Makarochkinite Grew E S, Barbier J, Britten J, Yates M G, Polyakov V O, Shcherbakova E P, Halenius U, Shearer C K American Mineralogist 90 (2005) 1402-1412 Makarochkinite, Ca2Fe2+4Fe3+TiSi4BeAlO20, a new beryllosilicate member of the aenigmatite-sapphirine-surinamite group from the Il'men Mountains (southern Urals), Russia Sample: 400shch6 _database_code_amcsd 0003889 CELL PARAMETERS: 10.3550 10.7510 8.8730 105.757 96.227 124.861 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 735.302 Density (g/cm3): 3.958 MAX. ABS. INTENSITY / VOLUME**2: 5.115551608 RIR: 0.421 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.50 1.63 9.3117 -1 1 0 2 10.99 78.62 8.0504 0 1 0 2 10.99 82.81 8.0495 0 0 1 2 11.05 34.38 8.0090 1 0 0 2 11.95 21.43 7.4038 0 -1 1 2 12.73 2.94 6.9564 -1 0 1 2 13.92 21.72 6.3623 1 -1 1 2 18.39 13.12 4.8246 -1 -1 1 2 18.50 68.22 4.7955 0 1 1 2 19.06 1.57 4.6559 -2 2 0 2 19.07 1.24 4.6548 -2 1 1 2 20.23 3.00 4.3890 0 -2 1 2 20.23 3.57 4.3885 0 -1 2 2 21.22 5.99 4.1870 2 -2 1 2 21.23 5.32 4.1858 -2 0 1 2 23.59 13.69 3.7714 1 -2 2 2 24.04 17.81 3.7019 0 -2 2 2 25.87 15.39 3.4440 -2 3 0 2 25.88 16.11 3.4430 -2 1 2 2 27.38 3.09 3.2572 -3 1 1 2 27.66 2.80 3.2255 -1 -2 1 2 27.94 4.33 3.1937 1 0 2 2 28.05 3.86 3.1811 2 -2 2 2 28.06 3.85 3.1805 -2 -1 1 2 28.56 50.75 3.1251 0 2 1 2 28.56 46.93 3.1249 0 1 2 2 29.12 2.10 3.0661 3 -2 1 2 29.19 11.12 3.0597 -1 -2 2 2 29.87 6.93 2.9914 2 -3 2 2 29.88 5.79 2.9905 -2 -1 2 2 29.96 8.51 2.9822 3 -3 1 2 30.48 7.89 2.9325 1 2 0 2 30.50 48.19 2.9305 0 -3 1 2 30.51 51.81 2.9302 0 -1 3 2 30.54 13.50 2.9267 2 -1 2 2 30.55 13.24 2.9265 2 1 0 2 30.56 9.26 2.9249 -2 3 1 2 30.57 7.88 2.9246 -2 2 2 2 31.77 18.93 2.8170 -3 3 1 2 32.26 25.79 2.7752 -1 2 2 2 32.43 47.68 2.7612 3 -1 1 2 32.93 23.34 2.7199 -3 2 2 2 33.39 1.16 2.6835 0 3 0 2 33.40 22.60 2.6828 -1 3 1 2 33.41 76.56 2.6821 2 -4 1 2 33.42 77.96 2.6812 -2 0 3 2 33.52 7.54 2.6737 -3 0 2 2 33.57 34.41 2.6697 3 0 0 2 33.98 4.64 2.6385 1 -1 3 2 34.55 1.35 2.5960 -1 -2 3 2 34.98 1.20 2.5653 3 -3 2 2 35.03 8.11 2.5617 1 -3 3 2 35.14 8.12 2.5537 -2 4 0 2 35.14 14.61 2.5537 -3 4 0 2 35.15 7.63 2.5530 -2 1 3 2 35.27 4.00 2.5444 -4 3 0 2 35.28 4.56 2.5441 -4 2 1 2 35.37 83.03 2.5379 -4 2 0 2 35.40 70.46 2.5355 2 -4 2 2 35.41 69.91 2.5347 -2 -1 3 2 35.60 15.64 2.5220 -1 1 3 2 35.75 14.41 2.5117 3 -2 2 2 36.40 7.75 2.4679 0 -3 3 2 36.56 10.47 2.4579 2 0 2 2 36.56 11.01 2.4579 2 1 1 2 36.65 5.75 2.4520 -4 3 1 2 37.23 34.01 2.4150 2 -2 3 2 37.24 32.32 2.4147 -2 -2 1 2 37.27 2.62 2.4128 2 -3 3 2 37.27 2.70 2.4123 -2 -2 2 2 37.46 1.59 2.4010 4 -3 1 2 37.46 1.11 2.4005 -4 1 1 2 37.51 16.50 2.3977 0 2 2 2 37.77 1.00 2.3819 3 -4 2 2 38.20 2.99 2.3561 -1 -3 1 2 38.27 7.42 2.3517 -3 1 3 2 38.68 7.40 2.3279 -1 4 0 2 38.68 3.52 2.3279 -4 4 0 2 38.69 3.49 2.3274 -4 2 2 2 38.83 3.74 2.3191 -3 -1 1 2 38.93 10.82 2.3132 4 -2 1 2 38.94 12.43 2.3130 -4 1 0 2 39.11 1.11 2.3030 -3 -1 2 2 40.19 1.07 2.2439 -2 2 3 2 40.64 1.16 2.2198 2 -4 3 2 40.66 1.26 2.2192 1 -4 3 2 41.08 3.12 2.1971 -1 -3 3 2 41.13 2.49 2.1945 0 -4 2 2 41.14 1.83 2.1943 0 -2 4 2 41.27 3.41 2.1873 -4 4 1 2 41.28 3.51 2.1871 -4 3 2 2 41.56 2.61 2.1727 0 -4 1 2 41.57 2.32 2.1725 0 -1 4 2 42.11 5.92 2.1459 3 -5 1 2 42.51 6.30 2.1267 -1 0 4 2 42.60 1.37 2.1223 -3 -1 3 2 42.73 1.01 2.1160 4 -3 2 2 43.03 76.45 2.1022 2 -5 1 2 43.04 76.59 2.1015 -2 0 4 2 43.21 8.85 2.0935 4 -4 2 2 43.23 7.32 2.0929 -4 0 2 2 43.51 77.00 2.0799 4 -1 1 2 44.17 1.27 2.0506 -5 3 1 2 45.29 2.16 2.0025 4 -2 2 2 45.29 2.14 2.0023 4 0 0 2 45.65 23.32 1.9872 -2 5 0 2 45.67 22.97 1.9867 -2 1 4 2 45.97 4.18 1.9741 -5 2 0 2 46.54 3.86 1.9512 2 -3 4 2 46.55 4.24 1.9510 -2 -3 2 2 46.57 2.81 1.9502 -3 0 4 2 46.66 1.73 1.9468 4 -5 2 2 46.67 1.22 1.9461 -4 0 3 2 46.69 3.67 1.9455 3 0 2 2 46.70 24.29 1.9449 -4 4 2 2 46.76 1.23 1.9426 2 -5 3 2 46.78 2.28 1.9417 -5 2 2 2 46.83 1.03 1.9401 5 -3 1 2 46.91 2.14 1.9367 1 -5 1 2 47.05 1.19 1.9315 -3 -2 2 2 47.54 1.81 1.9127 3 1 1 2 47.66 1.01 1.9083 -2 4 2 2 47.69 8.50 1.9070 2 -2 4 2 47.69 6.56 1.9069 -2 -3 1 2 48.38 4.74 1.8813 -4 5 1 2 48.39 4.39 1.8809 -4 3 3 2 49.28 3.59 1.8492 5 -5 1 2 50.30 2.73 1.8138 1 0 4 2 50.51 3.62 1.8069 4 -1 2 2 50.51 4.07 1.8069 4 0 1 2 50.93 1.47 1.7930 -2 5 1 2 50.94 1.29 1.7927 -2 2 4 2 50.95 2.38 1.7925 5 -4 2 2 51.49 3.66 1.7748 3 -6 2 2 51.55 5.22 1.7729 2 -1 4 2 51.55 4.10 1.7729 2 3 0 2 51.62 3.22 1.7707 3 2 0 2 51.84 1.89 1.7638 -1 -1 5 2 51.94 4.26 1.7605 3 -4 4 2 52.50 3.34 1.7431 -5 1 3 2 52.61 2.61 1.7398 4 -6 2 2 52.63 5.99 1.7391 2 -5 4 2 52.63 2.54 1.7391 -4 0 4 2 52.64 6.18 1.7388 -2 -3 4 2 52.87 1.32 1.7318 -5 3 3 2 53.06 1.62 1.7259 2 -6 2 2 53.08 1.91 1.7254 -2 -1 5 2 53.19 2.05 1.7220 -4 6 0 2 53.21 2.16 1.7215 -4 2 4 2 53.26 5.41 1.7198 0 -5 1 2 53.27 5.79 1.7196 0 -1 5 2 53.46 4.96 1.7139 1 4 0 2 53.46 1.58 1.7139 -6 4 0 2 53.47 2.06 1.7138 -6 3 1 2 53.83 1.13 1.7030 -1 2 4 2 54.09 5.60 1.6954 -5 0 2 2 54.55 1.29 1.6822 -5 0 1 2 54.72 5.05 1.6775 3 -2 4 2 54.74 2.67 1.6768 2 2 2 2 54.74 3.10 1.6768 2 1 3 2 55.30 1.49 1.6612 -6 5 0 2 55.31 1.90 1.6609 -6 3 2 2 56.10 1.29 1.6394 -1 5 1 2 56.20 1.83 1.6368 -5 0 3 2 56.65 4.69 1.6249 -6 5 1 2 56.65 4.30 1.6247 -6 4 2 2 56.77 18.98 1.6216 0 -5 4 2 56.77 19.25 1.6216 0 -4 5 2 56.87 3.87 1.6189 -3 -1 5 2 57.07 15.50 1.6137 -2 6 0 2 57.09 15.24 1.6134 -2 1 5 2 57.17 2.53 1.6113 1 -6 2 2 57.24 1.70 1.6094 1 -1 5 2 57.29 5.73 1.6082 -3 -3 3 2 57.48 1.04 1.6032 6 -3 1 2 57.54 1.53 1.6019 5 -4 3 2 57.54 3.29 1.6018 5 0 0 2 57.67 14.77 1.5985 0 3 3 2 57.82 3.06 1.5946 5 -5 3 2 57.88 16.01 1.5931 4 0 2 2 58.12 1.05 1.5872 1 -6 3 2 58.45 3.03 1.5791 -3 -3 1 2 59.34 1.01 1.5574 4 -1 3 2 59.34 1.05 1.5574 4 1 1 2 59.71 4.77 1.5486 5 -3 3 2 59.72 14.29 1.5485 6 -6 1 2 59.73 12.63 1.5481 -6 2 3 2 59.79 1.08 1.5467 3 -1 4 2 60.12 3.45 1.5390 6 -5 2 2 60.14 2.90 1.5386 -6 1 2 2 60.38 1.17 1.5330 6 -4 2 2 60.39 1.21 1.5328 -6 1 1 2 60.40 1.07 1.5326 -3 -3 4 2 60.42 1.44 1.5321 1 -5 5 2 62.05 2.86 1.4957 4 -6 4 2 62.07 2.86 1.4952 -4 -2 4 2 62.23 40.79 1.4918 -4 5 3 2 62.26 35.61 1.4911 6 -6 2 2 62.29 35.87 1.4906 -6 1 3 2 62.56 3.91 1.4847 -5 -1 1 2 62.61 2.09 1.4837 3 -7 3 2 62.62 4.52 1.4834 -2 6 1 2 62.64 4.59 1.4832 -2 2 5 2 62.72 1.01 1.4814 3 -3 5 2 62.75 28.43 1.4808 0 -5 5 2 62.90 1.09 1.4776 4 -7 3 2 62.92 2.09 1.4772 -1 -2 6 2 63.01 2.76 1.4753 3 -5 5 2 63.44 37.52 1.4663 2 4 0 2 63.44 36.76 1.4663 2 -1 5 2 63.44 4.74 1.4662 -7 4 0 2 63.60 8.00 1.4630 0 -6 3 2 63.61 8.23 1.4628 0 -3 6 2 63.62 2.52 1.4625 -4 6 2 2 63.63 2.91 1.4623 -4 4 4 2 64.14 2.13 1.4520 -7 3 1 2 64.88 5.19 1.4371 3 1 3 2 65.18 1.54 1.4314 6 -7 1 2 65.20 1.03 1.4309 -6 2 4 2 65.57 1.95 1.4238 3 2 2 2 65.80 1.69 1.4192 1 3 3 2 65.98 3.03 1.4158 -6 7 0 2 66.00 1.53 1.4155 5 -4 4 2 66.00 2.70 1.4155 -6 3 4 2 66.68 1.13 1.4028 6 -7 2 2 66.70 1.58 1.4023 -6 1 4 2 67.13 3.76 1.3944 6 -4 3 2 67.14 3.43 1.3941 -6 0 1 2 67.20 1.64 1.3931 -3 -4 3 2 67.49 1.93 1.3879 4 -7 4 2 67.51 1.34 1.3874 -4 -2 5 2 68.17 1.10 1.3756 -7 3 3 2 68.31 1.42 1.3731 2 -4 6 2 68.31 1.60 1.3731 -2 -5 3 2 68.81 1.33 1.3643 0 4 3 2 68.81 1.13 1.3643 0 3 4 2 69.03 1.51 1.3606 1 -7 3 2 69.14 2.41 1.3587 -3 -4 4 2 69.28 1.13 1.3563 7 -3 1 2 69.86 9.01 1.3464 4 -6 5 2 69.87 5.39 1.3462 2 4 1 2 69.87 6.05 1.3462 2 0 5 2 69.88 6.67 1.3461 -4 -3 4 2 70.03 1.51 1.3435 -5 -2 2 2 70.11 1.14 1.3422 5 0 2 2 70.16 1.07 1.3414 -2 6 2 2 70.43 1.27 1.3368 -6 0 4 2 70.81 2.35 1.3307 7 -7 1 2 71.12 4.18 1.3256 -7 6 2 2 71.48 6.01 1.3198 -4 -1 6 2 71.78 2.16 1.3150 -7 5 3 2 71.83 4.76 1.3142 -4 6 3 2 71.84 4.91 1.3141 -4 5 4 2 72.45 1.20 1.3045 1 5 1 2 72.76 2.71 1.2997 -1 4 4 2 73.41 2.81 1.2899 -1 5 3 2 74.01 1.62 1.2808 2 -6 6 2 74.02 2.11 1.2807 -2 -5 5 2 74.09 1.41 1.2797 -7 2 4 2 74.12 3.56 1.2792 4 -7 5 2 74.15 4.19 1.2788 -4 -3 5 2 74.30 1.38 1.2765 -4 2 6 2 74.31 3.79 1.2765 -6 3 5 2 74.70 1.69 1.2707 -1 3 5 2 75.45 1.04 1.2599 0 -7 3 2 75.46 1.38 1.2598 0 -3 7 2 75.65 1.62 1.2571 3 -6 6 2 75.65 1.08 1.2571 2 3 3 2 75.74 1.48 1.2559 6 -4 4 2 75.75 1.01 1.2557 -6 -1 1 2 77.33 1.21 1.2340 0 -6 6 2 78.32 6.97 1.2207 4 -5 6 2 78.34 6.12 1.2206 -4 -4 3 2 79.44 1.62 1.2064 4 -6 6 2 79.46 1.70 1.2062 -4 -4 4 2 79.76 1.09 1.2023 -3 -5 2 2 80.02 1.04 1.1991 2 -7 6 2 80.04 6.75 1.1989 0 4 4 2 80.96 1.57 1.1876 7 -2 2 2 81.41 2.08 1.1821 -4 0 7 2 81.75 1.09 1.1781 -2 -6 2 2 83.35 1.41 1.1594 -6 0 6 2 86.81 1.94 1.1219 -4 4 6 2 88.88 1.25 1.1011 -7 2 6 2 88.96 1.09 1.1003 -6 4 6 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.