Realgar Kyono A, Kimata M, Hatta T American Mineralogist 90 (2005) 1563-1570 Light-induced degradation dynamics in realgar: in situ structural investigation using single crystal X-ray diffraction and X-ray photoelectron spectroscopy Sample: Getchell mine, Nevada; t = 12 hours Note: space group corrected _database_code_amcsd 0003935 CELL PARAMETERS: 9.3600 13.5730 6.5900 90.000 105.710 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 805.941 Density (g/cm3): 3.526 MAX. ABS. INTENSITY / VOLUME**2: 19.70397491 RIR: 1.819 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.79 7.34 7.5068 1 1 0 4 13.05 6.17 6.7865 0 2 0 2 14.74 42.06 6.0093 -1 0 1 2 15.42 45.35 5.7471 0 1 1 4 16.13 25.86 5.4949 -1 1 1 4 16.35 100.00 5.4209 1 2 0 4 19.15 10.62 4.6344 0 2 1 4 19.17 2.98 4.6304 1 0 1 2 19.73 1.20 4.4990 -1 2 1 4 20.77 3.98 4.2758 2 1 0 4 21.88 20.40 4.0623 -2 1 1 4 21.98 2.63 4.0432 1 3 0 4 23.26 3.46 3.8249 1 2 1 4 23.70 6.87 3.7534 2 2 0 4 24.16 4.33 3.6835 0 3 1 4 24.69 8.44 3.6065 -2 2 1 4 27.56 2.13 3.2360 1 3 1 4 27.95 27.24 3.1924 2 3 0 4 27.96 1.11 3.1913 -1 1 2 4 28.00 2.47 3.1864 2 1 1 4 28.10 21.51 3.1755 1 4 0 4 28.13 37.68 3.1719 0 0 2 2 28.79 1.19 3.1005 -2 3 1 4 28.91 5.61 3.0887 0 1 2 4 29.25 28.86 3.0531 -3 0 1 2 29.86 17.35 2.9921 0 4 1 4 30.00 5.30 2.9786 -3 1 1 4 30.24 19.73 2.9556 -1 2 2 4 30.28 45.68 2.9517 2 2 1 4 30.47 13.32 2.9336 -2 1 2 4 30.48 1.08 2.9325 3 1 0 4 31.12 7.45 2.8735 0 2 2 4 32.15 9.00 2.7843 -3 2 1 4 32.59 1.11 2.7474 -2 2 2 4 32.60 10.77 2.7465 3 2 0 4 32.72 35.24 2.7370 1 4 1 4 33.04 11.27 2.7108 1 1 2 4 33.05 8.54 2.7104 2 4 0 4 33.78 4.46 2.6535 -2 4 1 4 34.51 13.27 2.5992 1 5 0 4 34.53 1.46 2.5972 0 3 2 4 35.47 1.63 2.5308 -3 3 1 4 35.79 9.56 2.5092 -3 1 2 4 35.88 1.39 2.5030 -2 3 2 4 35.89 11.63 2.5023 3 3 0 4 36.31 12.34 2.4739 -1 5 1 4 36.40 8.27 2.4684 3 0 1 2 37.02 3.65 2.4285 3 1 1 4 37.64 7.75 2.3897 -3 2 2 4 38.14 4.98 2.3596 -1 4 2 4 38.17 1.11 2.3576 2 4 1 4 38.82 1.84 2.3197 3 2 1 4 39.85 10.44 2.2622 0 6 0 2 40.03 1.72 2.2526 4 0 0 2 40.09 3.84 2.2490 3 4 0 4 40.57 8.46 2.2236 -3 3 2 4 40.60 1.85 2.2222 4 1 0 4 40.94 1.32 2.2046 -4 2 1 4 41.12 10.14 2.1951 -1 0 3 2 41.14 7.47 2.1941 1 6 0 4 41.20 2.23 2.1912 2 2 2 4 41.68 4.75 2.1670 -1 1 3 4 42.27 3.67 2.1379 4 2 0 4 42.46 7.51 2.1287 -4 0 2 2 42.55 8.09 2.1248 -2 1 3 4 42.71 3.09 2.1171 -1 6 1 4 43.01 2.99 2.1030 -4 1 2 4 43.30 2.37 2.0894 0 1 3 4 44.16 3.78 2.0508 -2 2 3 4 44.40 1.23 2.0402 -3 4 2 4 44.61 3.09 2.0312 -4 2 2 4 44.83 1.64 2.0216 2 6 0 4 45.01 1.80 2.0139 3 5 0 4 45.27 1.27 2.0031 -3 0 3 2 45.44 3.91 1.9961 3 4 1 4 45.95 1.73 1.9749 -1 3 3 4 46.89 1.94 1.9376 1 5 2 4 48.29 1.21 1.8847 4 2 1 4 48.64 1.24 1.8718 -5 0 1 2 48.70 6.11 1.8696 1 2 3 4 48.89 3.46 1.8628 -1 6 2 4 48.92 8.79 1.8618 2 6 1 4 49.13 1.75 1.8543 -5 1 1 4 49.49 5.04 1.8418 0 6 2 4 50.19 7.18 1.8176 -3 6 1 4 50.51 1.30 1.8070 3 6 0 4 50.58 7.16 1.8044 -5 2 1 4 50.62 1.35 1.8033 -4 4 2 4 50.72 3.92 1.7999 4 3 1 4 50.88 1.93 1.7947 0 4 3 4 51.12 1.64 1.7868 1 3 3 4 51.36 1.13 1.7791 3 3 2 4 51.69 2.90 1.7685 -4 5 1 4 51.91 1.10 1.7616 2 5 2 4 52.24 1.14 1.7512 1 6 2 4 52.54 1.30 1.7417 5 2 0 4 52.94 1.48 1.7296 -5 3 1 4 53.09 2.78 1.7250 -3 4 3 4 53.70 7.47 1.7069 -1 5 3 4 54.05 3.06 1.6966 0 8 0 2 54.17 4.15 1.6932 -3 6 2 4 54.37 7.99 1.6874 1 4 3 4 54.39 6.24 1.6868 2 2 3 4 54.76 2.78 1.6763 -4 3 3 4 54.80 1.88 1.6751 -4 5 2 4 55.05 1.94 1.6682 0 5 3 4 55.07 1.84 1.6677 3 6 1 4 55.22 1.65 1.6633 -5 3 2 4 56.02 1.36 1.6417 -2 0 4 2 56.12 4.09 1.6390 -5 4 1 4 56.20 1.33 1.6368 -3 7 1 4 56.70 1.84 1.6234 -4 6 1 4 57.20 2.33 1.6104 5 1 1 4 57.88 3.06 1.5932 4 2 2 4 58.51 1.11 1.5775 5 2 1 4 58.60 1.74 1.5754 -1 6 3 4 59.64 1.17 1.5503 -4 6 2 4 59.90 1.44 1.5442 -3 7 2 4 60.74 1.08 1.5248 3 7 1 4 60.98 2.88 1.5194 -6 2 1 4 61.09 1.38 1.5170 -6 1 2 4 61.55 2.36 1.5068 2 8 1 4 61.75 2.43 1.5023 -4 0 4 2 61.87 1.15 1.4997 -3 6 3 4 62.04 1.14 1.4961 0 8 2 4 62.17 1.34 1.4932 -4 1 4 4 62.53 1.56 1.4854 1 1 4 4 62.98 3.87 1.4758 4 4 2 4 63.07 2.19 1.4740 -6 3 1 4 63.58 2.61 1.4633 5 4 1 4 65.24 2.07 1.4301 2 9 0 4 65.29 1.10 1.4291 0 7 3 4 67.83 1.53 1.3817 5 2 2 4 68.46 1.25 1.3705 -1 9 2 4 71.05 1.40 1.3268 -4 8 2 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.