Pb3MoO5Cl2 Charkin D O, Lightfoot P American Mineralogist 91 (2006) 1918-1921 Synthesis of novel lead - molybdenum and tungsten oxyhalides with the pinalite structure, Pb3MoO5Cl2 and Pb3WO5Br2 _database_code_amcsd 0004256 CELL PARAMETERS: 11.0116 13.1149 5.5949 90.000 90.000 90.000 SPACE GROUP: Amam X-RAY WAVELENGTH: 1.541838 Cell Volume: 807.986 Density (g/cm3): 7.138 MAX. ABS. INTENSITY / VOLUME**2: 172.5788354 RIR: 7.872 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 13.50 16.27 6.5574 0 2 0 2 15.73 9.77 5.6341 1 2 0 4 17.23 1.87 5.1461 0 1 1 4 19.04 4.59 4.6621 1 1 1 8 21.07 2.48 4.2166 2 2 0 4 23.67 73.33 3.7596 2 1 1 8 25.86 22.25 3.4448 0 3 1 4 27.12 38.25 3.2876 1 3 1 8 27.20 10.07 3.2787 0 4 0 2 27.85 31.86 3.2029 3 2 0 4 28.40 7.03 3.1424 1 4 0 4 29.90 11.43 2.9883 3 1 1 8 30.61 100.00 2.9203 2 3 1 8 31.76 6.59 2.8171 2 4 0 4 31.99 41.62 2.7974 0 0 2 2 32.53 27.31 2.7529 4 0 0 2 35.75 7.58 2.5118 3 3 1 8 35.84 1.52 2.5056 1 2 2 8 37.88 3.05 2.3749 0 5 1 4 38.62 1.39 2.3311 2 2 2 8 38.79 8.09 2.3216 1 5 1 8 41.41 7.42 2.1807 2 5 1 8 42.01 3.96 2.1505 4 3 1 8 42.48 12.20 2.1281 0 4 2 4 42.90 6.89 2.1083 4 4 0 4 42.93 21.98 2.1069 3 2 2 8 43.30 6.85 2.0894 1 4 2 8 43.34 1.88 2.0877 5 2 0 4 44.60 19.62 2.0316 2 6 0 4 44.76 10.63 2.0247 5 1 1 8 45.49 1.45 1.9940 3 5 1 8 45.71 4.52 1.9850 2 4 2 8 46.27 28.40 1.9621 4 0 2 4 48.42 1.38 1.8798 4 2 2 8 48.47 4.61 1.8780 3 6 0 4 49.10 11.44 1.8555 5 3 1 8 49.88 6.48 1.8282 5 4 0 4 50.77 2.25 1.7982 4 5 1 8 51.43 8.71 1.7766 0 7 1 4 52.26 8.82 1.7506 2 1 3 8 52.97 3.13 1.7286 6 1 1 8 53.18 1.21 1.7224 0 6 2 4 53.41 2.77 1.7154 0 3 3 4 53.88 1.26 1.7017 1 6 2 8 54.11 4.87 1.6949 1 3 3 8 54.25 2.93 1.6907 2 7 1 8 54.50 3.19 1.6837 4 4 2 8 54.87 1.34 1.6731 5 2 2 8 55.73 2.12 1.6494 3 1 3 8 55.94 18.92 1.6438 2 6 2 8 56.10 1.80 1.6394 0 8 0 2 56.16 16.31 1.6377 2 3 3 8 56.78 1.02 1.6215 1 8 0 4 56.84 5.25 1.6197 6 3 1 8 57.03 12.20 1.6149 5 5 1 8 57.64 2.61 1.5991 3 7 1 8 59.26 3.53 1.5592 3 6 2 8 59.48 1.95 1.5540 3 3 3 8 60.50 5.54 1.5304 5 4 2 8 60.53 7.48 1.5297 7 2 0 4 61.60 1.65 1.5057 1 5 3 8 61.65 4.47 1.5044 7 1 1 8 62.19 5.66 1.4927 4 7 1 8 63.50 1.76 1.4651 2 5 3 8 63.95 1.21 1.4559 4 3 3 8 64.13 1.78 1.4522 6 5 1 8 66.03 2.84 1.4149 5 1 3 8 66.06 1.48 1.4144 0 8 2 4 66.28 4.98 1.4102 0 9 1 4 66.37 1.12 1.4085 4 8 0 4 66.53 2.28 1.4055 6 6 0 4 66.89 5.76 1.3987 0 0 4 2 68.12 1.28 1.3764 8 0 0 2 69.45 4.20 1.3533 5 3 3 8 70.11 8.93 1.3421 7 2 2 8 71.36 3.32 1.3218 0 7 3 4 71.70 3.56 1.3164 3 9 1 8 71.78 1.95 1.3150 5 8 0 4 72.01 2.17 1.3115 7 5 1 8 72.64 1.16 1.3016 6 1 3 8 73.63 1.39 1.2865 0 4 4 4 73.72 1.15 1.2852 2 7 3 8 73.94 3.74 1.2818 3 2 4 8 74.28 1.69 1.2768 7 6 0 4 74.35 3.17 1.2758 2 10 0 4 75.58 2.11 1.2581 4 8 2 8 75.73 3.24 1.2559 6 6 2 8 75.79 4.95 1.2551 4 9 1 8 75.93 2.01 1.2532 6 3 3 8 75.96 1.04 1.2528 2 4 4 8 76.09 5.19 1.2509 5 5 3 8 76.37 4.16 1.2470 4 0 4 4 77.25 1.02 1.2350 8 0 2 4 80.15 1.86 1.1974 7 1 3 8 80.63 2.36 1.1915 4 7 3 8 80.73 2.17 1.1903 9 1 1 8 80.75 3.78 1.1901 5 8 2 8 81.77 1.38 1.1777 7 7 1 8 82.82 1.67 1.1655 4 4 4 8 83.17 2.92 1.1615 7 6 2 8 83.23 4.63 1.1608 2 10 2 8 83.93 2.55 1.1529 9 3 1 8 84.00 5.42 1.1521 2 6 4 8 84.35 2.58 1.1483 0 9 3 4 84.53 1.21 1.1463 9 4 0 4 86.82 1.52 1.1218 3 6 4 8 87.84 1.92 1.1113 3 11 1 8 87.89 2.24 1.1109 5 4 4 8 89.41 2.01 1.0959 3 9 3 8 89.71 1.28 1.0931 7 5 3 8 89.74 1.79 1.0927 2 1 5 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.