Sartorite Berlepsch P, Armbruster T, Makovicky E, Topa D American Mineralogist 88 (2003) 450-461 Another step toward understanding the true nature of sartorite: Determination and refinement of a ninefold superstructure _database_code_amcsd 0002988 37.71 7.898 20.106 90 101.993 90 P2_1/c atom x y z occ Uiso U(1,1) U(2,2) U(3,3) U(1,2) U(1,3) U(2,3) Pb1 .11812 .06199 .31086 .0540 .0477 .0568 .0562 -.0069 .0081 -.0040 Pb2 .23129 .08379 .31078 .0599 .0549 .0565 .0731 .0134 .0243 .0047 Pb3 .34273 -.59717 -.18503 .0514 .0440 .0579 .0511 .0050 .0068 -.0009 Pb4 .45338 .09418 .31461 .0568 .0473 .0461 .0815 -.0002 .0233 .0013 Pb5 .43835 .64077 .18296 .0533 .0390 .0641 .0571 -.0012 .0107 -.0053 Pb6 .33030 -.40497 .20582 .0488 .0395 .0475 .0587 .0047 .0083 -.0047 Pb7 .21828 -.41642 .20383 .0613 .0420 .0603 .0830 -.0081 .0158 -.0065 Pb8 -.10761 .07053 .29305 .0553 .0446 .0538 .0684 -.0090 .0139 -.0078 Pb9 .00536 .07666 .29546 .0533 .0515 .0526 .0606 .0141 .0224 .0094 As1 .14473 -.1612 .50326 .0409 .0350 .0437 .0434 .0000 .0064 .0062 As2 -.14122 .4970 .37925 .0383 .0373 .0384 .0403 .0025 .0101 -.0036 As3 .23534 -.1793 .48906 .0439 .0441 .0476 .0403 -.0098 .0095 -.0078 As4 .26684 -.0059 .13459 .0415 .0367 .0423 .0422 .0015 .0009 -.0037 Pb5a .36331 -.2758 -.0178 .318 .0407 As5b .36549 -.3088 -.0044 .682 .0486 As6 .36103 .0221 .11955 .0454 .0537 .0401 .0448 .0008 .0158 .0017 As7 .46747 .7081 .01033 .0481 .0391 .0606 .0448 .0003 .0090 .0008 As8 .49761 .0354 .13258 .0421 .0377 .0392 .0487 .0031 .0074 -.0005 As9a .4085 -.7093 .0103 .67 .057 .076 .045 .059 .001 .032 -.002 As9b .4224 -.6619 .0197 .33 .022 .011 .016 .036 -.012 -.002 -.005 As10 .40337 .5095 .36345 .0421 .0381 .0453 .0423 .0012 .0070 .0047 As11 .30861 .1850 .49187 .0378 .0374 .0409 .0347 .0055 .0068 .0009 As12 .28781 .5218 .38204 .0678 .118 .0452 .0497 -.0336 .0392 -.0138 Pb13a .19864 .2524 .5261 .218 .0376 .042 .027 .045 -.007 .012 -.005 As13b .20500 .1935 .5417 .782 .0515 .046 .037 .078 .0021 .028 .015 As14 .18075 .4819 .36831 .0391 .0308 .0448 .0404 .0008 .0044 .0032 As15 .07986 .1697 .49597 .0440 .0349 .0440 .0488 -.0001 -.0008 .0082 As16 .07553 .4960 .38595 .0485 .0631 .0360 .0404 .0023 -.0029 -.0027 As17 .01729 -.1830 .47361 .0542 .0559 .0583 .0452 .0082 .0028 -.0035 As18 .04364 -.0260 .13245 .0367 .0326 .0374 .0388 -.0002 .0045 -.0060 S1 .05914 .3548 .2860 .0369 .035 .037 .037 -.0041 .002 -.004 S2 .06506 -.0469 .4188 .0513 .059 .037 .055 -.005 .003 .003 S3 -.10464 .2996 .4432 .0413 .034 .049 .040 .000 .007 .007 S4 .09407 .1477 .1533 .0364 .035 .033 .042 -.0021 .009 .001 S5 .17148 .3363 .2698 .0446 .037 .038 .057 -.002 .007 -.011 S6 .19372 .0068 .4287 .0415 .048 .045 .033 -.002 .012 .000 S7 .19347 -.3325 .5384 .0495 .034 .044 .071 -.003 .012 .006 S8 .22449 .1691 .1605 .0440 .039 .045 .047 .001 .006 -.001 S9 .28301 .3747 .2853 .0378 .038 .037 .039 .0022 .009 -.001 S10 .30124 -.0384 .4208 .0483 .055 .036 .056 -.002 .017 .001 S11 .32402 -.1802 .0648 .0640 .074 .048 .063 -.006 -.004 -.011 S12 .31640 .1724 .1581 .0404 .043 .028 .050 -.003 .009 .003 S13 .39195 .3540 .2686 .0462 .037 .040 .059 .004 .006 -.008 S14 .40903 -.5148 -.0741 .0431 .042 .048 .040 -.007 .009 -.002 S15 .42766 .8592 .0598 .0519 .055 .042 .065 .009 .026 .008 S16 .49967 .8788 .2270 .0504 .049 .053 .050 -.012 .013 .000 S17 .47646 .4724 .0782 .0477 .047 .042 .059 .006 .022 .003 S18 .52090 .8488 .0661 .0444 .043 .048 .041 .001 .006 .002 S19 .55163 .1855 .1625 .0409 .038 .039 .046 -.004 .009 -.001 S20 .38472 -.1184 .2156 .0444 .039 .043 .050 .004 .006 .001 S21 .37864 -.5356 .0741 .0413 .037 .041 .044 -.005 .004 .001 S22 .34784 .3424 .4425 .0436 .043 .037 .052 -.002 .011 .003 S23 .35571 .6851 .3407 .0426 .039 .041 .048 -.001 .010 -.004 S24 .27767 -.1522 .2326 .0402 .032 .038 .052 .0004 .011 .002 S25 .25394 .0133 .5763 .0378 .037 .039 .037 -.003 .004 -.001 S26 .25844 .3409 .4415 .0427 .030 .046 .053 .005 .009 .012 S27 .22385 .6686 .3448 .0388 .040 .037 .037 .002 .001 -.006 S28 -.16240 .3520 .2827 .0397 .034 .039 .046 -.002 .006 -.004 S29 .15915 .0510 .5842 .0440 .044 .040 .047 .007 .004 .006 S30 .11955 .3154 .4432 .0439 .035 .052 .043 .002 .006 .007 S31 -.13158 .1553 .1522 .0400 .042 .039 .039 .000 .008 .002 S32 -.05376 .3321 .2670 .0398 .035 .038 .046 .002 .008 -.004 S33 -.02922 -.0020 .4273 .0363 .036 .042 .031 -.004 .006 .001 S34 .03377 .3475 .4558 .068 .035 .048 .116 .001 .003 .022 S35 .00347 .1617 .1550 .0365 .036 .037 .036 .004 .009 .002