K2Ni(SO4)2(H2O)6 Bosi F, Belardi G, Ballirano P American Mineralogist 94 (2009) 74-82 Structural features in Tutton's salts K2[M2+(H2O)6](SO4)2, with M2+= Mg, Fe, Co, Ni, Cu, and Zn Locality: synthetic _database_code_amcsd 0004779 CELL PARAMETERS: 9.0049 12.1904 6.1368 90.000 105.047 90.000 SPACE GROUP: P2_1/a X-RAY WAVELENGTH: 1.541838 Cell Volume: 650.559 Density (g/cm3): 2.231 MAX. ABS. INTENSITY / VOLUME**2: 7.551380628 RIR: 1.102 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 14.53 15.98 6.0952 0 2 0 2 14.95 5.46 5.9264 0 0 1 2 16.63 10.54 5.3299 0 1 1 4 17.37 12.06 5.1064 -1 1 1 4 17.77 2.06 4.9913 1 2 0 4 20.43 21.61 4.3481 2 0 0 2 20.91 23.38 4.2490 0 2 1 4 21.49 77.34 4.1345 1 1 1 4 21.50 7.48 4.1332 -1 2 1 4 21.70 5.72 4.0954 2 1 0 4 21.99 75.36 4.0417 -2 0 1 2 23.19 3.99 3.8364 -2 1 1 4 24.18 100.00 3.6814 1 3 0 4 24.98 6.29 3.5649 1 2 1 4 25.16 7.96 3.5397 2 2 0 4 26.46 1.08 3.3684 -2 2 1 4 26.60 8.37 3.3513 0 3 1 4 27.07 20.54 3.2936 -1 3 1 4 28.44 13.29 3.1386 2 0 1 2 29.31 14.62 3.0476 0 4 0 2 29.39 19.69 3.0395 2 1 1 4 29.95 2.45 2.9836 1 3 1 4 30.10 1.44 2.9688 2 3 0 4 30.13 54.96 2.9658 -1 1 2 4 31.10 1.37 2.8761 1 4 0 4 31.21 2.58 2.8656 -2 3 1 4 31.50 3.32 2.8399 -3 1 1 4 31.73 12.47 2.8201 3 1 0 4 31.83 7.64 2.8118 -2 0 2 2 32.08 22.50 2.7904 2 2 1 4 32.68 5.31 2.7399 -2 1 2 4 32.77 13.18 2.7330 -1 2 2 4 33.44 5.37 2.6794 -1 4 1 4 34.04 4.37 2.6336 -3 2 1 4 35.15 3.08 2.5532 -2 2 2 4 35.86 2.37 2.5044 1 4 1 4 35.99 5.53 2.4956 2 4 0 4 36.16 7.89 2.4839 2 3 1 4 37.54 1.52 2.3961 1 2 2 4 37.57 2.77 2.3942 0 3 2 4 37.94 40.12 2.3714 -3 3 1 4 38.09 1.26 2.3624 -3 1 2 4 39.99 5.30 2.2547 0 5 1 4 40.27 3.02 2.2396 -3 2 2 4 41.01 2.31 2.2007 -4 1 1 4 41.07 2.35 2.1975 2 0 2 2 41.15 2.76 2.1936 1 3 2 4 41.29 21.66 2.1864 2 4 1 4 41.54 1.22 2.1740 4 0 0 2 41.77 1.55 2.1626 2 1 2 4 42.22 2.55 2.1403 4 1 0 4 42.40 2.56 2.1320 1 5 1 4 42.55 12.89 2.1245 0 4 2 4 42.89 2.11 2.1085 -3 4 1 4 43.07 2.88 2.1004 3 4 0 4 43.34 2.88 2.0877 -2 5 1 4 43.81 10.44 2.0666 -2 4 2 4 44.23 13.30 2.0477 4 2 0 4 45.22 2.57 2.0052 -2 0 3 2 45.94 10.33 1.9755 0 0 3 2 47.21 3.73 1.9254 2 5 1 4 47.30 2.06 1.9219 0 6 1 4 47.39 2.41 1.9182 -4 2 2 4 48.16 1.64 1.8894 -3 4 2 4 48.34 4.14 1.8827 0 5 2 4 48.44 1.25 1.8792 0 2 3 4 48.64 1.94 1.8719 3 4 1 4 48.65 4.15 1.8716 -3 5 1 4 48.81 5.50 1.8658 3 5 0 4 49.18 8.38 1.8528 -3 1 3 4 49.42 1.22 1.8442 1 6 1 4 49.52 1.17 1.8407 2 6 0 4 49.94 7.08 1.8263 -1 3 3 4 50.26 8.51 1.8153 -2 6 1 4 50.52 1.64 1.8065 1 1 3 4 50.60 1.72 1.8040 4 2 1 4 50.61 1.31 1.8036 -4 4 1 4 50.77 4.10 1.7982 -2 3 3 4 51.25 1.83 1.7825 2 4 2 4 51.31 3.06 1.7806 -5 1 1 4 51.43 2.84 1.7766 0 3 3 4 51.64 8.06 1.7699 4 4 0 4 51.73 1.42 1.7670 3 2 2 4 52.28 2.18 1.7498 1 2 3 4 53.20 7.65 1.7218 5 1 0 4 53.48 2.16 1.7133 -3 5 2 4 53.50 1.11 1.7127 4 3 1 4 53.93 3.72 1.7002 3 5 1 4 54.20 1.80 1.6922 -1 6 2 4 54.60 4.55 1.6809 3 3 2 4 54.80 3.01 1.6752 -2 4 3 4 54.90 1.10 1.6725 5 2 0 4 55.13 4.93 1.6661 1 3 3 4 56.25 2.53 1.6355 -4 2 3 4 56.73 1.64 1.6226 4 5 0 4 56.87 4.15 1.6190 1 7 1 4 57.40 1.35 1.6054 4 4 1 4 57.64 1.01 1.5993 -2 7 1 4 58.08 1.52 1.5881 2 2 3 4 58.70 3.73 1.5727 -5 3 2 4 59.38 1.06 1.5564 4 1 2 4 60.56 2.86 1.5288 -2 0 4 2 61.25 3.79 1.5133 -1 7 2 4 61.67 2.84 1.5041 -4 6 1 4 61.70 1.96 1.5034 -5 1 3 4 61.79 1.03 1.5014 0 7 2 4 62.23 2.36 1.4918 2 6 2 4 62.64 4.17 1.4832 -4 4 3 4 63.74 1.01 1.4601 -6 0 2 2 63.81 1.16 1.4587 5 3 1 4 63.89 1.09 1.4571 -6 2 1 4 64.01 1.73 1.4545 3 1 3 4 64.34 1.85 1.4479 1 7 2 4 65.10 2.07 1.4328 -4 6 2 4 65.25 2.91 1.4300 -1 3 4 4 65.46 1.15 1.4258 -2 8 1 4 65.95 1.94 1.4163 0 6 3 4 66.29 1.35 1.4100 6 2 0 4 66.62 2.99 1.4038 3 7 1 4 66.95 1.52 1.3976 -5 5 2 4 67.12 2.85 1.3945 -3 3 4 4 67.24 1.23 1.3924 1 1 4 4 68.69 1.85 1.3664 3 6 2 4 69.16 1.34 1.3584 1 6 3 4 69.87 1.09 1.3463 -6 4 1 4 70.34 1.02 1.3384 1 9 0 4 70.82 1.32 1.3304 6 0 1 2 71.31 1.55 1.3226 6 1 1 4 71.50 1.02 1.3196 4 5 2 4 71.52 1.18 1.3192 -4 7 2 4 71.67 1.94 1.3168 -1 9 1 4 71.75 1.06 1.3155 -6 2 3 4 72.72 2.08 1.3004 -5 1 4 4 73.05 1.03 1.2952 -2 5 4 4 73.10 1.32 1.2946 -1 5 4 4 74.23 1.41 1.2776 -7 1 1 4 74.35 1.72 1.2759 -3 7 3 4 74.44 1.18 1.2745 4 2 3 4 75.48 1.91 1.2595 -4 8 1 4 77.18 1.27 1.2359 7 1 0 4 77.58 1.17 1.2306 5 7 0 4 78.26 1.42 1.2216 -2 6 4 4 80.43 1.30 1.1940 0 10 1 4 84.79 1.38 1.1434 5 2 3 4 84.83 1.46 1.1430 -5 7 3 4 85.40 1.00 1.1368 7 2 1 4 87.01 1.44 1.1198 -6 4 4 4 87.15 1.22 1.1185 -2 10 2 4 89.69 1.13 1.0932 4 8 2 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.