Hyalotekite Moore P B, Araki T, Ghose S American Mineralogist 67 (1982) 1012-1020 Hyalotekite, a complex lead borosilicate: Its crystal structure and the lone-pair effect of Pb(II) _database_code_amcsd 0000880 CELL PARAMETERS: 11.3100 10.9550 10.3170 90.430 90.020 90.160 SPACE GROUP: I-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 1278.246 Density (g/cm3): 3.826 MAX. ABS. INTENSITY / VOLUME**2: 8.221700913 RIR: 0.700 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.23 68.26 7.8797 -1 1 0 2 11.26 69.81 7.8578 1 1 0 2 11.61 57.74 7.6234 -1 0 1 2 11.61 58.27 7.6206 1 0 1 2 11.74 39.96 7.5387 0 -1 1 2 11.83 44.93 7.4824 0 1 1 2 15.67 28.19 5.6550 2 0 0 2 16.18 30.54 5.4773 0 2 0 2 17.19 51.98 5.1584 0 0 2 2 19.66 3.22 4.5162 -2 1 1 2 19.70 3.79 4.5067 2 1 1 2 19.89 9.20 4.4634 1 -2 1 2 19.93 8.80 4.4560 -1 -2 1 2 20.00 10.40 4.4405 -1 2 1 2 20.03 10.00 4.4321 1 2 1 2 20.53 34.86 4.3260 1 -1 2 2 20.54 35.46 4.3234 -1 -1 2 2 20.63 19.79 4.3057 -1 1 2 2 20.65 20.05 4.3011 1 1 2 2 22.57 2.46 3.9399 -2 2 0 2 22.63 2.79 3.9289 2 2 0 2 23.34 76.03 3.8117 -2 0 2 2 23.35 76.33 3.8103 2 0 2 2 23.60 71.37 3.7694 0 -2 2 2 23.78 79.20 3.7412 0 2 2 2 24.96 1.30 3.5679 -3 1 0 2 25.00 1.60 3.5617 3 1 0 2 25.15 91.76 3.5414 -3 0 1 2 25.15 90.99 3.5405 3 0 1 2 25.61 1.95 3.4778 -1 3 0 2 25.66 2.16 3.4721 1 3 0 2 25.82 100.00 3.4504 0 -3 1 2 25.95 83.59 3.4342 0 3 1 2 27.10 11.91 3.2905 -1 0 3 2 27.10 11.85 3.2898 1 0 3 2 27.12 8.27 3.2881 0 -1 3 2 28.44 17.00 3.1389 2 -2 2 2 28.48 16.08 3.1341 -2 -2 2 2 28.58 31.39 3.1233 -2 2 2 2 28.64 30.77 3.1171 2 2 2 2 29.98 21.15 2.9805 3 -2 1 2 30.05 60.37 2.9740 -3 2 1 2 30.05 19.80 2.9739 -3 -2 1 2 30.13 58.53 2.9664 3 2 1 2 30.31 44.79 2.9488 2 -3 1 2 30.38 45.08 2.9422 -2 -3 1 2 30.41 8.26 2.9389 -2 3 1 2 30.43 40.79 2.9372 3 -1 2 2 30.46 43.77 2.9348 -3 -1 2 2 30.49 8.93 2.9317 2 3 1 2 30.49 26.93 2.9315 -3 1 2 2 30.54 28.72 2.9271 3 1 2 2 30.91 31.44 2.8931 1 -3 2 2 30.94 31.42 2.8901 -1 -3 2 2 31.12 24.09 2.8743 -1 3 2 2 31.16 24.03 2.8707 1 3 2 2 31.47 3.74 2.8431 2 -1 3 2 31.48 4.04 2.8419 -2 -1 3 2 31.61 4.35 2.8302 1 -2 3 2 31.63 4.10 2.8286 -1 -2 3 2 31.64 2.07 2.8275 4 0 0 2 31.81 15.66 2.8128 -1 2 3 2 31.84 15.42 2.8103 1 2 3 2 32.70 3.72 2.7387 0 4 0 2 34.14 46.88 2.6266 -3 3 0 2 34.23 47.44 2.6193 3 3 0 2 34.78 78.59 2.5792 0 0 4 2 35.32 28.13 2.5411 -3 0 3 2 35.33 28.24 2.5402 3 0 3 2 35.73 44.59 2.5129 0 -3 3 2 36.01 27.24 2.4941 0 3 3 2 36.22 8.04 2.4798 -4 0 2 2 36.24 7.90 2.4791 4 0 2 2 36.72 2.84 2.4475 -1 1 4 2 36.74 2.96 2.4465 1 1 4 2 37.05 5.76 2.4264 0 -4 2 2 38.35 6.25 2.3470 -2 0 4 2 38.36 6.60 2.3463 2 0 4 2 38.38 12.16 2.3455 3 -3 2 2 38.46 12.95 2.3408 -3 -3 2 2 38.54 5.34 2.3358 -3 3 2 2 38.64 5.56 2.3301 3 3 2 2 38.70 12.18 2.3267 0 2 4 2 38.97 14.36 2.3110 3 -2 3 2 39.02 13.51 2.3084 -3 -2 3 2 39.13 29.74 2.3019 -3 2 3 2 39.20 28.57 2.2979 3 2 3 2 39.21 17.20 2.2978 2 -3 3 2 39.26 17.16 2.2950 -2 -3 3 2 39.46 16.09 2.2839 -2 3 3 2 39.52 16.66 2.2802 2 3 3 2 39.82 5.70 2.2637 4 -2 2 2 39.89 5.56 2.2601 -4 -2 2 2 40.71 3.43 2.2165 -5 1 0 2 40.75 4.60 2.2140 5 1 0 2 40.84 14.62 2.2097 -5 0 1 2 40.84 14.99 2.2093 5 0 1 2 41.23 1.23 2.1897 4 -3 1 2 41.30 5.07 2.1858 -4 3 1 2 41.33 1.22 2.1843 -4 -3 1 2 41.42 5.21 2.1799 4 3 1 2 41.58 1.09 2.1717 3 -4 1 2 41.69 1.21 2.1664 -3 -4 1 2 41.76 2.73 2.1630 2 -2 4 2 41.79 2.59 2.1617 -2 -2 4 2 41.97 9.00 2.1528 -2 2 4 2 41.98 7.00 2.1521 -1 5 0 2 42.01 8.81 2.1505 2 2 4 2 42.03 7.01 2.1498 1 5 0 2 42.10 19.32 2.1464 0 -5 1 2 42.14 1.53 2.1444 4 -1 3 2 42.16 1.49 2.1433 -4 -1 3 2 42.23 41.54 2.1399 0 5 1 2 43.11 1.58 2.0984 -1 4 3 2 43.15 1.59 2.0966 1 4 3 2 43.24 2.00 2.0923 3 -1 4 2 43.25 2.37 2.0918 -3 -1 4 2 44.13 2.71 2.0520 5 -2 1 2 44.18 2.25 2.0500 -5 2 1 2 44.22 2.09 2.0484 -5 -2 1 2 44.27 1.85 2.0459 5 2 1 2 44.47 1.38 2.0373 5 -1 2 2 44.50 1.73 2.0359 -5 -1 2 2 44.63 23.27 2.0305 0 -1 5 2 44.64 5.76 2.0300 -1 0 5 2 44.64 5.79 2.0297 1 0 5 2 44.76 1.42 2.0249 0 1 5 2 45.14 1.52 2.0085 2 -5 1 2 45.23 1.49 2.0050 -2 -5 1 2 45.27 5.13 2.0032 -2 5 1 2 45.36 5.03 1.9995 2 5 1 2 45.80 3.11 1.9810 -1 5 2 2 45.85 3.19 1.9792 1 5 2 2 46.08 7.57 1.9699 -4 4 0 2 46.21 7.58 1.9644 4 4 0 2 47.21 2.77 1.9253 -5 3 0 2 47.33 3.34 1.9205 5 3 0 2 47.97 9.91 1.8966 -3 5 0 2 48.09 9.59 1.8920 3 5 0 2 48.14 1.77 1.8901 -5 0 3 2 48.16 1.77 1.8895 5 0 3 2 48.28 29.23 1.8850 6 0 0 2 48.63 3.42 1.8725 -4 3 3 2 48.68 2.78 1.8706 0 4 4 2 48.71 2.41 1.8693 3 -4 3 2 48.74 3.43 1.8684 4 3 3 2 48.80 2.73 1.8662 -3 -4 3 2 49.14 5.06 1.8541 0 -5 3 2 49.40 34.64 1.8450 3 -3 4 2 49.46 35.54 1.8430 -3 -3 4 2 49.50 2.01 1.8415 0 5 3 2 49.62 1.13 1.8372 -4 4 2 2 49.67 15.28 1.8356 -3 3 4 2 49.75 15.75 1.8326 3 3 4 2 49.76 1.13 1.8324 4 4 2 2 49.85 2.46 1.8294 6 -1 1 2 49.86 1.91 1.8288 -6 1 1 2 49.89 2.90 1.8280 -6 -1 1 2 49.92 2.31 1.8269 6 1 1 2 49.95 16.40 1.8258 0 6 0 2 50.41 7.90 1.8103 -3 0 5 2 50.43 8.06 1.8097 3 0 5 2 50.54 4.05 1.8060 5 -3 2 2 50.65 4.19 1.8023 -5 -3 2 2 50.65 14.28 1.8022 0 -3 5 2 50.67 2.48 1.8016 -5 3 2 2 50.80 2.84 1.7973 5 3 2 2 51.00 13.15 1.7906 0 3 5 2 51.03 6.73 1.7898 5 -2 3 2 51.09 5.97 1.7877 -5 -2 3 2 51.15 3.77 1.7858 -5 2 3 2 51.21 3.70 1.7839 -6 2 0 2 51.21 7.73 1.7837 3 -5 2 2 51.25 3.61 1.7827 5 2 3 2 51.30 3.38 1.7809 6 2 0 2 51.33 7.65 1.7801 -3 -5 2 2 51.37 2.34 1.7785 1 -6 1 2 51.42 2.43 1.7770 -1 -6 1 2 51.44 11.72 1.7764 -3 5 2 2 51.51 1.14 1.7741 -1 6 1 2 51.56 1.08 1.7725 1 6 1 2 51.56 11.62 1.7725 3 5 2 2 51.62 2.40 1.7707 -6 0 2 2 51.63 2.38 1.7703 6 0 2 2 51.86 2.08 1.7630 2 -5 3 2 51.93 1.96 1.7607 -2 -5 3 2 52.20 5.06 1.7523 -2 5 3 2 52.28 5.08 1.7497 2 5 3 2 53.08 6.30 1.7252 0 -6 2 2 53.18 3.96 1.7224 3 -2 5 2 53.21 3.66 1.7215 -3 -2 5 2 53.28 3.92 1.7195 0 0 6 2 53.34 5.33 1.7176 2 -3 5 2 53.35 1.25 1.7171 0 6 2 2 53.37 5.33 1.7166 -2 -3 5 2 53.39 12.06 1.7161 -3 2 5 2 53.45 11.64 1.7143 3 2 5 2 53.53 1.08 1.7118 4 -5 1 2 53.66 1.54 1.7079 -2 3 5 2 53.68 1.11 1.7074 -4 -5 1 2 53.72 1.63 1.7063 2 3 5 2 54.38 1.88 1.6870 6 -2 2 2 54.46 4.57 1.6849 -6 2 2 2 54.46 1.67 1.6848 -6 -2 2 2 54.56 1.51 1.6820 5 -1 4 2 54.56 4.25 1.6819 6 2 2 2 54.57 2.42 1.6817 1 -1 6 2 54.57 2.55 1.6817 -1 -1 6 2 54.58 1.79 1.6815 -5 -1 4 2 55.40 1.05 1.6584 1 -5 4 2 55.49 5.11 1.6560 6 -3 1 2 55.55 5.02 1.6544 -6 3 1 2 55.62 5.52 1.6525 -6 -3 1 2 55.66 2.26 1.6513 2 -6 2 2 55.69 5.11 1.6505 6 3 1 2 55.75 2.38 1.6490 -2 -6 2 2 55.84 2.00 1.6465 -1 5 4 2 55.88 1.96 1.6454 1 5 4 2 55.88 3.92 1.6453 -2 0 6 2 55.90 3.89 1.6449 2 0 6 2 55.92 1.42 1.6443 -2 6 2 2 55.93 5.76 1.6440 0 -2 6 2 56.01 1.51 1.6418 2 6 2 2 56.19 5.55 1.6370 0 2 6 2 56.60 5.28 1.6262 3 -6 1 2 56.72 3.02 1.6228 -3 6 1 2 56.73 5.67 1.6228 -3 -6 1 2 56.86 3.17 1.6193 3 6 1 2 57.92 1.92 1.5922 -1 6 3 2 57.97 1.99 1.5910 1 6 3 2 58.57 4.09 1.5759 -5 5 0 2 58.70 2.47 1.5729 -2 2 6 2 58.74 2.47 1.5720 2 2 6 2 58.75 3.96 1.5716 5 5 0 2 58.84 1.32 1.5694 4 -4 4 2 58.94 1.39 1.5670 -4 -4 4 2 59.23 1.14 1.5600 5 -4 3 2 59.36 1.42 1.5569 -5 -4 3 2 59.45 1.69 1.5548 -6 4 0 2 59.62 1.37 1.5507 6 4 0 2 59.64 6.86 1.5502 3 -1 6 2 59.65 7.24 1.5501 -3 -1 6 2 59.75 1.24 1.5477 -3 1 6 2 59.79 1.44 1.5468 3 1 6 2 59.84 2.55 1.5457 1 -3 6 2 59.85 2.58 1.5453 -1 -3 6 2 59.87 2.10 1.5449 -4 5 3 2 60.02 2.13 1.5413 4 5 3 2 60.07 1.97 1.5402 -5 3 4 2 60.20 2.17 1.5373 5 3 4 2 60.21 1.27 1.5371 -1 3 6 2 60.23 1.30 1.5364 1 3 6 2 60.40 4.94 1.5326 3 -5 4 2 60.49 4.70 1.5304 -3 -5 4 2 60.75 1.84 1.5247 -5 0 5 2 60.77 1.99 1.5241 5 0 5 2 60.80 3.40 1.5234 -3 5 4 2 60.86 9.42 1.5221 -6 0 4 2 60.88 9.45 1.5216 6 0 4 2 60.92 3.41 1.5207 3 5 4 2 61.22 1.97 1.5140 -4 3 5 2 61.23 1.01 1.5138 -3 -4 5 2 61.33 1.98 1.5116 4 3 5 2 61.43 4.73 1.5093 5 -5 2 2 61.44 4.38 1.5091 6 -3 3 2 61.50 1.85 1.5077 0 -5 5 2 61.55 4.48 1.5067 -6 -3 3 2 61.59 4.49 1.5057 -5 -5 2 2 61.61 3.49 1.5054 -6 3 3 2 61.63 5.49 1.5050 -5 5 2 2 61.75 3.73 1.5022 6 3 3 2 61.81 5.46 1.5010 5 5 2 2 62.02 8.56 1.4965 0 5 5 2 62.06 10.54 1.4955 0 -6 4 2 62.30 1.33 1.4903 6 -4 2 2 62.42 2.69 1.4878 3 -6 3 2 62.46 1.64 1.4869 -6 -4 2 2 62.53 2.92 1.4853 -3 -6 3 2 62.55 5.47 1.4849 0 6 4 2 62.78 1.94 1.4802 -3 6 3 2 62.91 2.22 1.4774 3 6 3 2 63.05 1.70 1.4744 4 -6 2 2 63.21 1.69 1.4711 -4 -6 2 2 63.29 1.20 1.4695 -4 6 2 2 63.29 1.29 1.4694 -4 0 6 2 63.31 1.30 1.4689 4 0 6 2 63.38 1.97 1.4675 -5 2 5 2 63.46 1.17 1.4659 4 6 2 2 63.48 1.81 1.4655 5 2 5 2 63.64 2.49 1.4621 0 -1 7 2 63.67 2.31 1.4615 -1 0 7 2 63.68 2.34 1.4614 1 0 7 2 64.48 1.02 1.4450 -2 -6 4 2 65.62 1.06 1.4228 7 -3 2 2 65.72 2.15 1.4208 -7 3 2 2 65.74 1.26 1.4204 0 7 3 2 65.75 1.00 1.4203 -7 -3 2 2 65.88 2.08 1.4178 7 3 2 2 65.95 3.34 1.4164 -6 5 1 2 66.00 1.93 1.4156 2 -1 7 2 66.00 1.94 1.4156 -2 -1 7 2 66.16 3.34 1.4125 6 5 1 2 66.27 1.34 1.4104 5 -6 1 2 66.31 3.92 1.4096 -1 2 7 2 66.33 3.88 1.4093 1 2 7 2 66.46 1.51 1.4067 -5 -6 1 2 67.84 1.02 1.3816 6 -1 5 2 67.85 1.24 1.3814 -6 -1 5 2 68.01 3.19 1.3785 -2 7 3 2 68.11 3.02 1.3767 2 7 3 2 68.33 2.48 1.3728 -3 0 7 2 68.35 2.52 1.3725 3 0 7 2 68.47 4.07 1.3703 0 -3 7 2 68.53 1.89 1.3693 0 8 0 2 68.85 2.44 1.3636 -8 0 2 2 68.87 2.48 1.3633 8 0 2 2 68.88 2.81 1.3631 0 3 7 2 68.90 1.23 1.3628 1 -6 5 2 68.94 1.32 1.3622 -1 -6 5 2 69.10 2.79 1.3593 5 -1 6 2 69.11 3.01 1.3593 -5 -1 6 2 69.76 1.99 1.3481 1 -5 6 2 69.78 1.96 1.3477 -1 -5 6 2 70.33 1.13 1.3386 -1 5 6 2 70.37 1.13 1.3379 1 5 6 2 71.10 3.33 1.3260 0 -8 2 2 71.12 1.23 1.3256 -2 3 7 2 71.17 1.22 1.3248 2 3 7 2 71.19 1.15 1.3244 8 -2 2 2 71.26 1.59 1.3234 -8 2 2 2 71.27 1.35 1.3233 6 -5 3 2 71.37 1.43 1.3215 8 2 2 2 71.40 4.19 1.3210 0 8 2 2 71.44 1.33 1.3204 -6 -5 3 2 71.89 4.68 1.3133 -6 6 0 2 72.12 4.98 1.3096 6 6 0 2 72.14 1.83 1.3094 8 -3 1 2 72.29 1.92 1.3070 -8 -3 1 2 72.53 2.90 1.3033 6 -3 5 2 72.62 3.16 1.3019 -6 -3 5 2 72.78 1.27 1.2993 -6 3 5 2 72.93 1.40 1.2972 6 3 5 2 73.29 1.32 1.2917 2 -8 2 2 73.37 2.12 1.2904 3 -6 5 2 73.38 1.27 1.2902 -2 -8 2 2 73.43 6.61 1.2896 0 0 8 2 73.47 2.31 1.2889 -3 -6 5 2 73.74 1.53 1.2848 5 -3 6 2 73.81 1.54 1.2838 -5 -3 6 2 74.11 1.36 1.2794 3 -8 1 2 74.21 1.23 1.2779 3 -5 6 2 74.26 5.59 1.2772 -3 8 1 2 74.26 1.41 1.2772 -3 -8 1 2 74.29 1.20 1.2767 -3 -5 6 2 74.41 5.63 1.2749 3 8 1 2 74.71 1.43 1.2706 -6 0 6 2 74.74 1.50 1.2701 6 0 6 2 74.76 4.74 1.2699 -3 5 6 2 74.87 4.72 1.2683 3 5 6 2 74.91 1.01 1.2677 6 6 2 2 75.57 1.30 1.2582 -3 7 4 2 75.63 1.03 1.2574 -2 0 8 2 75.64 1.06 1.2572 2 0 8 2 75.70 3.65 1.2565 0 -6 6 2 75.72 1.23 1.2562 3 7 4 2 76.37 1.03 1.2471 0 6 6 2 77.12 1.28 1.2367 -6 2 6 2 77.23 1.14 1.2353 6 2 6 2 77.54 2.02 1.2311 -8 3 3 2 77.72 2.24 1.2288 8 3 3 2 77.84 1.01 1.2272 0 -5 7 2 77.85 1.48 1.2270 2 -6 6 2 77.92 1.52 1.2261 -2 -6 6 2 78.90 1.08 1.2132 0 -8 4 2 79.17 1.90 1.2099 0 -9 1 2 79.22 4.60 1.2091 3 -8 3 2 79.37 4.67 1.2073 -3 -8 3 2 79.66 2.00 1.2036 -5 2 7 2 79.76 1.94 1.2024 5 2 7 2 79.98 1.50 1.1996 2 -5 7 2 80.03 1.45 1.1989 -2 -5 7 2 80.81 1.34 1.1893 -9 3 0 2 80.98 1.42 1.1872 9 3 0 2 82.06 1.90 1.1743 5 -6 5 2 82.15 2.76 1.1733 -6 5 5 2 82.20 2.26 1.1727 6 -6 4 2 82.23 2.00 1.1724 -5 -6 5 2 82.36 2.75 1.1708 6 5 5 2 82.40 2.50 1.1704 -6 -6 4 2 82.61 1.14 1.1679 -6 6 4 2 82.86 1.32 1.1651 6 6 4 2 82.88 2.48 1.1648 5 -5 6 2 83.01 2.35 1.1633 -5 -5 6 2 83.31 3.50 1.1600 3 -3 8 2 83.34 3.50 1.1596 -3 -3 8 2 83.72 1.77 1.1552 -3 3 8 2 83.80 1.88 1.1544 3 3 8 2 84.29 1.09 1.1489 4 -6 6 2 84.42 1.08 1.1475 -4 -6 6 2 84.67 2.14 1.1447 0 9 3 2 85.01 1.18 1.1410 0 -1 9 2 85.94 1.80 1.1310 10 0 0 2 86.62 1.04 1.1238 -5 4 7 2 86.72 1.01 1.1228 7 -3 6 2 86.82 1.04 1.1218 -7 -3 6 2 87.69 1.06 1.1129 8 -3 5 2 87.80 1.09 1.1118 -8 -3 5 2 88.10 1.25 1.1087 6 -3 7 2 88.18 1.26 1.1080 -6 -3 7 2 88.18 1.15 1.1080 -5 8 3 2 88.44 1.17 1.1054 5 8 3 2 88.95 1.02 1.1004 -3 -6 7 2 89.31 1.54 1.0968 -3 0 9 2 89.34 1.58 1.0966 3 0 9 2 89.40 2.56 1.0960 0 -3 9 2 89.46 1.27 1.0955 0 10 0 2 89.60 1.32 1.0941 -3 6 7 2 89.72 1.44 1.0929 3 6 7 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.