Franckeite Makovicky E, Petricek V, Dusek M, Topa D American Mineralogist 96 (2011) 1686-1702 The crystal structure of franckeite, Pb21.7Sn9.3Fe4.0Sb8.1S56.9 Locality: San Jose, Bolivia _database_code_amcsd 0018603 CELL PARAMETERS: 5.8050 5.8560 17.3380 94.970 88.450 89.940 SPACE GROUP: C-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 586.955 Density (g/cm3): 5.300 MAX. ABS. INTENSITY / VOLUME**2: 48.22155631 RIR: 2.963 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 5.12 94.76 17.2664 0 0 1 2 10.25 33.74 8.6332 0 0 2 2 20.58 20.44 4.3166 0 0 4 2 21.56 5.96 4.1212 1 1 0 2 21.64 1.10 4.1072 -1 1 0 2 21.84 2.27 4.0700 1 -1 1 2 21.96 5.37 4.0471 -1 -1 1 2 22.39 22.20 3.9712 1 1 1 2 22.65 5.45 3.9254 -1 1 1 2 23.53 43.62 3.7813 -1 -1 2 2 24.74 49.43 3.5984 -1 1 2 2 25.61 100.00 3.4779 1 -1 3 2 25.80 59.91 3.4533 0 0 5 2 26.06 29.95 3.4193 -1 -1 3 2 27.14 31.88 3.2862 1 1 3 2 27.68 21.68 3.2231 -1 1 3 2 29.33 23.66 3.0452 -1 -1 4 2 30.61 19.83 2.9203 1 1 4 2 30.65 45.32 2.9170 0 2 0 2 30.82 22.36 2.9014 2 0 0 2 31.08 51.82 2.8777 0 0 6 2 31.12 44.02 2.8741 2 0 1 2 31.40 41.76 2.8487 -2 0 1 2 31.51 27.49 2.8391 0 -2 2 2 31.55 40.80 2.8361 0 2 1 2 32.28 9.61 2.7732 2 0 2 2 33.14 1.89 2.7032 -1 -1 5 2 33.26 6.17 2.6936 0 2 2 2 34.23 3.12 2.6197 2 0 3 2 34.58 6.01 2.5939 1 1 5 2 35.27 1.10 2.5444 -1 1 5 2 35.69 7.10 2.5154 0 2 3 2 36.85 9.85 2.4390 2 0 4 2 37.83 6.18 2.3782 -2 0 4 2 38.64 18.19 2.3302 0 -2 5 2 38.73 4.17 2.3252 0 2 4 2 38.91 4.33 2.3144 1 1 6 2 39.66 10.81 2.2726 -1 1 6 2 40.04 2.68 2.2518 2 0 5 2 41.15 4.97 2.1938 1 -1 7 2 41.18 26.22 2.1922 -2 0 5 2 41.86 3.00 2.1583 0 0 8 2 41.89 2.46 2.1567 -1 -1 7 2 42.16 15.02 2.1436 0 -2 6 2 43.54 2.09 2.0785 1 1 7 2 43.69 8.80 2.0716 2 0 6 2 43.94 2.07 2.0606 2 2 0 2 43.98 21.13 2.0587 2 -2 1 2 44.04 11.37 2.0562 -2 -2 1 2 44.10 9.98 2.0536 -2 2 0 2 44.33 3.02 2.0434 -1 1 7 2 44.50 20.07 2.0361 2 2 1 2 44.79 1.57 2.0235 -2 -2 2 2 45.90 7.86 1.9771 1 -1 8 2 46.09 6.06 1.9696 0 -2 7 2 46.19 21.96 1.9652 0 2 6 2 46.26 1.85 1.9627 -2 2 2 2 46.68 15.68 1.9458 -1 -1 8 2 47.39 2.17 1.9185 0 0 9 2 47.74 13.11 1.9051 2 0 7 2 48.13 7.01 1.8906 -2 -2 4 2 48.23 4.74 1.8868 -2 2 3 2 49.13 3.41 1.8545 -2 0 7 2 49.24 5.82 1.8504 -1 1 8 2 49.27 2.00 1.8494 1 -3 1 2 49.48 2.45 1.8420 -1 3 0 2 49.66 4.53 1.8358 1 -3 2 2 49.75 11.15 1.8328 -1 -3 2 2 49.83 1.07 1.8300 2 2 4 2 49.89 7.15 1.8278 -3 -1 1 2 50.31 2.70 1.8138 -3 1 1 2 50.31 4.45 1.8138 3 -1 2 2 50.63 3.08 1.8031 -2 -2 5 2 50.64 4.01 1.8025 1 -3 3 2 50.74 2.98 1.7992 -2 2 4 2 50.78 1.24 1.7981 -3 -1 2 2 50.81 2.61 1.7971 3 1 2 2 50.89 5.91 1.7943 1 -1 9 2 51.38 3.30 1.7784 1 3 2 2 51.48 6.37 1.7750 -3 1 2 2 51.48 2.73 1.7750 3 -1 3 2 52.46 1.65 1.7442 -1 -3 4 2 52.63 14.42 1.7390 2 -2 6 2 52.67 8.79 1.7378 2 2 5 2 53.21 3.19 1.7213 3 -1 4 2 53.22 3.09 1.7211 1 3 3 2 53.52 10.08 1.7120 1 1 9 2 53.60 6.40 1.7098 -1 3 3 2 53.61 1.38 1.7096 -2 -2 6 2 53.73 6.49 1.7059 -2 2 5 2 54.22 2.42 1.6918 -3 -1 4 2 54.27 2.10 1.6902 1 -3 5 2 54.28 6.85 1.6901 3 1 4 2 54.38 2.08 1.6870 -1 1 9 2 55.57 2.10 1.6537 1 3 4 2 55.91 1.44 1.6445 2 -2 7 2 55.96 1.13 1.6431 2 2 6 2 56.70 1.04 1.6234 -3 -1 5 2 57.02 5.37 1.6150 -2 -2 7 2 57.16 2.75 1.6115 -2 2 6 2 58.83 3.16 1.5697 0 0 11 2 59.65 2.34 1.5499 -3 -1 6 2 59.66 3.05 1.5498 2 2 7 2 59.74 1.70 1.5479 -1 1 10 2 60.38 3.33 1.5329 -1 -3 7 2 60.98 1.25 1.5194 -2 2 7 2 61.37 1.44 1.5107 3 -1 7 2 62.26 1.29 1.4912 -1 3 6 2 63.03 2.16 1.4748 -3 -1 7 2 63.33 2.44 1.4685 1 -3 8 2 63.44 4.27 1.4663 -2 0 10 2 63.55 2.41 1.4640 0 -4 1 2 63.79 1.67 1.4590 0 -4 2 2 63.82 1.91 1.4585 0 4 0 2 63.90 1.54 1.4567 -1 -3 8 2 64.20 1.45 1.4507 4 0 0 2 64.59 1.91 1.4429 0 4 1 2 64.62 2.47 1.4423 -4 0 1 2 64.79 2.67 1.4389 0 0 12 2 64.89 3.92 1.4371 4 0 2 2 64.95 5.14 1.4358 -3 1 7 2 64.98 4.80 1.4351 0 -2 11 2 65.34 2.95 1.4282 1 3 7 2 66.92 2.56 1.3983 3 1 8 2 66.95 1.10 1.3977 -4 0 3 2 67.18 1.89 1.3934 1 -3 9 2 67.19 1.30 1.3933 1 -1 12 2 67.51 3.93 1.3874 0 -4 5 2 68.54 1.05 1.3691 -3 3 0 2 68.83 1.40 1.3640 -4 0 4 2 68.93 1.24 1.3624 3 -1 9 2 69.28 1.06 1.3562 -3 3 1 2 69.61 1.46 1.3507 4 0 5 2 69.70 2.77 1.3490 -3 -3 3 2 69.77 1.89 1.3479 3 3 2 2 69.84 3.15 1.3468 0 4 4 2 70.11 2.47 1.3422 -1 3 8 2 70.47 2.03 1.3363 3 -3 4 2 70.50 1.08 1.3357 -3 3 2 2 70.56 1.75 1.3348 0 2 11 2 70.97 1.69 1.3281 -3 -1 9 2 72.10 1.10 1.3100 -1 -3 10 2 72.25 2.73 1.3076 -2 -4 1 2 72.53 3.21 1.3033 2 0 12 2 72.66 3.01 1.3013 -2 4 0 2 72.70 3.81 1.3007 4 2 0 2 72.76 2.07 1.2997 4 -2 1 2 72.84 1.00 1.2984 2 -2 11 2 72.94 1.66 1.2970 2 2 10 2 73.08 1.52 1.2948 4 -2 2 2 73.10 1.09 1.2945 2 -4 3 2 73.27 1.46 1.2919 3 -1 10 2 73.97 1.94 1.2815 -4 0 6 2 74.07 2.36 1.2799 -1 -1 13 2 75.05 1.44 1.2656 4 0 7 2 76.86 1.32 1.2403 4 -2 5 2 77.79 1.28 1.2277 2 -4 6 2 77.96 1.40 1.2256 2 -2 12 2 78.28 2.73 1.2213 -4 2 4 2 78.48 2.23 1.2187 -2 -4 6 2 79.03 1.27 1.2115 4 2 5 2 79.66 1.21 1.2036 -2 -2 12 2 79.83 1.53 1.2014 -2 2 11 2 80.34 1.05 1.1951 2 4 5 2 80.62 1.02 1.1916 -4 -2 6 2 81.31 1.79 1.1833 -2 4 5 2 83.36 1.65 1.1593 3 -3 9 2 83.66 1.43 1.1559 -1 1 14 2 87.05 1.09 1.1194 5 1 3 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.