Bikitaite Ferro O, Quartieri S, Vezzalini G, Ceriani C, Fois E, Gamba A, Cruciani G American Mineralogist 89 (2004) 94-101 Dehydration dynamics of bikitaite: I. In situ synchrotron powder X-ray diffraction study Sample: T = 30 C Locality: Bikita, Zimbabwe _database_code_amcsd 0003188 CELL PARAMETERS: 8.6121 4.9579 7.6040 89.892 114.423 89.955 SPACE GROUP: P1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 295.621 Density (g/cm3): 2.317 MAX. ABS. INTENSITY / VOLUME**2: 5.323905626 RIR: 0.748 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.28 41.45 7.8415 1 0 0 1 12.79 28.57 6.9236 0 0 1 1 13.10 13.49 6.7585 -1 0 1 1 20.32 29.83 4.3703 1 0 1 1 20.92 7.80 4.2467 -2 0 1 1 21.19 70.01 4.1938 1 1 0 1 21.22 64.28 4.1873 -1 1 0 1 22.08 1.25 4.0263 0 -1 1 1 22.23 8.89 3.9993 -1 1 1 1 22.25 5.25 3.9959 -1 -1 1 1 22.68 3.81 3.9207 2 0 0 1 23.41 8.68 3.8002 -1 0 2 1 25.73 100.00 3.4618 0 0 2 1 26.37 80.50 3.3792 -2 0 2 1 27.17 24.19 3.2825 1 1 1 1 27.23 24.00 3.2744 1 -1 1 1 27.65 21.03 3.2258 -2 -1 1 1 27.66 19.61 3.2247 -2 1 1 1 29.01 16.00 3.0779 2 1 0 1 29.06 15.78 3.0727 -2 1 0 1 29.65 1.33 3.0134 -1 -1 2 1 30.50 5.87 2.9313 2 0 1 1 31.18 10.16 2.8685 -3 0 1 1 32.04 4.25 2.7935 -2 1 2 1 32.07 1.04 2.7912 -2 -1 2 1 35.54 11.25 2.5258 2 1 1 1 35.62 9.51 2.5207 2 -1 1 1 36.09 1.91 2.4890 -2 0 3 1 36.16 20.41 2.4838 -3 -1 1 1 36.19 15.26 2.4819 -3 1 1 1 36.24 38.72 2.4789 0 2 0 1 37.12 1.41 2.4219 1 1 2 1 37.21 1.03 2.4167 1 -1 2 1 38.08 3.23 2.3630 -3 1 2 1 38.09 3.50 2.3628 -3 -1 2 1 38.55 1.10 2.3357 0 2 1 1 38.61 2.94 2.3321 0 -2 1 1 38.68 2.72 2.3280 -1 2 1 1 38.98 1.72 2.3105 -3 1 0 1 40.19 1.88 2.2436 -1 1 3 1 40.27 2.16 2.2398 -1 -1 3 1 41.85 1.03 2.1585 1 2 1 1 44.14 3.04 2.0517 -3 1 3 1 44.17 2.72 2.0503 -3 -1 3 1 44.92 3.58 2.0178 0 2 2 1 45.03 3.56 2.0132 0 -2 2 1 45.32 5.86 2.0012 1 0 3 1 45.35 4.30 1.9996 -2 2 2 1 45.39 4.27 1.9980 -2 -2 2 1 45.65 3.82 1.9873 3 1 1 1 45.73 3.03 1.9841 3 -1 1 1 46.31 5.14 1.9604 4 0 0 1 46.52 1.30 1.9521 -4 -1 2 1 46.78 1.46 1.9419 -4 0 3 1 47.87 12.01 1.9001 -2 0 4 1 48.01 1.79 1.8950 2 2 1 1 48.13 1.24 1.8907 2 -2 1 1 48.52 2.45 1.8764 -3 -2 1 1 48.56 1.91 1.8748 -3 2 1 1 49.05 6.03 1.8573 1 1 3 1 49.14 5.87 1.8541 1 -1 3 1 50.00 1.10 1.8241 4 1 0 1 50.47 2.45 1.8084 -4 1 3 1 50.48 1.64 1.8079 -4 -1 3 1 51.54 1.44 1.7732 -2 -1 4 1 51.74 1.02 1.7667 -1 2 3 1 53.78 1.67 1.7045 2 0 3 1 55.59 2.92 1.6533 -5 0 3 1 56.95 1.27 1.6170 -4 -2 1 1 56.97 2.52 1.6165 -1 3 0 1 57.10 2.42 1.6132 2 1 3 1 57.19 1.61 1.6106 2 -1 3 1 58.88 2.37 1.5684 -5 -1 3 1 58.89 2.01 1.5683 -5 1 3 1 59.88 1.91 1.5445 1 -3 1 1 60.12 2.64 1.5389 4 2 0 1 60.24 2.00 1.5364 -4 2 0 1 60.78 1.43 1.5238 2 3 0 1 60.87 1.70 1.5219 -2 3 0 1 61.43 1.65 1.5094 -2 2 4 1 61.55 1.42 1.5067 -2 -2 4 1 63.17 1.14 1.4718 -1 0 5 1 63.47 3.73 1.4657 4 0 2 1 64.54 1.03 1.4439 -3 1 5 1 64.61 1.62 1.4426 -3 -1 5 1 64.83 1.32 1.4382 2 -3 1 1 65.03 3.59 1.4342 -6 0 2 1 65.12 2.70 1.4325 -3 -3 1 1 65.17 3.60 1.4314 -3 3 1 1 66.19 2.11 1.4118 -1 1 5 1 66.28 1.88 1.4101 -1 -1 5 1 66.40 1.57 1.4079 -3 3 2 1 66.41 1.16 1.4077 -3 -3 2 1 66.49 1.30 1.4062 2 2 3 1 66.94 1.48 1.3979 3 3 0 1 67.05 1.03 1.3958 -3 3 0 1 67.66 1.23 1.3847 0 0 5 1 69.55 1.74 1.3517 -5 0 5 1 70.01 1.05 1.3439 -6 0 4 1 72.30 1.37 1.3069 6 0 0 1 75.24 1.45 1.2629 4 2 2 1 75.42 1.16 1.2604 4 -2 2 1 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.