K2Fe(SO4)2(H2O)6 Bosi F, Belardi G, Ballirano P American Mineralogist 94 (2009) 74-82 Structural features in Tutton's salts K2[M2+(H2O)6](SO4)2, with M2+= Mg, Fe, Co, Ni, Cu, and Zn Locality: synthetic _database_code_amcsd 0004777 CELL PARAMETERS: 9.0822 12.2786 6.1765 90.000 104.568 90.000 SPACE GROUP: P2_1/a X-RAY WAVELENGTH: 1.541838 Cell Volume: 666.638 Density (g/cm3): 2.163 MAX. ABS. INTENSITY / VOLUME**2: 6.625883261 RIR: 0.997 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 14.43 11.89 6.1393 0 2 0 2 14.82 3.45 5.9779 0 0 1 2 16.49 11.47 5.3748 0 1 1 4 17.28 8.54 5.1309 -1 1 1 4 17.62 2.79 5.0332 1 2 0 4 20.20 19.73 4.3951 2 0 0 2 20.74 20.08 4.2829 0 2 1 4 21.24 77.05 4.1837 1 1 1 4 21.38 8.19 4.1565 -1 2 1 4 21.47 6.49 4.1380 2 1 0 4 21.88 74.98 4.0621 -2 0 1 2 23.06 4.46 3.8565 -2 1 1 4 23.98 100.00 3.7104 1 3 0 4 24.71 6.03 3.6030 1 2 1 4 24.92 6.58 3.5737 2 2 0 4 26.39 9.81 3.3772 0 3 1 4 26.90 19.70 3.3141 -1 3 1 4 28.06 16.37 3.1798 2 0 1 2 29.01 22.66 3.0783 2 1 1 4 29.09 19.46 3.0696 0 4 0 2 29.66 2.76 3.0124 1 3 1 4 29.83 1.79 2.9952 2 3 0 4 29.89 1.14 2.9890 0 0 2 2 29.95 56.09 2.9833 -1 1 2 4 30.85 1.76 2.8980 1 4 0 4 31.02 2.64 2.8831 -2 3 1 4 31.29 4.95 2.8586 -3 1 1 4 31.39 12.45 2.8500 3 1 0 4 31.69 8.62 2.8238 -2 0 2 2 31.69 22.52 2.8236 2 2 1 4 32.54 5.92 2.7520 -2 1 2 4 32.56 14.97 2.7497 -1 2 2 4 33.22 5.17 2.6970 -1 4 1 4 33.81 5.05 2.6512 -3 2 1 4 34.98 3.34 2.5655 -2 2 2 4 35.53 2.36 2.5268 1 4 1 4 35.68 4.77 2.5166 2 4 0 4 35.76 9.36 2.5111 2 3 1 4 36.55 1.02 2.4587 -1 3 2 4 37.13 1.14 2.4214 1 2 2 4 37.25 2.61 2.4138 0 3 2 4 37.68 42.34 2.3875 -3 3 1 4 37.92 1.14 2.3729 -3 1 2 4 39.68 5.75 2.2715 0 5 1 4 40.07 3.25 2.2502 -3 2 2 4 40.54 2.45 2.2250 2 0 2 2 40.69 2.03 2.2173 -4 1 1 4 40.72 2.44 2.2156 1 3 2 4 40.86 23.26 2.2085 2 4 1 4 41.07 1.35 2.1976 4 0 0 2 41.23 1.91 2.1893 2 1 2 4 41.76 2.46 2.1632 4 1 0 4 42.02 2.66 2.1501 1 5 1 4 42.20 13.73 2.1415 0 4 2 4 42.58 1.84 2.1230 -3 4 1 4 42.66 2.63 2.1195 3 4 0 4 43.04 2.77 2.1015 -2 5 1 4 43.55 10.30 2.0782 -2 4 2 4 43.75 13.44 2.0690 4 2 0 4 44.61 1.11 2.0310 -4 0 2 2 44.98 2.33 2.0155 -2 0 3 2 45.52 11.08 1.9926 0 0 3 2 46.74 4.63 1.9436 2 5 1 4 46.93 2.33 1.9361 0 6 1 4 47.13 2.39 1.9283 -4 2 2 4 47.54 1.12 1.9127 4 0 1 2 47.88 1.78 1.8997 -3 4 2 4 47.94 4.26 1.8974 0 5 2 4 48.00 1.14 1.8953 0 2 3 4 48.09 1.86 1.8922 3 4 1 4 48.29 3.88 1.8846 -3 5 1 4 48.36 4.63 1.8821 3 5 0 4 48.95 8.03 1.8608 -3 1 3 4 48.99 1.11 1.8593 1 6 1 4 49.58 6.85 1.8388 -1 3 3 4 49.90 8.52 1.8276 -2 6 1 4 49.94 1.74 1.8261 4 2 1 4 49.97 1.28 1.8253 1 1 3 4 50.21 1.03 1.8170 -4 4 1 4 50.47 3.86 1.8081 -2 3 3 4 50.67 1.76 1.8015 2 4 2 4 50.86 2.99 1.7952 -5 1 1 4 50.97 2.57 1.7916 0 3 3 4 51.05 1.13 1.7892 3 2 2 4 51.12 7.06 1.7869 4 4 0 4 51.71 2.52 1.7676 1 2 3 4 52.59 7.79 1.7403 5 1 0 4 52.83 1.07 1.7328 4 3 1 4 53.15 1.91 1.7231 -3 5 2 4 53.34 2.98 1.7175 3 5 1 4 53.81 2.11 1.7037 -1 6 2 4 53.89 4.46 1.7012 3 3 2 4 54.28 1.20 1.6901 5 2 0 4 54.33 1.05 1.6886 0 6 2 4 54.46 2.72 1.6848 -2 4 3 4 54.54 4.51 1.6826 1 3 3 4 55.98 2.29 1.6427 -4 2 3 4 56.17 1.81 1.6376 4 5 0 4 56.38 3.84 1.6319 1 7 1 4 56.71 1.10 1.6233 4 4 1 4 57.01 1.34 1.6153 5 3 0 4 57.20 1.23 1.6104 -2 7 1 4 57.36 1.28 1.6063 2 2 3 4 58.32 3.64 1.5822 -5 3 2 4 58.54 1.20 1.5768 4 1 2 4 60.18 2.57 1.5377 -2 0 4 2 60.79 3.61 1.5237 -1 7 2 4 61.16 2.64 1.5152 -4 6 1 4 61.39 1.86 1.5103 -5 1 3 4 61.57 2.27 1.5062 2 6 2 4 62.30 3.61 1.4904 -4 4 3 4 62.98 1.04 1.4759 5 3 1 4 63.13 1.53 1.4726 3 1 3 4 63.28 1.03 1.4697 -6 0 2 2 63.74 1.74 1.4602 1 7 2 4 64.66 1.80 1.4416 -4 6 2 4 64.72 2.84 1.4403 -1 3 4 4 64.95 1.05 1.4358 -2 8 1 4 65.37 1.66 1.4276 0 6 3 4 65.50 1.22 1.4250 6 2 0 4 65.93 2.68 1.4168 3 7 1 4 66.48 1.36 1.4064 -5 5 2 4 66.48 1.20 1.4064 1 1 4 4 66.74 2.74 1.4016 -3 3 4 4 67.89 1.66 1.3806 3 6 2 4 68.45 1.50 1.3706 1 6 3 4 69.20 1.02 1.3576 -6 4 1 4 69.84 1.24 1.3468 6 0 1 2 70.32 1.40 1.3387 6 1 1 4 70.57 1.23 1.3346 4 5 2 4 71.00 1.07 1.3275 -4 7 2 4 71.09 1.77 1.3261 -1 9 1 4 72.37 1.87 1.3058 -5 1 4 4 72.49 1.16 1.3039 -1 5 4 4 72.53 1.02 1.3033 -2 5 4 4 73.36 1.06 1.2906 4 2 3 4 73.46 1.18 1.2891 -7 1 1 4 73.84 1.57 1.2833 -3 7 3 4 74.84 1.78 1.2687 -4 8 1 4 76.21 1.02 1.2492 7 1 0 4 76.76 1.28 1.2417 5 7 0 4 77.67 1.27 1.2293 -2 6 4 4 83.46 1.27 1.1582 5 2 3 4 84.16 1.13 1.1503 7 2 1 4 84.24 1.34 1.1495 -5 7 3 4 86.41 1.01 1.1260 -2 10 2 4 86.50 1.38 1.1251 -6 4 4 4 88.56 1.06 1.1042 4 8 2 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.