Realgar Kyono A, Kimata M, Hatta T American Mineralogist 90 (2005) 1563-1570 Light-induced degradation dynamics in realgar: in situ structural investigation using single crystal X-ray diffraction and X-ray photoelectron spectroscopy Sample: Getchell mine, Nevada; t = 0 hours Note: space group corrected _database_code_amcsd 0003933 CELL PARAMETERS: 9.3270 13.5630 6.5900 90.000 106.460 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 799.484 Density (g/cm3): 3.555 MAX. ABS. INTENSITY / VOLUME**2: 19.63074995 RIR: 1.798 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.85 8.20 7.4671 1 1 0 4 13.05 5.89 6.7815 0 2 0 2 14.69 41.80 6.0291 -1 0 1 2 15.47 44.55 5.7285 0 1 1 4 16.09 26.02 5.5093 -1 1 1 4 16.40 100.00 5.4040 1 2 0 4 19.20 10.06 4.6234 0 2 1 4 19.36 2.19 4.5854 1 0 1 2 19.70 1.23 4.5058 -1 2 1 4 20.91 4.19 4.2474 2 1 0 4 21.85 21.11 4.0683 -2 1 1 4 22.03 2.91 4.0349 1 3 0 4 23.42 3.85 3.7986 1 2 1 4 23.83 7.00 3.7336 2 2 0 4 24.20 4.90 3.6770 0 3 1 4 24.66 9.07 3.6102 -2 2 1 4 27.71 2.38 3.2194 1 3 1 4 27.94 1.09 3.1939 -1 1 2 4 28.06 29.85 3.1795 2 3 0 4 28.14 23.49 3.1706 1 4 0 4 28.24 39.95 3.1600 0 0 2 2 28.29 2.91 3.1541 2 1 1 4 28.78 1.54 3.1023 -2 3 1 4 29.01 6.30 3.0775 0 1 2 4 29.28 31.32 3.0507 -3 0 1 2 29.90 18.96 2.9879 0 4 1 4 30.02 6.29 2.9763 -3 1 1 4 30.22 22.10 2.9573 -1 2 2 4 30.37 14.45 2.9427 -2 1 2 4 30.56 48.38 2.9257 2 2 1 4 30.70 1.50 2.9121 3 1 0 4 31.23 8.20 2.8643 0 2 2 4 32.17 10.38 2.7821 -3 2 1 4 32.50 1.39 2.7546 -2 2 2 4 32.81 11.29 2.7294 3 2 0 4 32.85 38.81 2.7263 1 4 1 4 33.16 9.07 2.7020 2 4 0 4 33.30 13.21 2.6906 1 1 2 4 33.77 5.51 2.6541 -2 4 1 4 34.55 15.70 2.5959 1 5 0 4 34.63 2.06 2.5900 0 3 2 4 35.50 2.03 2.5288 -3 3 1 4 35.68 11.64 2.5164 -3 1 2 4 35.80 1.56 2.5081 -2 3 2 4 36.09 12.23 2.4890 3 3 0 4 36.32 14.21 2.4738 -1 5 1 4 36.79 8.70 2.4427 3 0 1 2 37.41 4.13 2.4040 3 1 1 4 37.54 8.25 2.3957 -3 2 2 4 38.14 5.95 2.3598 -1 4 2 4 38.41 1.47 2.3437 2 4 1 4 39.20 2.30 2.2981 3 2 1 4 39.30 1.29 2.2927 2 0 2 2 39.88 11.87 2.2605 0 6 0 2 40.28 4.46 2.2391 3 4 0 4 40.33 1.70 2.2362 4 0 0 2 40.48 9.93 2.2282 -3 3 2 4 40.90 1.82 2.2064 4 1 0 4 41.03 1.73 2.1997 -4 2 1 4 41.14 10.82 2.1939 -1 0 3 2 41.19 8.54 2.1916 1 6 0 4 41.58 2.77 2.1719 2 2 2 4 41.70 6.10 2.1658 -1 1 3 4 42.39 8.59 2.1324 -4 0 2 2 42.46 10.02 2.1290 -2 1 3 4 42.57 4.22 2.1237 4 2 0 4 42.72 3.70 2.1166 -1 6 1 4 42.94 3.58 2.1065 -4 1 2 4 43.47 2.50 2.0817 0 1 3 4 44.08 4.15 2.0545 -2 2 3 4 44.33 1.53 2.0435 -3 4 2 4 44.54 3.74 2.0342 -4 2 2 4 44.93 2.28 2.0174 2 6 0 4 45.11 1.75 2.0097 -3 0 3 2 45.19 1.86 2.0065 3 5 0 4 45.63 1.09 1.9880 -3 1 3 4 45.78 4.01 1.9819 3 4 1 4 45.98 1.94 1.9738 -1 3 3 4 47.10 2.74 1.9295 1 5 2 4 47.54 1.25 1.9127 1 1 3 4 48.77 1.69 1.8671 4 2 1 4 48.82 1.67 1.8654 -5 0 1 2 48.90 4.15 1.8624 -1 6 2 4 49.03 7.16 1.8581 1 2 3 4 49.13 10.49 1.8545 2 6 1 4 49.31 2.37 1.8480 -5 1 1 4 49.46 1.18 1.8426 3 2 2 4 49.58 6.18 1.8385 0 6 2 4 50.23 8.90 1.8162 -3 6 1 4 50.57 1.49 1.8051 -4 4 2 4 50.68 1.53 1.8013 3 6 0 4 50.76 8.55 1.7986 -5 2 1 4 50.88 1.16 1.7948 -4 1 3 4 51.04 2.45 1.7894 0 4 3 4 51.19 5.35 1.7845 4 3 1 4 51.43 1.98 1.7766 1 3 3 4 51.78 3.99 1.7655 -4 5 1 4 51.83 1.04 1.7640 -2 7 1 4 51.86 1.43 1.7631 3 3 2 4 52.24 1.31 1.7510 2 5 2 4 52.44 1.50 1.7450 1 6 2 4 52.93 1.50 1.7298 5 2 0 4 52.96 3.94 1.7288 -3 4 3 4 53.11 1.90 1.7244 -5 3 1 4 53.50 1.36 1.7127 2 1 3 4 53.74 9.54 1.7058 -1 5 3 4 54.09 3.63 1.6954 0 8 0 2 54.12 5.10 1.6947 -3 6 2 4 54.60 3.48 1.6809 -4 3 3 4 54.68 9.89 1.6786 1 4 3 4 54.76 2.58 1.6764 -4 5 2 4 54.87 7.46 1.6731 2 2 3 4 55.14 1.10 1.6657 1 8 0 4 55.21 2.49 1.6638 0 5 3 4 55.21 2.42 1.6637 -5 3 2 4 55.38 2.24 1.6591 3 6 1 4 55.96 1.90 1.6431 -2 0 4 2 56.24 1.75 1.6356 -3 7 1 4 56.29 4.75 1.6344 -5 4 1 4 56.46 1.23 1.6299 -2 7 2 4 56.66 1.29 1.6247 3 7 0 4 56.80 2.53 1.6209 -4 6 1 4 57.23 1.06 1.6097 2 6 2 4 57.72 1.13 1.5972 -4 4 3 4 57.81 3.17 1.5950 5 1 1 4 58.44 1.29 1.5791 4 5 1 4 58.53 3.72 1.5771 4 2 2 4 58.64 2.26 1.5744 -1 6 3 4 59.11 1.24 1.5629 5 2 1 4 59.23 1.22 1.5601 -2 6 3 4 59.60 1.50 1.5511 -4 6 2 4 59.86 1.98 1.5451 -3 7 2 4 61.04 1.45 1.5180 3 7 1 4 61.14 1.82 1.5158 -6 1 2 4 61.25 3.53 1.5134 -6 2 1 4 61.52 3.16 1.5073 -4 0 4 2 61.74 3.08 1.5025 2 8 1 4 61.77 1.58 1.5019 -3 6 3 4 61.94 1.95 1.4980 -4 1 4 4 62.13 1.44 1.4939 0 8 2 4 62.94 2.25 1.4766 1 1 4 4 63.34 3.03 1.4684 -6 3 1 4 63.61 5.01 1.4629 4 4 2 4 64.14 1.15 1.4519 -5 4 3 4 64.16 3.28 1.4516 5 4 1 4 64.47 1.05 1.4453 -6 3 2 4 64.55 1.39 1.4437 -3 4 4 4 64.68 1.07 1.4411 -2 7 3 4 65.34 2.93 1.4281 2 9 0 4 65.45 1.38 1.4261 0 7 3 4 66.53 1.19 1.4054 -2 5 4 4 68.50 1.80 1.3698 -1 9 2 4 68.62 1.89 1.3677 5 2 2 4 71.03 2.05 1.3270 -4 8 2 4 72.20 1.31 1.3085 6 3 1 4 78.60 1.14 1.2171 -3 4 5 4 85.91 1.15 1.1314 -7 3 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.