Leonite Hertweck B, Giester G, Libowitzky E American Mineralogist 86 (2001) 1282-1292 The crystal structures of the low-temperature phases of leonite-type compounds, K2Me(SO4)2.4H2O (Me=Mg,Mn,Fe) Sample: K2Mn(SO4)2.4H2O, T = 293 K _database_code_amcsd 0002732 CELL PARAMETERS: 12.0170 9.5940 9.9490 90.000 95.030 90.000 SPACE GROUP: C2/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 1142.614 Density (g/cm3): 2.309 MAX. ABS. INTENSITY / VOLUME**2: 9.038518583 RIR: 1.274 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 14.43 24.65 6.1377 -1 1 1 4 14.80 11.67 5.9854 2 0 0 2 15.22 8.94 5.8220 1 1 1 4 16.62 6.17 5.3347 -2 0 1 2 17.90 23.27 4.9553 0 0 2 2 17.97 2.21 4.9356 2 0 1 2 18.50 28.66 4.7970 0 2 0 2 20.95 8.85 4.2405 -1 1 2 4 22.05 11.38 4.0316 1 1 2 4 23.77 1.34 3.7432 2 2 0 4 24.96 7.16 3.5670 -2 2 1 4 25.10 65.69 3.5485 -3 1 1 4 25.85 100.00 3.4466 0 2 2 4 25.90 3.73 3.4399 2 2 1 4 26.48 51.85 3.3655 3 1 1 4 28.90 7.27 3.0896 1 3 0 4 28.94 5.25 3.0855 -1 1 3 4 29.01 2.70 3.0784 -3 1 2 4 29.10 19.12 3.0688 -2 2 2 4 29.72 1.62 3.0059 -2 0 3 2 29.86 2.61 2.9927 4 0 0 2 30.10 3.67 2.9688 -1 3 1 4 30.43 7.21 2.9371 -4 0 1 2 30.50 1.90 2.9309 1 3 1 4 30.71 8.57 2.9110 2 2 2 4 31.99 7.73 2.7978 4 0 1 2 32.07 15.92 2.7906 2 0 3 2 32.92 1.95 2.7208 0 2 3 4 33.60 12.17 2.6673 -4 0 2 2 33.84 3.74 2.6488 -1 3 2 4 34.56 2.44 2.5955 1 3 2 4 34.98 1.46 2.5650 -3 1 3 4 35.23 3.15 2.5471 -2 2 3 4 35.35 10.56 2.5391 4 2 0 4 35.85 2.63 2.5048 -4 2 1 4 36.26 6.76 2.4777 0 0 4 2 36.41 1.43 2.4678 4 0 2 2 37.20 4.57 2.4168 4 2 1 4 37.28 15.94 2.4121 2 2 3 4 37.50 20.43 2.3985 0 4 0 2 37.61 12.86 2.3916 -1 1 4 4 37.65 4.84 2.3891 3 3 1 4 38.03 1.69 2.3662 3 1 3 4 38.79 5.35 2.3215 -4 0 3 2 38.91 2.00 2.3146 1 1 4 4 39.48 2.19 2.2825 -1 3 3 4 40.42 4.74 2.2315 1 3 3 4 41.27 11.54 2.1876 -2 4 1 4 41.51 2.02 2.1756 -5 1 2 4 41.84 1.97 2.1589 0 4 2 4 41.88 4.45 2.1573 2 4 1 4 42.64 5.16 2.1203 -2 2 4 4 43.30 7.15 2.0897 -4 2 3 4 44.27 2.45 2.0459 -3 3 3 4 44.46 1.21 2.0377 5 1 2 4 44.97 3.31 2.0158 2 2 4 4 45.46 15.96 1.9951 6 0 0 2 46.76 1.50 1.9426 -1 1 5 4 46.81 3.95 1.9407 3 3 3 4 47.01 2.82 1.9329 -2 0 5 2 47.56 1.18 1.9119 1 3 4 4 48.13 4.22 1.8906 1 1 5 4 48.65 3.62 1.8716 4 4 0 4 48.81 1.18 1.8657 -1 5 1 4 49.04 1.91 1.8577 -4 4 1 4 49.08 3.97 1.8562 1 5 1 4 49.45 5.93 1.8431 -4 2 4 4 49.79 1.74 1.8312 4 0 4 2 50.09 4.13 1.8210 4 4 1 4 50.46 1.19 1.8085 -3 3 4 4 50.94 1.22 1.7928 -2 2 5 4 51.22 3.40 1.7835 -4 4 2 4 51.51 2.75 1.7742 -6 2 2 4 52.38 2.23 1.7468 5 3 2 4 53.15 12.04 1.7233 0 4 4 4 53.26 4.62 1.7200 4 4 2 4 53.44 1.96 1.7146 -3 5 1 4 53.48 2.04 1.7133 2 2 5 4 53.57 2.62 1.7108 4 2 4 4 54.19 1.60 1.6927 3 5 1 4 54.30 1.10 1.6894 3 1 5 4 54.43 1.95 1.6858 -1 3 5 4 54.49 3.64 1.6840 -7 1 1 4 54.53 5.70 1.6828 6 2 2 4 56.20 2.67 1.6366 7 1 1 4 56.38 1.23 1.6319 -1 1 6 4 56.48 2.26 1.6293 -2 0 6 2 57.65 1.87 1.5990 0 6 0 2 57.80 2.16 1.5953 -3 3 5 4 57.82 1.15 1.5947 1 1 6 4 59.16 1.41 1.5618 0 2 6 4 59.33 1.17 1.5576 2 0 6 2 59.38 1.04 1.5565 -3 5 3 4 59.43 2.92 1.5553 -7 1 3 4 59.44 1.63 1.5550 -3 1 6 4 60.32 1.08 1.5344 -4 4 4 4 60.35 3.19 1.5338 6 4 0 4 60.88 4.93 1.5217 0 6 2 4 61.30 1.14 1.5122 3 3 5 4 61.45 1.45 1.5089 4 2 5 4 61.46 1.06 1.5087 3 5 3 4 61.48 2.97 1.5083 -7 3 1 4 62.25 1.05 1.4914 6 0 4 2 63.07 3.63 1.4740 7 3 1 4 63.23 1.29 1.4706 -1 3 6 4 64.23 1.24 1.4502 7 1 3 4 66.27 1.94 1.4103 4 6 0 4 67.08 1.77 1.3953 4 0 6 2 69.92 2.16 1.3454 -6 4 4 4 70.64 1.06 1.3335 7 3 3 4 73.40 1.05 1.2900 -3 7 1 4 74.12 1.19 1.2792 3 5 5 4 74.28 1.38 1.2768 -7 5 1 4 74.50 1.01 1.2736 -4 4 6 4 74.55 1.12 1.2729 8 2 3 4 74.99 1.59 1.2665 6 4 4 4 75.74 2.35 1.2558 7 5 1 4 77.49 1.25 1.2318 7 1 5 4 77.93 1.20 1.2260 -6 6 2 4 78.54 1.10 1.2179 -7 5 3 4 80.01 1.76 1.1992 0 8 0 2 81.80 1.31 1.1774 2 4 7 4 83.17 1.09 1.1615 10 2 0 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.