Getchellite Kyono A, Kimata M American Mineralogist 89 (2004) 696-700 Structural reinvestigation of getchellite As0.98Sb1.02S3.00 _database_code_amcsd 0003539 CELL PARAMETERS: 11.9490 9.0280 10.1300 90.000 116.150 90.000 SPACE GROUP: P2_1/a X-RAY WAVELENGTH: 1.541838 Cell Volume: 980.926 Density (g/cm3): 3.982 MAX. ABS. INTENSITY / VOLUME**2: 17.26304356 RIR: 1.412 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.73 23.26 9.0931 0 0 1 2 13.72 22.96 6.4525 -1 1 1 4 13.82 13.41 6.4067 0 1 1 4 15.03 8.78 5.8938 -2 0 1 2 16.53 6.55 5.3630 2 0 0 2 17.97 40.43 4.9352 -2 1 1 4 18.20 2.84 4.8741 1 1 1 4 19.24 3.67 4.6129 -2 0 2 2 19.25 14.91 4.6108 2 1 0 4 19.52 17.41 4.5466 0 0 2 2 19.67 10.98 4.5140 0 2 0 2 20.10 100.00 4.4167 -1 1 2 4 21.36 18.41 4.1606 1 2 0 4 21.63 13.89 4.1077 -2 1 2 4 21.89 2.66 4.0607 0 1 2 4 21.92 4.92 4.0547 -1 2 1 4 21.98 43.19 4.0432 0 2 1 4 22.66 6.56 3.9242 2 0 1 2 24.46 67.18 3.6398 -3 1 1 4 24.74 18.39 3.5989 2 1 1 4 24.85 3.92 3.5837 -2 2 1 4 25.01 7.66 3.5601 1 2 1 4 25.80 3.42 3.4535 2 2 0 4 26.35 2.63 3.3823 1 1 2 4 26.45 12.32 3.3696 -1 2 2 4 26.65 3.04 3.3447 -2 0 3 2 26.82 40.58 3.3241 3 1 0 4 27.65 25.83 3.2263 -2 2 2 4 27.85 7.31 3.2033 0 2 2 4 28.61 41.76 3.1205 -1 1 3 4 29.47 24.66 3.0310 0 0 3 2 29.94 24.95 2.9842 -3 2 1 4 30.18 4.00 2.9616 2 2 1 4 30.86 22.95 2.8975 1 3 0 4 30.88 73.97 2.8953 2 0 2 2 31.13 7.71 2.8734 0 1 3 4 31.26 49.15 2.8610 -1 3 1 4 31.31 23.79 2.8569 0 3 1 4 31.53 16.36 2.8373 1 2 2 4 31.93 3.01 2.8029 -4 1 1 4 31.93 1.48 2.8027 3 2 0 4 31.95 59.05 2.8014 -4 1 2 4 32.24 9.30 2.7766 3 1 1 4 32.48 3.72 2.7570 2 1 2 4 33.34 2.13 2.6874 -2 2 3 4 33.47 37.31 2.6777 -4 0 3 2 33.47 1.04 2.6774 -1 2 3 4 33.56 1.11 2.6703 1 3 1 4 34.17 1.17 2.6244 2 3 0 4 34.67 16.14 2.5870 -1 3 2 4 35.32 4.30 2.5415 -3 2 3 4 35.56 26.59 2.5244 1 1 3 4 35.62 20.83 2.5204 -2 3 2 4 35.68 1.91 2.5164 0 2 3 4 36.87 3.80 2.4380 -2 1 4 4 36.88 2.71 2.4371 2 2 2 4 37.48 17.37 2.3998 -3 3 1 4 37.69 1.29 2.3867 -3 1 4 4 38.00 2.46 2.3681 -1 1 4 4 38.49 19.68 2.3389 -3 3 2 4 38.79 17.19 2.3214 1 3 2 4 39.05 7.38 2.3064 -4 0 4 2 39.11 36.81 2.3030 -4 2 3 4 39.60 1.18 2.2757 3 1 2 4 39.65 1.73 2.2733 0 0 4 2 39.67 1.81 2.2720 1 2 3 4 39.94 2.61 2.2570 0 4 0 2 40.11 24.65 2.2482 2 0 3 2 40.29 1.32 2.2384 4 1 1 4 40.32 2.89 2.2371 -2 3 3 4 40.36 15.84 2.2347 -4 1 4 4 40.63 1.36 2.2203 -5 1 3 4 40.86 2.26 2.2084 -2 2 4 4 41.18 6.31 2.1923 -1 4 1 4 41.21 3.09 2.1905 0 4 1 4 41.39 1.28 2.1816 2 1 3 4 41.90 2.90 2.1560 -1 2 4 4 42.91 7.90 2.1077 -2 4 1 4 42.94 1.30 2.1061 -4 3 1 4 43.01 13.69 2.1029 1 4 1 4 43.18 16.52 2.0949 3 3 1 4 43.35 3.57 2.0871 5 1 0 4 43.37 6.07 2.0864 2 3 2 4 43.39 1.97 2.0856 3 2 2 4 43.50 6.10 2.0803 2 4 0 4 43.72 1.62 2.0704 -5 2 1 4 44.03 3.56 2.0567 4 2 1 4 44.09 5.64 2.0539 -4 2 4 4 44.35 10.46 2.0427 -5 2 3 4 44.61 1.56 2.0314 -5 1 4 4 44.63 7.53 2.0303 0 2 4 4 44.83 3.34 2.0216 0 4 2 4 45.03 6.09 2.0131 -2 0 5 2 45.05 6.92 2.0124 2 2 3 4 45.30 5.39 2.0020 4 3 0 4 45.83 2.21 1.9800 1 3 3 4 46.20 3.93 1.9649 -2 1 5 4 46.21 2.33 1.9646 -6 0 3 2 46.41 1.39 1.9565 2 4 1 4 46.89 3.11 1.9375 5 2 0 4 46.89 2.49 1.9375 -2 3 4 4 47.30 13.15 1.9217 -6 0 1 2 47.36 1.98 1.9197 -6 1 3 4 47.36 1.62 1.9194 1 4 2 4 47.42 7.75 1.9173 4 1 2 4 47.50 3.17 1.9141 -4 1 5 4 47.83 16.01 1.9018 -1 3 4 4 48.43 3.10 1.8796 -6 1 1 4 48.76 1.91 1.8675 -1 4 3 4 48.77 3.82 1.8671 5 1 1 4 48.83 2.30 1.8653 1 2 4 4 49.02 4.31 1.8585 -6 0 4 2 49.43 6.14 1.8440 -3 2 5 4 49.58 1.06 1.8386 -2 2 5 4 49.75 2.10 1.8327 4 3 1 4 50.00 1.98 1.8240 2 0 4 2 50.04 9.85 1.8227 -5 3 3 4 50.11 1.54 1.8203 -6 1 4 4 50.48 2.15 1.8078 -5 1 5 4 50.68 3.00 1.8014 -6 2 3 4 50.68 3.25 1.8011 2 3 3 4 50.73 1.13 1.7995 4 2 2 4 50.95 2.02 1.7922 -4 4 1 4 50.97 3.14 1.7918 -4 4 2 4 51.17 3.94 1.7853 3 4 1 4 51.58 1.48 1.7720 -1 5 1 4 51.61 2.07 1.7710 0 5 1 4 51.70 4.77 1.7681 -6 2 1 4 52.03 6.31 1.7577 5 2 1 4 52.16 9.49 1.7536 6 1 0 4 52.38 2.26 1.7468 5 3 0 4 53.04 12.33 1.7264 -2 5 1 4 53.66 2.83 1.7080 -5 2 5 4 53.78 3.67 1.7046 -6 0 5 2 53.91 2.09 1.7007 -1 5 2 4 54.17 5.24 1.6933 1 3 4 4 54.24 4.43 1.6912 2 2 4 4 54.39 3.07 1.6869 0 2 5 4 54.46 3.45 1.6848 -2 4 4 4 54.58 3.51 1.6814 -2 5 2 4 54.70 2.83 1.6781 0 5 2 4 54.72 2.71 1.6773 -3 3 5 4 54.87 3.18 1.6731 -7 1 3 4 55.07 8.02 1.6676 -3 4 4 4 55.11 1.23 1.6666 -7 1 2 4 55.25 2.18 1.6627 -2 0 6 2 55.27 12.22 1.6621 6 2 0 4 55.37 6.36 1.6593 -3 1 6 4 55.37 2.27 1.6592 -6 3 2 4 55.79 7.04 1.6477 5 1 2 4 55.81 9.67 1.6473 1 1 5 4 56.02 1.18 1.6415 -4 3 5 4 56.06 10.53 1.6404 -5 4 2 4 56.26 3.49 1.6352 -2 1 6 4 56.64 4.95 1.6251 -7 1 4 4 56.68 6.02 1.6241 -3 5 2 4 56.79 1.29 1.6211 -5 4 1 4 57.04 4.15 1.6145 4 4 1 4 57.10 1.24 1.6131 -4 4 4 4 57.16 3.34 1.6116 5 3 1 4 57.87 4.04 1.5935 -5 1 6 4 57.89 6.11 1.5928 2 4 3 4 58.36 2.22 1.5812 -6 3 4 4 58.36 1.63 1.5811 -3 2 6 4 58.69 4.38 1.5730 -5 3 5 4 59.22 9.53 1.5602 -2 2 6 4 59.24 2.66 1.5598 2 3 4 4 59.35 1.09 1.5571 -3 5 3 4 59.38 4.59 1.5565 0 3 5 4 59.44 1.31 1.5549 5 4 0 4 59.59 3.74 1.5515 -7 2 4 4 59.60 2.67 1.5512 0 5 3 4 60.25 1.42 1.5361 -7 2 1 4 60.28 4.52 1.5354 3 5 1 4 60.54 1.32 1.5294 2 0 5 2 60.67 1.43 1.5263 3 2 4 4 60.78 2.21 1.5238 -5 2 6 4 61.15 1.44 1.5155 0 0 6 2 62.22 1.39 1.4921 -6 4 2 4 62.82 1.60 1.4793 -4 4 5 4 62.91 3.63 1.4773 -7 3 2 4 63.05 2.36 1.4743 -8 0 2 2 63.41 1.97 1.4669 3 4 3 4 63.85 2.48 1.4579 -2 6 1 4 63.93 4.53 1.4563 1 6 1 4 63.96 1.07 1.4555 -6 2 6 4 64.02 1.06 1.4544 -1 5 4 4 64.46 1.71 1.4454 -4 0 7 2 64.72 1.37 1.4404 6 1 2 4 64.96 1.63 1.4357 -7 3 1 4 65.36 1.25 1.4277 3 3 4 4 65.39 1.02 1.4273 -4 1 7 4 65.62 3.94 1.4227 4 5 1 4 65.97 1.29 1.4161 0 4 5 4 66.08 5.28 1.4139 0 5 4 4 66.41 1.12 1.4078 2 5 3 4 66.87 1.28 1.3992 5 2 3 4 67.31 1.33 1.3910 1 6 2 4 67.72 2.61 1.3836 -7 3 5 4 67.84 1.02 1.3814 5 5 0 4 67.99 1.17 1.3789 -6 0 7 2 68.17 1.63 1.3757 3 1 5 4 68.29 1.58 1.3734 -3 2 7 4 68.36 1.19 1.3722 -2 6 3 4 69.05 1.76 1.3603 -6 4 5 4 69.78 1.83 1.3477 0 6 3 4 69.94 2.20 1.3451 4 4 3 4 70.31 3.72 1.3388 -8 0 6 2 71.00 1.43 1.3276 -4 5 5 4 71.37 1.67 1.3215 -1 5 5 4 71.59 1.48 1.3181 6 4 1 4 71.96 1.61 1.3122 4 6 0 4 71.99 2.47 1.3117 -4 6 3 4 73.62 1.08 1.2867 -5 3 7 4 73.80 2.64 1.2840 -8 3 1 4 73.87 1.52 1.2829 -8 3 5 4 73.95 1.32 1.2817 1 3 6 4 74.03 1.01 1.2805 1 7 0 4 74.54 1.25 1.2731 -5 6 2 4 74.90 1.76 1.2678 4 0 5 2 75.89 1.02 1.2538 -4 1 8 4 76.08 1.33 1.2511 -9 2 2 4 76.65 1.94 1.2431 -9 1 1 4 76.69 1.41 1.2426 -3 1 8 4 76.92 2.43 1.2395 -6 5 5 4 78.46 1.41 1.2190 -4 2 8 4 78.60 1.01 1.2172 -4 4 7 4 79.54 1.07 1.2051 3 1 6 4 80.13 1.46 1.1977 -2 4 7 4 80.16 1.54 1.1973 7 4 1 4 80.39 1.01 1.1946 -6 6 3 4 80.81 1.10 1.1894 -3 7 3 4 83.99 1.05 1.1522 -8 3 7 4 84.58 1.49 1.1457 -9 3 6 4 85.96 1.48 1.1308 3 7 2 4 86.19 1.06 1.1284 -4 5 7 4 86.19 1.29 1.1284 -5 7 1 4 86.77 1.20 1.1223 1 8 0 4 87.07 1.88 1.1192 8 2 2 4 87.14 1.64 1.1186 -4 6 6 4 87.39 1.70 1.1160 2 2 7 4 87.70 1.03 1.1128 -2 5 7 4 88.68 1.90 1.1031 3 6 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.