Gillulyite Foit F F, Robinson P D, Wilson J R American Mineralogist 80 (1995) 394-399 The crystal structure of gillulyite, Tl2(As,Sb)8S13, from the Mercur gold deposit, Tooele County, Utah, U.S.A _database_code_amcsd 0001733 CELL PARAMETERS: 9.5840 5.6790 21.5010 90.000 100.070 90.000 SPACE GROUP: P2/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 1152.219 Density (g/cm3): 4.136 MAX. ABS. INTENSITY / VOLUME**2: 15.64160708 RIR: 1.231 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.91 4.16 8.1078 1 0 1 2 14.30 16.99 6.1945 -1 0 3 2 16.16 12.17 5.4851 0 1 1 4 16.75 32.42 5.2924 0 0 4 2 16.95 4.90 5.2296 1 0 3 2 17.72 19.73 5.0042 0 1 2 4 18.23 20.07 4.8658 1 1 0 4 18.81 46.36 4.7182 2 0 0 2 19.08 4.31 4.6515 1 1 1 4 20.07 3.63 4.4242 0 1 3 4 20.77 1.24 4.2771 1 1 2 4 21.22 34.30 4.1861 -1 1 3 4 21.45 100.00 4.1430 -1 0 5 2 21.93 16.80 4.0539 2 0 2 2 22.97 33.52 3.8718 0 1 4 4 23.12 6.20 3.8470 1 1 3 4 23.70 31.20 3.7546 -1 1 4 4 24.32 3.52 3.6598 -2 1 1 4 24.50 54.77 3.6330 1 0 5 2 24.53 76.35 3.6291 2 1 0 4 24.84 10.27 3.5840 -2 1 2 4 25.45 7.62 3.4994 2 1 1 4 25.97 20.45 3.4312 1 1 4 4 26.25 12.80 3.3944 0 1 5 4 26.63 29.98 3.3470 -1 1 5 4 27.02 16.83 3.2995 2 1 2 4 27.44 35.69 3.2508 2 0 4 2 27.88 2.31 3.2005 -2 1 4 4 27.94 2.76 3.1935 -3 0 1 2 28.83 22.00 3.0973 -2 0 6 2 28.99 42.27 3.0802 -3 0 3 2 29.14 2.63 3.0641 2 1 3 4 29.18 38.44 3.0603 1 1 5 4 29.40 1.96 3.0385 -1 0 7 2 29.43 26.50 3.0351 3 0 1 2 29.81 2.08 2.9970 0 1 6 4 31.51 26.04 2.8395 0 2 0 2 31.80 54.37 2.8143 0 2 1 4 32.16 1.74 2.7836 -3 1 1 4 32.35 8.06 2.7671 -3 0 5 2 32.54 1.90 2.7516 3 1 0 4 32.63 13.88 2.7439 1 0 7 2 32.65 1.06 2.7425 0 2 2 4 32.67 2.08 2.7413 1 1 6 4 32.94 26.40 2.7191 1 2 0 4 33.08 4.11 2.7076 -3 1 3 4 33.15 6.64 2.7026 3 0 3 2 33.45 4.31 2.6791 -1 1 7 4 33.57 1.63 2.6693 0 1 7 4 33.61 1.00 2.6661 -1 2 2 4 33.87 2.64 2.6462 0 0 8 2 34.03 6.27 2.6342 0 2 3 4 34.29 32.88 2.6148 2 0 6 2 34.36 11.28 2.6102 -3 1 4 4 34.65 3.80 2.5888 2 1 5 4 34.92 5.08 2.5691 3 1 2 4 35.89 43.05 2.5022 -2 0 8 2 35.99 2.01 2.4954 1 2 3 4 36.11 34.86 2.4876 -3 1 5 4 36.38 2.30 2.4697 -1 2 4 4 36.83 27.40 2.4404 3 1 3 4 37.48 7.38 2.3998 -3 0 7 2 37.50 16.41 2.3986 0 1 8 4 37.58 23.59 2.3932 -4 0 2 2 37.76 3.89 2.3822 -1 0 9 2 37.88 1.36 2.3751 2 1 6 4 38.02 6.20 2.3667 -2 2 3 4 38.15 3.34 2.3591 4 0 0 2 38.16 7.95 2.3583 0 2 5 4 38.43 1.42 2.3422 -1 2 5 4 38.52 14.97 2.3369 3 0 5 2 39.34 1.73 2.2903 -2 2 4 4 40.23 1.80 2.2414 1 1 8 4 40.29 5.28 2.2387 2 2 3 4 40.61 2.01 2.2216 4 0 2 2 40.82 3.10 2.2105 -3 1 7 4 40.87 2.06 2.2082 -1 2 6 4 40.92 4.53 2.2053 -4 1 2 4 41.09 1.15 2.1968 -1 1 9 4 41.56 3.55 2.1732 0 1 9 4 41.80 1.31 2.1611 3 1 5 4 42.26 4.10 2.1386 2 2 4 4 43.22 3.34 2.0930 -2 2 6 4 43.34 1.41 2.0877 -3 2 3 4 43.65 1.51 2.0735 3 2 1 4 43.70 2.82 2.0715 -2 0 10 2 43.85 3.85 2.0648 -3 0 9 2 44.26 1.96 2.0467 1 1 9 4 44.60 3.59 2.0318 2 2 5 4 44.71 4.49 2.0270 4 0 4 2 45.74 9.94 1.9836 0 1 10 4 45.79 3.01 1.9818 -3 2 5 4 46.38 2.65 1.9576 3 2 3 4 46.68 1.70 1.9460 -1 2 8 4 46.82 3.88 1.9405 -3 1 9 4 46.90 5.83 1.9372 -4 0 8 2 47.26 2.24 1.9235 2 2 6 4 47.59 7.85 1.9107 -3 2 6 4 47.64 1.36 1.9090 4 1 4 4 47.98 5.19 1.8960 3 1 7 4 48.06 2.83 1.8930 0 3 0 2 48.32 14.86 1.8838 3 2 4 4 48.49 2.12 1.8773 -2 2 8 4 48.88 1.61 1.8634 0 3 2 4 49.13 1.12 1.8545 -1 3 1 4 49.21 3.37 1.8514 5 0 1 2 49.24 1.79 1.8504 1 2 8 4 49.31 2.40 1.8481 -5 0 5 2 49.33 2.53 1.8475 -1 1 11 4 49.44 2.68 1.8434 1 3 1 4 49.83 1.03 1.8299 -4 2 2 4 49.88 2.16 1.8284 0 3 3 4 50.00 1.25 1.8243 1 0 11 2 50.13 3.48 1.8196 4 0 6 2 50.19 2.31 1.8175 1 3 2 4 50.20 3.01 1.8173 2 2 7 4 50.23 15.18 1.8165 2 0 10 2 50.42 1.34 1.8100 -5 1 1 4 50.45 1.21 1.8090 -5 1 3 4 51.44 1.70 1.7764 3 1 8 4 51.55 8.44 1.7728 -2 2 9 4 51.62 11.01 1.7706 -1 3 4 4 51.82 8.69 1.7641 0 0 12 2 51.95 2.20 1.7602 5 1 1 4 52.04 2.91 1.7574 -5 1 5 4 52.06 1.45 1.7569 2 3 0 4 52.08 7.19 1.7562 -2 0 12 2 52.22 6.61 1.7517 -3 2 8 4 52.22 1.57 1.7517 -2 3 2 4 52.32 6.29 1.7485 5 0 3 2 52.47 7.12 1.7439 -5 0 7 2 52.49 1.57 1.7432 3 0 9 2 52.55 9.29 1.7415 2 3 1 4 52.70 3.85 1.7369 1 1 11 4 52.81 1.01 1.7334 -4 0 10 2 52.83 8.40 1.7329 1 3 4 4 52.88 4.25 1.7315 -2 3 3 4 53.17 2.03 1.7228 3 2 6 4 53.27 1.00 1.7196 5 1 2 4 53.39 1.48 1.7161 -5 1 6 4 53.42 1.47 1.7152 2 3 2 4 53.91 4.28 1.7008 -2 3 4 4 54.03 1.15 1.6972 0 2 10 4 54.46 1.68 1.6847 0 1 12 4 54.99 1.82 1.6700 -3 2 9 4 55.05 4.59 1.6681 0 3 6 4 55.09 1.51 1.6671 -5 1 7 4 55.11 1.60 1.6665 3 1 9 4 55.57 3.74 1.6539 -1 0 13 2 56.03 1.28 1.6413 3 2 7 4 56.23 2.85 1.6359 2 3 4 4 56.76 1.94 1.6219 3 3 0 4 56.77 1.50 1.6216 5 0 5 2 56.85 7.05 1.6197 2 2 9 4 56.97 2.39 1.6164 -5 0 9 2 57.74 17.42 1.5968 -6 0 2 2 57.95 9.10 1.5915 -3 3 4 4 58.06 5.24 1.5887 -5 2 2 4 58.09 3.36 1.5879 -1 1 13 4 58.20 1.26 1.5851 -6 0 4 2 58.33 5.86 1.5820 3 3 2 4 58.40 2.42 1.5803 -2 2 11 4 58.74 1.78 1.5718 5 2 0 4 58.80 1.35 1.5704 -5 2 4 4 59.13 2.40 1.5624 -3 3 5 4 59.15 1.81 1.5619 -3 0 13 2 59.24 2.01 1.5597 1 0 13 2 59.26 2.77 1.5592 5 1 5 4 59.45 2.00 1.5547 -5 1 9 4 59.62 1.64 1.5509 5 2 1 4 59.63 2.89 1.5505 3 3 3 4 59.70 1.43 1.5489 -5 2 5 4 59.71 2.32 1.5486 -4 0 12 2 60.07 1.25 1.5401 -6 0 6 2 60.51 1.18 1.5302 2 2 10 4 61.45 1.31 1.5088 2 1 12 4 61.58 2.54 1.5060 -3 1 13 4 61.92 1.97 1.4985 0 2 12 4 62.39 2.92 1.4885 5 0 7 2 62.63 2.04 1.4834 -5 0 11 2 62.88 1.12 1.4779 -4 3 3 4 63.03 8.39 1.4747 0 3 9 4 63.04 1.89 1.4747 3 1 11 4 64.38 1.17 1.4470 -5 2 8 4 64.64 1.74 1.4420 -3 3 8 4 65.47 1.21 1.4257 3 3 6 4 65.94 5.80 1.4166 0 4 1 4 66.12 1.33 1.4132 3 2 10 4 66.15 5.79 1.4126 0 2 13 4 66.23 2.32 1.4111 0 3 10 4 67.08 1.80 1.3954 -3 3 9 4 67.27 1.90 1.3919 0 4 3 4 67.27 2.20 1.3918 -6 2 2 4 67.53 1.45 1.3871 1 4 2 4 67.55 2.37 1.3867 -6 2 1 4 68.01 1.58 1.3785 3 3 7 4 68.72 1.46 1.3658 -1 4 4 4 69.36 1.77 1.3548 -7 0 5 2 69.48 1.53 1.3528 3 0 13 2 69.80 1.20 1.3475 -3 3 10 4 69.99 1.38 1.3443 -6 1 10 4 70.13 1.48 1.3419 -3 1 15 4 70.82 2.32 1.3304 3 3 8 4 71.24 1.07 1.3236 5 3 1 4 71.28 2.45 1.3231 0 0 16 2 71.28 1.75 1.3230 5 1 9 4 71.55 1.12 1.3187 -5 1 13 4 71.72 1.46 1.3160 3 1 13 4 72.26 1.37 1.3074 4 0 12 2 72.35 2.87 1.3060 5 3 2 4 72.45 3.38 1.3045 -5 3 6 4 73.02 1.27 1.2958 -3 4 2 4 73.20 1.37 1.2930 1 4 6 4 73.68 1.40 1.2858 -7 1 7 4 75.18 1.43 1.2638 0 2 15 4 76.05 1.25 1.2515 -3 3 12 4 76.58 1.50 1.2442 -3 4 6 4 76.65 1.29 1.2432 5 0 11 2 76.96 1.87 1.2389 -5 0 15 2 77.13 1.19 1.2367 3 4 4 4 77.32 1.55 1.2340 -3 0 17 2 77.70 1.06 1.2289 6 1 8 4 78.59 1.02 1.2173 -4 4 3 4 78.59 1.99 1.2173 2 4 7 4 79.66 2.97 1.2036 -2 4 9 4 80.55 1.36 1.1926 -1 3 14 4 81.49 1.10 1.1811 1 1 17 4 81.91 2.02 1.1761 0 0 18 2 82.36 1.19 1.1709 -8 1 4 4 83.99 1.77 1.1522 2 4 9 4 84.16 1.34 1.1504 8 0 2 2 86.86 1.19 1.1214 0 5 3 4 87.31 2.55 1.1168 -8 0 10 2 87.65 1.00 1.1133 -3 0 19 2 87.90 1.82 1.1108 8 0 4 2 89.51 1.05 1.0949 4 4 7 4 89.59 1.44 1.0942 3 0 17 2 89.65 1.08 1.0936 -7 3 6 4 89.76 1.35 1.0925 -6 3 11 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.