Makarochkinite Grew E S, Barbier J, Britten J, Yates M G, Polyakov V O, Shcherbakova E P, Halenius U, Shearer C K American Mineralogist 90 (2005) 1402-1412 Makarochkinite, Ca2Fe2+4Fe3+TiSi4BeAlO20, a new beryllosilicate member of the aenigmatite-sapphirine-surinamite group from the Il'men Mountains (southern Urals), Russia Sample: 3319 _database_code_amcsd 0003890 CELL PARAMETERS: 10.3730 10.7680 8.8780 105.794 96.183 124.934 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 737.315 Density (g/cm3): 3.926 MAX. ABS. INTENSITY / VOLUME**2: 5.005624827 RIR: 0.415 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.48 1.63 9.3296 -1 1 0 2 10.99 81.10 8.0532 0 1 0 2 10.99 84.65 8.0519 0 0 1 2 11.04 37.22 8.0152 1 0 0 2 11.94 21.25 7.4106 0 -1 1 2 12.72 2.91 6.9612 -1 0 1 2 13.90 20.54 6.3715 1 -1 1 2 18.38 12.39 4.8271 -1 -1 1 2 18.50 69.59 4.7959 0 1 1 2 19.02 1.27 4.6648 -2 2 0 2 19.04 1.25 4.6605 -2 1 1 2 20.22 2.58 4.3923 0 -2 1 2 20.22 3.31 4.3917 0 -1 2 2 21.18 5.24 4.1952 2 -2 1 2 21.21 4.67 4.1893 -2 0 1 2 23.56 12.76 3.7764 1 -2 2 2 24.02 17.96 3.7053 0 -2 2 2 24.83 1.19 3.5864 -1 1 2 2 25.83 15.52 3.4491 -2 3 0 2 25.86 16.98 3.4454 -2 1 2 2 27.35 3.56 3.2613 -3 1 1 2 27.64 3.15 3.2268 -1 -2 1 2 27.93 4.19 3.1949 1 0 2 2 28.01 3.78 3.1858 2 -2 2 2 28.04 3.57 3.1821 -2 -1 1 2 28.56 50.69 3.1255 0 2 1 2 28.56 46.95 3.1252 0 1 2 2 29.07 2.18 3.0714 3 -2 1 2 29.17 11.20 3.0615 -1 -2 2 2 29.82 7.65 2.9966 2 -3 2 2 29.86 6.32 2.9922 -2 -1 2 2 29.90 9.04 2.9883 3 -3 1 2 30.48 8.32 2.9331 1 2 0 2 30.48 48.60 2.9324 0 -3 1 2 30.49 51.40 2.9319 0 -1 3 2 30.52 13.89 2.9294 2 -1 2 2 30.54 13.72 2.9276 2 1 0 2 30.54 8.87 2.9276 -2 3 1 2 30.55 7.56 2.9264 -2 2 2 2 31.72 18.73 2.8210 -3 3 1 2 32.25 26.47 2.7759 -1 2 2 2 32.39 48.49 2.7642 3 -1 1 2 32.90 23.10 2.7227 -3 2 2 2 33.36 77.57 2.6861 2 -4 1 2 33.38 1.14 2.6844 0 3 0 2 33.38 1.02 2.6840 0 0 3 2 33.39 22.21 2.6839 -1 3 1 2 33.40 77.94 2.6826 -2 0 3 2 33.49 8.05 2.6758 -3 0 2 2 33.54 34.22 2.6717 3 0 0 2 33.96 4.55 2.6401 1 -1 3 2 34.53 1.45 2.5977 -1 -2 3 2 34.91 1.05 2.5699 3 -3 2 2 34.99 8.51 2.5647 1 -3 3 2 35.08 14.64 2.5578 -3 4 0 2 35.10 7.66 2.5565 -2 4 0 2 35.13 6.98 2.5542 -2 1 3 2 35.20 4.28 2.5493 -4 3 0 2 35.22 4.87 2.5480 -4 2 1 2 35.31 83.28 2.5420 -4 2 0 2 35.34 70.80 2.5397 2 -4 2 2 35.39 69.64 2.5362 -2 -1 3 2 35.59 15.66 2.5226 -1 1 3 2 35.70 14.73 2.5152 3 -2 2 2 36.37 8.12 2.4702 0 -3 3 2 36.54 10.01 2.4590 2 0 2 2 36.55 10.80 2.4586 2 1 1 2 36.59 5.63 2.4560 -4 3 1 2 37.19 34.13 2.4176 2 -2 3 2 37.21 2.38 2.4162 2 -3 3 2 37.22 32.18 2.4156 -2 -2 1 2 37.26 2.52 2.4135 -2 -2 2 2 37.38 1.70 2.4056 4 -3 1 2 37.42 1.01 2.4034 -4 1 1 2 37.51 16.06 2.3979 0 2 2 2 38.18 2.95 2.3570 -1 -3 1 2 38.24 7.12 2.3534 -3 1 3 2 38.60 3.28 2.3324 -4 4 0 2 38.64 3.24 2.3303 -4 2 2 2 38.65 7.22 2.3294 -1 4 0 2 38.81 3.61 2.3204 -3 -1 1 2 38.87 10.97 2.3167 4 -2 1 2 38.89 12.70 2.3157 -4 1 0 2 40.17 1.10 2.2448 -2 2 3 2 40.58 1.03 2.2231 2 -4 3 2 40.60 1.36 2.2219 1 -4 3 2 41.05 2.94 2.1986 -1 -3 3 2 41.10 2.29 2.1962 0 -4 2 2 41.11 1.59 2.1959 0 -2 4 2 41.21 3.36 2.1907 -4 4 1 2 41.23 3.43 2.1898 -4 3 2 2 41.54 2.39 2.1739 0 -4 1 2 41.55 2.24 2.1736 0 -1 4 2 42.04 5.97 2.1494 3 -5 1 2 42.49 6.32 2.1275 -1 0 4 2 42.57 1.17 2.1237 -3 -1 3 2 42.66 1.03 2.1196 4 -3 2 2 42.97 77.78 2.1047 2 -5 1 2 43.02 77.84 2.1025 -2 0 4 2 43.13 8.90 2.0976 4 -4 2 2 43.19 7.18 2.0947 -4 0 2 2 43.46 78.83 2.0820 4 -1 1 2 43.78 1.05 2.0676 0 -4 3 2 44.09 1.13 2.0540 -5 3 1 2 45.22 1.91 2.0050 4 -2 2 2 45.25 2.05 2.0038 4 0 0 2 45.61 24.16 1.9890 -2 5 0 2 45.65 23.53 1.9874 -2 1 4 2 45.90 4.04 1.9770 -5 2 0 2 46.49 3.83 1.9534 2 -3 4 2 46.53 4.26 1.9518 -2 -3 2 2 46.54 2.96 1.9513 -3 0 4 2 46.56 1.64 1.9507 4 -5 2 2 46.63 1.06 1.9476 -4 0 3 2 46.65 24.62 1.9471 -4 4 2 2 46.66 3.77 1.9466 3 0 2 2 46.69 1.27 1.9455 2 -5 3 2 46.72 2.36 1.9442 -5 2 2 2 46.74 1.02 1.9434 5 -3 1 2 46.87 2.23 1.9383 1 -5 1 2 47.02 1.31 1.9324 -3 -2 2 2 47.52 1.68 1.9135 3 1 1 2 47.65 8.58 1.9087 2 -2 4 2 47.68 6.76 1.9075 -2 -3 1 2 48.31 5.02 1.8838 -4 5 1 2 48.35 4.51 1.8826 -4 3 3 2 49.17 3.50 1.8530 5 -5 1 2 50.29 2.49 1.8144 1 0 4 2 50.46 3.74 1.8085 4 -1 2 2 50.48 4.16 1.8081 4 0 1 2 50.84 2.33 1.7958 5 -4 2 2 50.90 1.44 1.7941 -2 5 1 2 50.92 1.25 1.7932 -2 2 4 2 51.40 3.69 1.7776 3 -6 2 2 51.52 5.45 1.7740 2 -1 4 2 51.54 4.34 1.7733 2 3 0 2 51.60 3.32 1.7712 3 2 0 2 51.81 1.92 1.7646 -1 -1 5 2 51.86 4.29 1.7630 3 -4 4 2 52.44 3.40 1.7448 -5 1 3 2 52.50 2.84 1.7430 4 -6 2 2 52.55 5.99 1.7415 2 -5 4 2 52.59 2.64 1.7403 -4 0 4 2 52.60 6.09 1.7398 -2 -3 4 2 52.80 1.37 1.7337 -5 3 3 2 52.99 1.49 1.7280 2 -6 2 2 53.05 1.85 1.7263 -2 -1 5 2 53.11 2.03 1.7246 -4 6 0 2 53.17 2.25 1.7227 -4 2 4 2 53.23 5.57 1.7207 0 -5 1 2 53.24 6.06 1.7204 0 -1 5 2 53.35 1.69 1.7171 -6 4 0 2 53.38 2.12 1.7165 -6 3 1 2 53.45 5.13 1.7143 1 4 0 2 53.82 1.14 1.7033 -1 2 4 2 54.04 5.69 1.6969 -5 0 2 2 54.50 1.37 1.6836 -5 0 1 2 54.67 4.96 1.6790 3 -2 4 2 54.73 3.17 1.6771 2 1 3 2 54.74 2.76 1.6770 2 2 2 2 55.18 1.51 1.6645 -6 5 0 2 55.22 1.93 1.6633 -6 3 2 2 56.08 1.36 1.6400 -1 5 1 2 56.15 1.89 1.6381 -5 0 3 2 56.54 4.54 1.6277 -6 5 1 2 56.56 4.18 1.6272 -6 4 2 2 56.71 19.22 1.6231 0 -5 4 2 56.72 19.66 1.6230 0 -4 5 2 56.84 3.98 1.6198 -3 -1 5 2 57.02 15.16 1.6150 -2 6 0 2 57.07 15.11 1.6139 -2 1 5 2 57.11 2.61 1.6127 1 -6 2 2 57.21 1.82 1.6102 1 -1 5 2 57.26 5.79 1.6090 -3 -3 3 2 57.39 1.02 1.6057 6 -3 1 2 57.43 1.66 1.6045 5 -4 3 2 57.49 3.31 1.6030 5 0 0 2 57.66 14.83 1.5986 0 3 3 2 57.71 3.08 1.5975 5 -5 3 2 57.85 15.95 1.5940 4 0 2 2 58.05 1.16 1.5888 1 -6 3 2 58.43 2.88 1.5796 -3 -3 1 2 59.29 1.04 1.5586 4 -1 3 2 59.31 1.01 1.5581 4 1 1 2 59.58 14.75 1.5517 6 -6 1 2 59.62 4.73 1.5506 5 -3 3 2 59.66 12.88 1.5498 -6 2 3 2 59.75 1.07 1.5476 3 -1 4 2 59.99 3.68 1.5420 6 -5 2 2 60.07 3.01 1.5402 -6 1 2 2 60.27 1.26 1.5357 6 -4 2 2 60.32 1.35 1.5344 -6 1 1 2 60.35 1.42 1.5338 1 -5 5 2 60.36 1.09 1.5335 -3 -3 4 2 61.93 2.86 1.4983 4 -6 4 2 62.03 2.86 1.4961 -4 -2 4 2 62.12 35.94 1.4942 6 -6 2 2 62.18 41.19 1.4929 -4 5 3 2 62.22 36.20 1.4921 -6 1 3 2 62.51 2.06 1.4859 3 -7 3 2 62.52 3.80 1.4857 -5 -1 1 2 62.58 4.61 1.4843 -2 6 1 2 62.62 4.71 1.4835 -2 2 5 2 62.68 28.39 1.4821 0 -5 5 2 62.78 1.01 1.4801 4 -7 3 2 62.88 2.02 1.4780 -1 -2 6 2 62.91 2.72 1.4773 3 -5 5 2 63.32 4.77 1.4688 -7 4 0 2 63.40 36.86 1.4670 2 -1 5 2 63.43 37.60 1.4666 2 4 0 2 63.54 7.96 1.4641 0 -6 3 2 63.55 8.25 1.4639 0 -3 6 2 63.56 2.46 1.4638 -4 6 2 2 63.59 2.93 1.4632 -4 4 4 2 64.03 2.02 1.4541 -7 3 1 2 64.86 5.20 1.4375 3 1 3 2 65.03 1.53 1.4342 6 -7 1 2 65.13 1.07 1.4323 -6 2 4 2 65.55 1.92 1.4241 3 2 2 2 65.80 1.61 1.4193 1 3 3 2 65.85 3.10 1.4184 -6 7 0 2 65.89 1.50 1.4176 5 -4 4 2 65.92 2.74 1.4169 -6 3 4 2 66.52 1.17 1.4056 6 -7 2 2 66.63 1.56 1.4035 -6 1 4 2 67.01 3.78 1.3965 6 -4 3 2 67.08 3.40 1.3953 -6 0 1 2 67.16 1.73 1.3938 -3 -4 3 2 67.36 2.02 1.3902 4 -7 4 2 67.47 1.44 1.3882 -4 -2 5 2 68.07 1.11 1.3773 -7 3 3 2 68.23 1.50 1.3745 2 -4 6 2 68.28 1.61 1.3737 -2 -5 3 2 68.80 1.31 1.3645 0 4 3 2 68.81 1.14 1.3644 0 3 4 2 68.96 1.47 1.3618 1 -7 3 2 69.10 2.37 1.3594 -3 -4 4 2 69.16 1.10 1.3582 7 -3 1 2 69.73 9.17 1.3485 4 -6 5 2 69.84 6.75 1.3468 -4 -3 4 2 69.84 6.19 1.3467 2 0 5 2 69.86 5.48 1.3464 2 4 1 2 69.99 1.50 1.3442 -5 -2 2 2 70.06 1.10 1.3431 5 0 2 2 70.37 1.33 1.3379 -6 0 4 2 70.64 2.31 1.3334 7 -7 1 2 70.99 4.29 1.3277 -7 6 2 2 71.43 5.90 1.3206 -4 -1 6 2 71.67 2.15 1.3168 -7 5 3 2 71.78 4.77 1.3151 -4 6 3 2 71.79 4.98 1.3149 -4 5 4 2 72.44 1.19 1.3047 1 5 1 2 72.75 2.78 1.2999 -1 4 4 2 73.39 2.78 1.2901 -1 5 3 2 73.91 1.67 1.2824 2 -6 6 2 73.97 2.18 1.2815 -2 -5 5 2 73.98 3.45 1.2812 4 -7 5 2 74.00 1.37 1.2810 -7 2 4 2 74.10 4.16 1.2795 -4 -3 5 2 74.23 3.74 1.2775 -6 3 5 2 74.26 1.43 1.2771 -4 2 6 2 74.69 1.70 1.2708 -1 3 5 2 75.40 1.32 1.2606 0 -3 7 2 75.53 1.61 1.2588 3 -6 6 2 75.62 1.46 1.2576 6 -4 4 2 75.64 1.05 1.2572 2 3 3 2 75.69 1.01 1.2565 -6 -1 1 2 77.24 1.22 1.2351 0 -6 6 2 78.21 7.08 1.2223 4 -5 6 2 78.30 6.10 1.2211 -4 -4 3 2 79.30 1.66 1.2081 4 -6 6 2 79.41 1.76 1.2068 -4 -4 4 2 79.73 1.08 1.2028 -3 -5 2 2 79.90 1.04 1.2006 2 -7 6 2 80.03 6.86 1.1990 0 4 4 2 80.85 1.63 1.1888 7 -2 2 2 81.36 2.13 1.1827 -4 0 7 2 81.71 1.08 1.1785 -2 -6 2 2 83.28 1.43 1.1602 -6 0 6 2 86.76 1.92 1.1224 -4 4 6 2 88.79 1.25 1.1020 -7 2 6 2 88.88 1.11 1.1010 -6 4 6 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.