 6 4 1 78.01 1.26 1.2248 6 0 12 78.34 1.01 1.2206 -9 1 2 78.51 1.15 1.2184 5 4 6 79.55 2.49 1.2050 -9 1 4 80.55 1.57 1.1925 -2 2 16 81.83 1.09 1.1771 5 1 14 83.59 1.01 1.1568 -9 2 3 83.81 1.44 1.1543 1 3 15 85.86 2.73 1.1318 -5 5 1 86.14 1.36 1.1289 -5 5 2 86.19 1.05 1.1284 -7 4 4 88.49 1.24 1.1049 -3 1 18 88.81 2.58 1.1018 -7 4 6 89.04 1.05 1.0995 4 3 14 89.10 1.35 1.0989 -10 1 3 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.