Yuksporite Krivovichev S V, Yakovenchuk V N, Armbruster T, Dobelin N, Pattison P, Weber H-P, Depmeier W American Mineralogist 89 (2004) 1561-1565 Porous titanosilicate nanorods in the structure of yuksporite, (Sr,Ba)2K4(Ca,Na)14(_,Mn,Fe){(Ti,Nb)4(O,OH)4[Si6O17]2[Si2O7]3}(H2O,OH)n, resolved using synchrotron radiation Sample: Kola peninsula, Russia _database_code_amcsd 0003651 CELL PARAMETERS: 7.1260 24.9130 17.0750 90.000 101.890 90.000 SPACE GROUP: P2_1/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 2966.288 Density (g/cm3): 2.951 MAX. ABS. INTENSITY / VOLUME**2: 7.091686753 RIR: 0.782 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.10 100.00 12.4565 0 2 0 2 11.90 18.77 7.4365 0 3 1 4 12.69 2.24 6.9731 1 0 0 2 12.71 5.17 6.9655 -1 0 1 2 13.18 5.12 6.7150 1 1 0 4 14.22 48.30 6.2283 0 4 0 2 14.74 1.18 6.0101 1 0 1 2 17.76 10.60 4.9933 0 4 2 4 19.19 16.97 4.6256 0 3 3 4 19.58 2.97 4.5343 -1 2 3 4 21.11 2.33 4.2082 1 3 2 4 21.27 6.68 4.1772 0 0 4 2 21.92 2.43 4.0540 1 5 0 4 22.39 6.50 3.9711 1 0 3 2 22.73 3.63 3.9121 -1 1 4 4 23.93 5.78 3.7183 0 6 2 4 24.90 3.66 3.5753 -1 3 4 4 24.97 2.11 3.5666 -1 6 1 4 25.25 15.97 3.5271 -2 1 1 4 25.55 9.24 3.4869 1 5 2 4 25.55 1.56 3.4866 2 0 0 2 25.58 2.21 3.4827 -2 0 2 2 25.68 3.18 3.4692 0 4 4 4 26.55 1.47 3.3575 2 2 0 4 27.11 4.88 3.2892 -1 0 5 2 27.24 8.17 3.2743 -2 3 1 4 27.29 9.07 3.2680 1 1 4 4 27.42 1.16 3.2525 2 1 1 4 27.48 1.40 3.2463 -2 1 3 4 28.06 7.88 3.1802 -1 2 5 4 28.25 17.68 3.1592 -1 6 3 4 28.67 5.47 3.1141 0 8 0 2 28.80 32.33 3.1001 0 3 5 4 29.18 1.66 3.0604 -1 7 2 4 29.27 6.45 3.0511 2 3 1 4 29.32 5.83 3.0460 -2 3 3 4 29.36 44.16 3.0423 2 4 0 4 29.38 33.81 3.0398 -2 4 2 4 29.73 14.07 3.0050 2 0 2 2 29.79 45.47 2.9990 0 7 3 4 29.80 15.10 2.9977 -2 0 4 2 30.64 34.67 2.9180 0 8 2 4 30.74 1.80 2.9085 -1 4 5 4 30.85 1.03 2.8982 -2 5 1 4 31.10 11.43 2.8758 1 7 2 4 31.47 4.28 2.8429 -1 8 1 4 32.14 34.85 2.7848 0 0 6 2 32.25 19.25 2.7753 0 5 5 4 32.57 4.18 2.7493 1 5 4 4 32.68 23.62 2.7400 2 5 1 4 32.73 21.34 2.7363 -2 5 3 4 32.96 15.37 2.7177 0 2 6 4 33.10 17.63 2.7065 2 4 2 4 33.17 14.93 2.7011 -2 4 4 4 33.20 7.64 2.6984 2 1 3 4 33.29 8.58 2.6914 -2 1 5 4 33.56 10.83 2.6701 2 6 0 4 33.59 9.61 2.6684 -2 6 2 4 34.18 3.25 2.6233 -1 8 3 4 34.77 7.78 2.5801 2 3 3 4 34.86 8.17 2.5739 -2 3 5 4 34.87 7.81 2.5728 1 9 0 4 35.17 2.47 2.5517 1 4 5 4 35.97 1.55 2.4967 0 8 4 4 36.67 2.30 2.4505 1 8 3 4 36.90 3.61 2.4362 0 7 5 4 36.91 2.02 2.4356 -1 5 6 4 36.92 1.35 2.4344 2 6 2 4 36.99 1.21 2.4305 -2 6 4 4 37.18 1.20 2.4185 1 7 4 4 37.55 1.26 2.3952 2 2 4 4 37.65 1.04 2.3890 -2 2 6 4 38.37 3.93 2.3458 -1 10 1 4 39.72 3.41 2.2690 -1 9 4 4 39.86 4.41 2.2614 -1 8 5 4 40.29 1.22 2.2383 3 3 0 4 41.30 16.51 2.1859 -2 9 1 4 41.48 1.03 2.1769 1 5 6 4 41.85 4.56 2.1583 2 7 3 4 41.93 3.71 2.1547 -2 7 5 4 41.97 6.03 2.1527 0 5 7 4 42.24 3.76 2.1397 0 10 4 4 42.48 1.61 2.1280 1 0 7 2 42.65 4.05 2.1199 1 9 4 4 42.71 1.51 2.1170 -1 1 8 4 42.78 1.11 2.1139 -2 9 3 4 42.85 1.74 2.1104 1 10 3 4 42.99 7.87 2.1041 2 6 4 4 43.08 9.13 2.0999 -2 6 6 4 43.32 2.07 2.0886 0 0 8 2 43.33 2.87 2.0882 -1 6 7 4 43.60 1.88 2.0758 0 8 6 4 44.40 1.77 2.0402 -3 5 4 4 44.71 1.28 2.0270 2 10 0 4 44.73 1.11 2.0263 -2 10 2 4 44.99 2.20 2.0148 0 12 2 4 45.20 1.45 2.0059 -2 5 7 4 45.26 1.17 2.0034 3 0 3 2 45.31 2.63 2.0013 1 7 6 4 45.53 1.53 1.9921 -3 1 6 4 45.60 2.51 1.9896 -1 12 1 4 45.69 2.19 1.9855 2 0 6 2 45.77 2.33 1.9824 0 7 7 4 45.81 2.23 1.9806 -2 0 8 2 46.04 2.83 1.9715 3 6 1 4 46.30 1.26 1.9608 2 2 6 4 46.95 1.07 1.9355 -2 9 5 4 47.57 3.03 1.9114 -2 11 1 4 47.77 3.23 1.9039 0 13 1 4 48.10 12.51 1.8917 2 4 6 4 48.21 11.18 1.8875 -2 4 8 4 48.81 1.46 1.8658 0 6 8 4 49.06 2.00 1.8567 0 10 6 4 49.31 1.59 1.8481 -3 2 7 4 49.32 4.37 1.8479 1 13 0 4 49.90 1.66 1.8277 3 3 4 4 50.98 6.37 1.7913 2 6 6 4 51.09 6.06 1.7876 -2 6 8 4 51.28 29.55 1.7815 -4 0 2 2 51.84 2.60 1.7635 -4 2 2 4 51.99 1.09 1.7589 -1 11 6 4 52.05 1.90 1.7569 1 8 7 4 52.12 1.29 1.7549 -3 8 5 4 52.37 1.28 1.7469 3 0 5 2 52.63 2.17 1.7390 2 11 3 4 52.69 2.16 1.7371 -2 11 5 4 52.78 1.24 1.7344 -1 10 7 4 53.09 1.13 1.7251 -1 13 4 4 53.12 1.32 1.7241 -1 14 1 4 53.23 1.48 1.7209 2 9 5 4 53.32 2.00 1.7181 -2 9 7 4 53.36 1.08 1.7170 -3 10 1 4 53.50 1.37 1.7128 -4 4 2 4 53.66 2.98 1.7081 2 12 2 4 53.70 2.99 1.7067 -2 12 4 4 54.07 3.36 1.6962 2 5 7 4 54.19 3.65 1.6927 -2 5 9 4 54.36 7.47 1.6877 -2 13 1 4 54.37 2.91 1.6875 3 9 2 4 54.44 4.05 1.6854 -1 9 8 4 54.93 2.43 1.6716 -1 3 10 4 54.95 1.26 1.6709 0 0 10 2 55.54 1.97 1.6547 2 13 1 4 55.57 2.21 1.6539 -2 13 3 4 55.61 2.63 1.6527 0 15 1 4 55.79 1.44 1.6478 1 4 9 4 55.85 2.75 1.6460 0 7 9 4 56.91 3.02 1.6181 1 10 7 4 56.97 1.75 1.6165 -3 10 5 4 57.21 1.04 1.6102 3 6 5 4 57.25 1.63 1.6091 2 7 7 4 57.37 2.14 1.6061 -2 7 9 4 59.54 2.26 1.5527 2 10 6 4 59.64 2.21 1.5504 -2 10 8 4 59.81 2.57 1.5463 -4 8 2 4 59.81 1.58 1.5463 4 3 3 4 59.95 1.57 1.5430 -4 3 7 4 60.00 3.55 1.5419 0 9 9 4 60.40 1.69 1.5326 4 7 1 4 60.48 1.66 1.5307 -4 7 5 4 61.34 1.90 1.5113 2 9 7 4 61.42 1.06 1.5096 -3 1 10 4 61.45 1.68 1.5089 -2 9 9 4 61.74 2.00 1.5025 4 0 4 2 61.74 1.27 1.5024 1 13 6 4 61.82 2.61 1.5007 4 5 3 4 61.91 2.73 1.4989 -4 0 8 2 61.96 2.31 1.4977 -4 5 7 4 62.11 1.05 1.4944 0 13 7 4 62.12 1.18 1.4942 0 3 11 4 62.24 2.94 1.4917 4 2 4 4 62.32 1.76 1.4899 -3 13 2 4 62.33 2.91 1.4898 2 3 9 4 62.40 3.65 1.4881 -4 2 8 4 62.44 5.05 1.4873 0 15 5 4 62.46 2.84 1.4868 -2 3 11 4 62.56 1.14 1.4848 -3 12 5 4 63.10 1.49 1.4734 3 4 7 4 63.75 1.81 1.4599 0 17 1 4 64.09 1.83 1.4530 0 5 11 4 64.36 1.06 1.4475 4 9 1 4 64.38 1.31 1.4472 -3 5 10 4 64.78 1.49 1.4391 -3 8 9 4 65.54 1.55 1.4243 3 13 2 4 65.91 1.74 1.4172 0 17 3 4 66.43 1.00 1.4073 -1 16 5 4 66.68 1.81 1.4027 3 9 6 4 66.98 1.36 1.3970 0 7 11 4 67.31 1.16 1.3910 -2 7 11 4 67.50 2.68 1.3877 0 10 10 4 67.70 3.01 1.3841 0 18 0 2 68.25 1.01 1.3741 4 5 5 4 68.87 1.89 1.3633 0 15 7 4 70.30 1.14 1.3391 1 17 4 4 71.88 1.37 1.3135 2 13 7 4 71.98 1.61 1.3119 -2 13 9 4 73.74 1.17 1.2849 -1 4 13 4 74.67 1.50 1.2711 0 8 12 4 78.18 1.35 1.2226 -5 8 7 4 80.47 1.32 1.1935 0 0 14 2 82.68 1.41 1.1671 4 9 7 4 82.90 1.08 1.1646 -4 9 11 4 82.95 1.38 1.1640 -6 4 2 4 83.15 1.25 1.1617 2 6 12 4 83.31 1.27 1.1599 -2 6 14 4 85.01 1.02 1.1410 -4 15 7 4 86.46 1.69 1.1256 -2 21 1 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.