Metatorbernite Stubbs J E, Post J E, Elbert D C, Heaney P J, Veblen D R American Mineralogist 95 (2010) 1132-1140 Uranyl phosphate sheet reconstruction during dehydration of metatorbernite [Cu(UO2)2(PO4)2*8H2O] Note: This is the 6.9 Angstrom phase while heating at 173 C Locality: Bois Noirs, France _database_code_amcsd 0016813 CELL PARAMETERS: 14.4979 7.0159 6.6312 90.000 107.585 90.000 SPACE GROUP: P2_1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 642.979 Density (g/cm3): 4.388 MAX. ABS. INTENSITY / VOLUME**2: 102.0823440 RIR: 7.575 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 12.81 100.00 6.9102 2 0 0 2 13.53 2.80 6.5449 -1 0 1 2 14.01 7.75 6.3213 0 0 1 2 14.16 4.84 6.2560 1 1 0 2 15.89 28.46 5.5784 -2 0 1 2 18.90 38.80 4.6963 0 1 1 2 20.13 1.81 4.4110 -3 0 1 2 20.34 21.10 4.3664 -2 1 1 2 21.30 4.61 4.1705 1 1 1 2 21.73 3.44 4.0893 2 0 1 2 23.10 1.82 3.8508 3 1 0 2 23.83 2.03 3.7343 -3 1 1 2 25.21 22.74 3.5330 2 1 1 2 25.37 10.76 3.5109 -4 0 1 2 25.39 19.07 3.5080 0 2 0 1 25.79 26.98 3.4551 4 0 0 2 26.21 11.13 3.4001 1 2 0 2 27.25 4.12 3.2725 -2 0 2 2 28.23 2.11 3.1607 0 0 2 2 28.43 5.64 3.1397 -4 1 1 2 28.54 37.37 3.1280 2 2 0 2 28.80 1.06 3.0996 4 1 0 2 28.88 1.24 3.0918 -1 2 1 2 29.11 4.80 3.0673 0 2 1 2 29.88 5.00 2.9905 -1 1 2 2 30.09 5.51 2.9696 -2 2 1 2 30.13 32.46 2.9657 -2 1 2 2 31.03 28.12 2.8817 0 1 2 2 32.07 3.55 2.7909 3 2 0 2 32.61 1.48 2.7456 -3 2 1 2 34.59 3.46 2.5932 2 0 2 2 34.61 9.59 2.5919 -4 1 2 2 35.55 7.24 2.5256 4 1 1 2 36.13 2.21 2.4859 -5 0 2 2 36.20 7.00 2.4815 -4 2 1 2 36.50 4.24 2.4616 4 2 0 2 36.96 8.08 2.4323 2 1 2 2 37.29 4.37 2.4112 -6 0 1 2 38.33 2.20 2.3481 0 2 2 2 38.42 1.36 2.3431 -5 1 2 2 39.11 4.16 2.3034 6 0 0 2 39.52 2.00 2.2803 -6 1 1 2 40.61 1.12 2.2217 -5 2 1 2 40.82 5.05 2.2104 -2 0 3 2 40.98 4.17 2.2023 -1 3 1 2 41.16 5.19 2.1933 0 3 1 2 41.25 2.35 2.1885 6 1 0 2 41.28 1.86 2.1872 3 1 2 2 41.36 1.18 2.1832 -4 2 2 2 41.46 1.14 2.1780 5 1 1 2 41.60 1.30 2.1711 5 2 0 2 41.89 4.54 2.1568 -2 3 1 2 42.40 2.64 2.1319 1 3 1 2 42.92 7.20 2.1071 0 0 3 2 42.99 6.44 2.1040 -6 1 2 2 43.00 4.10 2.1035 -4 0 3 2 44.30 1.28 2.0446 4 0 2 2 44.64 5.28 2.0301 2 3 1 2 44.99 3.10 2.0149 -4 1 3 2 45.66 3.55 1.9871 -6 2 1 2 45.68 1.10 1.9863 -7 1 1 2 46.25 5.23 1.9630 4 1 2 2 46.67 1.82 1.9464 -4 3 1 2 47.21 7.00 1.9254 6 2 0 2 47.63 2.11 1.9092 -1 3 2 2 47.72 5.49 1.9058 6 1 1 2 47.76 2.66 1.9044 3 3 1 2 47.80 5.58 1.9027 -2 3 2 2 48.42 5.32 1.8800 0 3 2 2 48.69 5.39 1.8701 -2 2 3 2 48.85 2.20 1.8645 2 0 3 2 48.93 4.86 1.8616 -3 3 2 2 48.99 1.16 1.8595 -6 0 3 2 49.15 1.87 1.8538 -1 2 3 2 50.13 4.53 1.8196 1 3 2 2 50.32 1.44 1.8132 -5 3 1 2 50.38 3.14 1.8114 -8 0 1 2 50.53 3.09 1.8063 0 2 3 2 50.60 1.86 1.8040 -4 2 3 2 50.80 1.84 1.7974 -6 1 3 2 50.96 3.06 1.7921 -4 3 2 2 51.65 2.77 1.7697 4 3 1 2 51.75 2.20 1.7665 4 2 2 2 52.15 2.10 1.7540 0 4 0 1 52.60 4.10 1.7400 1 4 0 2 52.71 2.33 1.7367 2 3 2 2 53.01 2.63 1.7276 8 0 0 2 53.83 3.71 1.7029 -8 1 2 2 54.72 1.44 1.6774 8 1 0 2 54.87 1.06 1.6732 -2 4 1 2 55.60 2.05 1.6529 -2 0 4 2 55.84 3.30 1.6464 2 2 3 2 55.97 1.67 1.6429 -6 2 3 2 56.06 1.91 1.6405 6 0 2 2 56.11 2.85 1.6392 3 4 0 2 56.20 1.33 1.6366 5 3 1 2 57.24 3.20 1.6095 -8 2 1 2 57.26 1.72 1.6089 -2 1 4 2 57.43 1.81 1.6045 -6 3 2 2 57.71 1.84 1.5974 6 1 2 2 57.72 1.85 1.5972 4 0 3 2 57.87 1.08 1.5935 -4 1 4 2 57.91 1.15 1.5925 -8 0 3 2 59.07 1.49 1.5640 4 4 0 2 59.52 1.86 1.5530 -8 1 3 2 59.66 1.24 1.5498 8 2 0 2 60.01 1.70 1.5417 0 1 4 2 60.11 1.30 1.5393 4 3 2 2 61.18 3.31 1.5149 8 1 1 2 61.34 1.92 1.5113 6 3 1 2 61.72 1.24 1.5030 -7 3 2 2 62.00 1.43 1.4967 -5 4 1 2 62.07 1.52 1.4952 -2 2 4 2 62.65 1.83 1.4829 -4 2 4 2 62.74 1.10 1.4810 5 4 0 2 64.06 1.08 1.4536 4 2 3 2 64.69 1.39 1.4409 0 2 4 2 64.79 1.30 1.4389 5 3 2 2 65.84 1.10 1.4185 2 1 4 2 66.38 1.04 1.4084 -6 2 4 2 66.49 1.83 1.4063 -10 1 2 2 66.61 1.50 1.4039 -8 3 2 2 68.66 1.03 1.3670 -3 4 3 2 68.88 1.03 1.3631 6 0 3 2 69.38 1.18 1.3545 1 5 1 2 69.76 1.03 1.3481 0 4 3 2 70.51 1.52 1.3355 -10 2 1 2 70.58 1.12 1.3344 -10 1 3 2 71.64 1.04 1.3173 1 4 3 2 72.02 1.18 1.3113 7 4 0 2 72.72 1.38 1.3004 -4 1 5 2 73.01 1.17 1.2960 -8 2 4 2 73.17 1.67 1.2934 -2 1 5 2 73.21 1.50 1.2929 8 3 1 2 73.29 1.70 1.2916 -1 5 2 2 74.30 1.10 1.2766 -3 5 2 2 74.41 1.15 1.2750 4 1 4 2 74.71 1.77 1.2705 6 2 3 2 75.25 1.05 1.2628 8 2 2 2 76.02 1.03 1.2519 10 1 1 2 76.57 1.11 1.2442 0 1 5 2 78.23 1.06 1.2219 -5 5 2 2 80.10 1.04 1.1981 3 5 2 2 80.22 1.03 1.1966 5 5 1 2 82.85 1.66 1.1652 1 6 0 2 85.72 1.24 1.1334 3 6 0 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.