Fillowite Araki T, Moore P B American Mineralogist 66 (1981) 827-842 Fillowite, Na2Ca(Mn,Fe)7(PO4)6: Its crystal structure _database_code_amcsd 0000842 CELL PARAMETERS: 15.2820 15.2820 43.5070 90.000 90.000 120.000 SPACE GROUP: R-3 X-RAY WAVELENGTH: 1.541838 Cell Volume: 8799.341 Density (g/cm3): 3.554 MAX. ABS. INTENSITY / VOLUME**2: 12.21757563 RIR: 1.119 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 6.09 4.64 14.5023 0 0 3 2 7.82 26.98 11.3065 0 1 2 6 10.53 18.00 8.4030 1 0 4 6 12.17 1.61 7.2707 0 1 5 6 12.21 6.73 7.2512 0 0 6 2 13.10 1.33 6.7601 1 1 3 6 13.99 4.32 6.3309 2 0 2 6 15.68 8.91 5.6533 0 2 4 6 16.86 2.89 5.2598 1 1 6 6 16.86 7.39 5.2598 2 -1 6 6 17.63 1.94 5.0302 0 1 8 6 18.20 1.20 4.8750 -1 3 2 6 19.53 6.00 4.5446 2 1 4 6 19.53 3.23 4.5446 3 -1 4 6 20.13 1.00 4.4115 3 0 0 6 20.48 4.10 4.3367 -1 3 5 6 21.05 6.08 4.2206 0 3 3 6 21.15 5.28 4.2015 2 0 8 6 21.50 4.14 4.1331 1 0 10 6 23.28 4.14 3.8205 2 2 0 6 23.61 18.22 3.7688 0 3 6 6 24.09 4.97 3.6945 4 -2 3 6 24.09 2.28 3.6945 2 2 3 6 24.17 1.51 3.6817 1 2 8 6 24.34 1.24 3.6576 1 3 1 6 24.55 14.52 3.6256 0 0 12 2 24.60 18.21 3.6195 4 -1 2 6 24.60 21.30 3.6195 3 1 2 6 25.61 1.60 3.4779 1 3 4 6 25.61 9.26 3.4779 -1 4 4 6 26.25 3.50 3.3950 2 0 11 6 26.35 1.63 3.3820 4 -1 5 6 26.35 3.93 3.3820 3 1 5 6 26.37 3.36 3.3800 2 2 6 6 27.16 5.07 3.2828 2 1 10 6 27.37 3.50 3.2586 3 0 9 6 28.19 4.93 3.1654 4 0 4 6 28.78 1.53 3.1025 -1 3 11 6 29.36 2.10 3.0425 3 1 8 6 29.53 18.20 3.0254 0 1 14 6 29.71 17.13 3.0071 2 3 2 6 29.71 25.27 3.0071 -2 5 2 6 29.81 2.34 2.9974 4 -2 9 6 30.57 1.11 2.9244 5 -2 4 6 30.57 3.30 2.9244 3 2 4 6 30.96 7.01 2.8880 4 1 0 6 31.20 1.46 2.8667 2 3 5 6 31.20 3.01 2.8667 -2 5 5 6 31.59 8.88 2.8324 1 4 3 6 31.59 12.38 2.8324 -1 5 3 6 31.81 30.34 2.8129 2 0 14 6 31.90 7.17 2.8055 1 3 10 6 31.90 4.63 2.8055 -1 4 10 6 31.95 55.55 2.8010 0 3 12 6 31.95 44.45 2.8010 3 0 12 6 32.83 1.42 2.7281 3 2 7 6 33.30 4.06 2.6905 4 -1 11 6 33.30 1.46 2.6905 3 1 11 6 33.40 5.31 2.6830 4 1 6 6 33.40 1.08 2.6830 5 -1 6 6 33.81 1.21 2.6510 2 3 8 6 33.81 3.98 2.6510 -2 5 8 6 33.96 3.36 2.6397 -1 3 14 6 33.96 2.72 2.6397 1 2 14 6 34.04 3.72 2.6336 4 0 10 6 34.89 3.69 2.5719 0 5 4 6 35.24 60.72 2.5470 3 3 0 6 35.97 2.13 2.4970 -2 6 1 6 35.97 5.25 2.4970 2 4 1 6 36.15 2.03 2.4847 4 2 2 6 36.23 1.34 2.4793 -1 5 9 6 36.88 2.07 2.4375 -2 6 4 6 36.88 2.23 2.4375 2 4 4 6 37.42 6.23 2.4031 6 -3 6 6 37.42 2.57 2.4031 3 3 6 6 37.65 3.98 2.3890 3 -1 16 6 37.94 1.46 2.3718 4 -1 14 6 37.94 3.91 2.3718 3 1 14 6 38.08 4.18 2.3629 1 5 2 6 38.81 1.05 2.3203 2 4 7 6 39.55 1.19 2.2784 1 2 17 6 39.91 1.06 2.2589 -1 5 12 6 39.91 1.70 2.2589 4 1 12 6 40.64 1.83 2.2202 6 -1 7 6 40.91 2.03 2.2058 6 0 0 6 41.56 4.26 2.1730 4 3 1 6 41.56 3.74 2.1730 7 -3 1 6 41.65 1.05 2.1683 -2 6 10 6 41.65 1.19 2.1683 2 4 10 6 41.72 1.35 2.1650 -3 7 2 6 41.72 5.04 2.1650 3 4 2 6 42.37 1.11 2.1335 4 3 4 6 42.65 1.23 2.1197 0 3 18 6 42.66 2.68 2.1192 5 2 0 6 42.85 5.10 2.1103 0 6 6 6 43.06 1.19 2.1008 4 0 16 6 43.42 1.24 2.0841 6 -3 12 6 43.42 3.09 2.0841 3 3 12 6 44.35 3.61 2.0426 4 -2 18 6 44.35 1.16 2.0426 2 2 18 6 44.54 1.12 2.0341 5 2 6 6 44.74 1.72 2.0256 3 2 16 6 44.87 1.34 2.0201 -3 7 8 6 44.96 1.19 2.0161 1 6 1 6 44.99 3.12 2.0151 5 0 14 6 45.47 1.59 1.9949 1 2 20 6 46.40 1.55 1.9568 2 3 17 6 46.43 3.36 1.9559 1 0 22 6 46.61 1.26 1.9484 4 2 14 6 46.61 1.26 1.9484 6 -2 14 6 46.76 1.50 1.9428 1 3 19 6 46.81 2.17 1.9409 7 -2 9 6 47.51 1.02 1.9138 3 3 15 6 48.20 10.96 1.8880 1 5 14 6 48.20 2.52 1.8880 -1 6 14 6 48.30 8.00 1.8844 0 6 12 6 48.30 10.84 1.8844 6 0 12 6 48.32 1.46 1.8836 0 7 2 6 48.32 1.17 1.8836 8 -3 2 6 49.15 3.03 1.8536 1 4 18 6 49.15 4.32 1.8536 -1 5 18 6 49.15 2.82 1.8536 5 -1 18 6 49.80 5.99 1.8309 -1 7 10 6 49.80 2.44 1.8309 1 6 10 6 49.84 1.08 1.8296 2 5 12 6 49.84 1.41 1.8296 5 2 12 6 49.84 1.45 1.8296 7 -2 12 6 50.34 5.46 1.8128 0 0 24 2 50.79 1.01 1.7977 7 -1 11 6 51.44 1.98 1.7766 8 -4 9 6 51.44 1.36 1.7766 4 4 9 6 51.83 2.25 1.7638 2 -1 24 6 51.95 1.40 1.7602 6 2 7 6 52.17 1.08 1.7533 3 3 18 6 52.18 1.83 1.7530 1 7 0 6 52.54 2.17 1.7417 1 5 17 6 52.57 2.51 1.7410 -1 4 22 6 52.59 3.96 1.7403 8 -1 3 6 52.59 3.29 1.7403 7 1 3 6 52.63 1.12 1.7390 2 6 8 6 53.56 2.49 1.7111 -2 7 15 6 53.56 1.96 1.7111 2 5 15 6 53.74 1.08 1.7058 5 3 11 6 53.80 1.50 1.7039 -1 8 6 6 53.80 1.46 1.7039 1 7 6 6 53.97 2.44 1.6989 4 3 16 6 53.97 1.46 1.6989 7 -3 16 6 54.17 1.14 1.6932 5 4 1 6 54.28 2.27 1.6900 8 -4 12 6 54.51 3.16 1.6834 4 1 21 6 54.61 2.06 1.6806 5 0 20 6 55.08 2.25 1.6674 3 6 0 6 55.34 6.16 1.6601 0 1 26 6 55.78 1.45 1.6480 8 -1 9 6 55.78 4.48 1.6480 7 1 9 6 57.02 2.78 1.6152 0 7 14 6 57.02 2.01 1.6152 5 3 14 6 57.02 4.15 1.6152 8 -3 14 6 57.79 2.89 1.5953 8 -4 15 6 57.79 2.88 1.5953 4 4 15 6 58.30 2.40 1.5827 8 0 8 6 58.40 1.17 1.5803 2 6 14 6 59.60 2.76 1.5513 -2 6 22 6 60.36 1.44 1.5335 8 1 4 6 60.36 1.58 1.5335 9 -1 4 6 60.73 1.02 1.5250 -1 9 5 6 60.73 2.05 1.5250 1 8 5 6 60.84 1.53 1.5226 4 -1 26 6 60.84 1.05 1.5226 3 1 26 6 61.18 3.22 1.5149 -3 9 12 6 61.18 1.16 1.5149 3 6 12 6 61.18 1.72 1.5149 6 3 12 6 62.33 1.82 1.4897 1 8 8 6 62.52 1.61 1.4855 -3 10 2 6 62.52 1.52 1.4855 3 7 2 6 62.93 1.74 1.4769 3 3 24 6 63.24 6.10 1.4705 9 0 0 6 63.48 4.91 1.4655 2 3 26 6 63.48 4.71 1.4655 -2 5 26 6 64.53 2.22 1.4440 2 8 0 6 64.62 1.48 1.4423 -1 9 11 6 64.89 1.11 1.4370 1 2 29 6 64.89 1.32 1.4369 2 8 3 6 65.02 2.14 1.4343 7 2 14 6 65.20 1.15 1.4309 1 3 28 6 66.35 2.14 1.4088 10 -3 10 6 66.38 1.05 1.4082 10 -5 12 6 67.33 1.24 1.3908 4 2 26 6 67.33 1.48 1.3908 6 -2 26 6 68.35 1.77 1.3724 7 4 0 6 68.58 1.53 1.3683 1 5 26 6 68.70 2.30 1.3663 -4 11 3 6 68.70 1.04 1.3663 4 7 3 6 68.83 1.08 1.3641 10 -4 14 6 68.91 1.13 1.3627 9 0 12 6 71.46 1.04 1.3202 4 7 9 6 74.51 2.26 1.2735 6 6 0 6 79.75 1.00 1.2025 -2 11 14 6 79.91 1.11 1.2004 7 0 28 6 83.36 1.13 1.1593 12 -3 12 6 83.36 1.75 1.1593 9 3 12 6 85.04 1.06 1.1407 0 1 38 6 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.