Nambulite Nagashima M, Armbruster T, Kolitsch U, Pettke T American Mineralogist 99 (2014) 1462-1470 The relation between Li <-> Na substitution and hydrogen bonding in five-periodic single-chain silicates nambulite and marsturite: A single-crystal X-ray study Locality: Gozaisho mine, Iwaki, Japan _database_code_amcsd 0020223 CELL PARAMETERS: 7.5372 11.7267 6.7078 93.057 95.147 106.240 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 565.017 Density (g/cm3): 3.540 MAX. ABS. INTENSITY / VOLUME**2: 8.034334962 RIR: 0.739 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.88 10.45 11.2209 0 1 0 2 12.30 1.09 7.1932 1 0 0 2 12.58 27.08 7.0391 -1 1 0 2 13.30 31.58 6.6582 0 0 1 2 15.80 3.51 5.6104 0 2 0 2 16.03 1.76 5.5305 0 1 1 2 17.13 6.31 5.1760 -1 0 1 2 18.85 15.75 4.7088 1 -1 1 2 19.13 2.55 4.6404 1 0 1 2 21.64 3.57 4.1061 -1 2 1 2 22.72 2.26 3.9142 1 2 0 2 23.46 3.80 3.7919 -1 3 0 2 23.72 3.17 3.7510 -2 1 0 2 25.01 3.06 3.5606 -1 -2 1 2 25.31 19.15 3.5196 -2 2 0 2 26.24 1.12 3.3959 -2 1 1 2 26.76 7.39 3.3319 1 -3 1 2 26.78 12.50 3.3291 0 0 2 2 26.86 12.50 3.3196 -2 0 1 2 27.36 3.04 3.2593 -1 3 1 2 27.75 1.67 3.2146 1 2 1 2 28.28 53.79 3.1553 -1 0 2 2 28.30 4.12 3.1536 2 -1 1 2 28.31 2.27 3.1525 0 3 1 2 28.59 19.61 3.1226 0 1 2 2 29.03 8.71 3.0760 -1 1 2 2 29.11 10.36 3.0676 -2 3 0 2 29.35 48.12 3.0428 2 -2 1 2 29.72 1.59 3.0060 -2 -1 1 2 29.78 22.31 3.0004 -1 -1 2 2 29.91 4.69 2.9872 1 3 0 2 30.07 18.22 2.9720 0 -2 2 2 30.33 56.12 2.9471 1 -1 2 2 30.72 100.00 2.9104 -1 4 0 2 30.80 1.63 2.9029 1 0 2 2 31.80 4.51 2.8139 -2 3 1 2 31.90 1.28 2.8052 0 4 0 2 31.95 1.99 2.8008 1 -2 2 2 32.45 1.09 2.7592 2 -3 1 2 33.08 1.51 2.7078 1 -4 1 2 33.21 99.57 2.6976 2 2 0 2 33.29 2.42 2.6911 1 1 2 2 33.64 2.59 2.6645 0 -4 1 2 34.12 27.15 2.6276 -1 4 1 2 34.24 1.77 2.6192 1 3 1 2 34.32 9.59 2.6129 -2 -2 1 2 34.44 27.32 2.6041 -2 1 2 2 34.47 1.50 2.6021 -2 4 0 2 34.66 3.19 2.5880 -2 0 2 2 35.99 4.82 2.4952 -3 1 0 2 36.29 21.43 2.4755 -3 2 0 2 37.26 2.31 2.4133 -3 1 1 2 37.45 19.92 2.4015 1 2 2 2 37.46 1.80 2.4009 2 2 1 2 37.61 5.15 2.3913 0 3 2 2 37.79 2.59 2.3805 -3 2 1 2 38.18 1.52 2.3570 -1 -3 2 2 38.23 1.91 2.3544 2 -2 2 2 38.36 1.30 2.3464 -3 3 0 2 38.81 1.72 2.3202 2 0 2 2 39.77 2.52 2.2666 3 -1 1 2 40.19 1.26 2.2440 1 -5 1 2 40.31 24.29 2.2375 0 -4 2 2 40.50 1.20 2.2275 2 -3 2 2 40.66 13.95 2.2187 3 1 0 2 40.79 5.79 2.2120 0 -1 3 2 40.86 26.79 2.2087 -2 5 0 2 41.24 33.77 2.1891 -1 0 3 2 41.39 1.36 2.1815 0 -5 1 2 41.99 2.79 2.1518 -3 4 0 2 42.15 1.45 2.1440 0 1 3 2 42.56 1.10 2.1243 0 -2 3 2 42.97 12.75 2.1050 2 -5 1 2 43.34 1.11 2.0878 -2 5 1 2 43.35 1.72 2.0871 2 3 1 2 43.88 4.40 2.0635 -3 2 2 2 44.11 1.24 2.0530 -2 4 2 2 44.53 20.96 2.0346 3 1 1 2 45.66 7.15 1.9868 -2 1 3 2 45.79 1.31 1.9816 2 2 2 2 46.33 1.30 1.9599 -1 -5 1 2 46.93 4.60 1.9359 0 -5 2 2 48.65 6.79 1.8715 -1 5 2 2 48.95 2.89 1.8608 -4 1 0 2 49.19 1.58 1.8522 2 -5 2 2 49.44 1.84 1.8435 0 3 3 2 49.52 2.66 1.8408 1 2 3 2 49.57 3.36 1.8391 -4 3 0 2 49.86 3.57 1.8290 -2 5 2 2 49.95 1.72 1.8260 -2 -2 3 2 50.10 3.47 1.8206 -2 3 3 2 50.16 5.22 1.8187 -3 -2 2 2 50.54 3.48 1.8061 -4 3 1 2 50.77 2.22 1.7983 4 0 0 2 51.09 4.72 1.7876 2 3 2 2 51.32 2.72 1.7803 -2 -4 2 2 51.36 1.53 1.7790 3 -4 2 2 52.15 4.14 1.7538 3 1 2 2 52.56 3.52 1.7411 4 -3 1 2 52.89 1.34 1.7310 -1 4 3 2 53.08 1.46 1.7253 -3 0 3 2 53.12 5.50 1.7242 2 1 3 2 54.04 1.34 1.6971 -2 -3 3 2 54.07 1.34 1.6960 -4 -1 1 2 54.08 28.04 1.6957 1 6 0 2 54.24 6.28 1.6910 -2 4 3 2 54.27 7.97 1.6903 4 0 1 2 54.36 10.09 1.6878 -3 5 2 2 54.72 14.14 1.6775 3 -6 1 2 55.01 6.56 1.6692 -3 -3 2 2 55.11 17.83 1.6665 0 -1 4 2 55.13 1.22 1.6660 2 -6 2 2 55.35 1.02 1.6598 -4 0 2 2 55.62 8.75 1.6525 1 -5 3 2 56.35 2.32 1.6327 0 -2 4 2 57.40 7.84 1.6053 1 6 1 2 57.49 3.12 1.6030 0 7 0 2 57.95 11.20 1.5913 -4 -1 2 2 58.13 6.16 1.5870 -3 -2 3 2 58.24 3.54 1.5841 1 -2 4 2 58.56 4.39 1.5762 0 6 2 2 58.71 4.32 1.5727 -2 1 4 2 58.83 8.64 1.5696 3 -3 3 2 60.07 1.35 1.5402 -3 6 2 2 60.23 3.81 1.5366 3 -6 2 2 61.19 5.84 1.5146 4 0 2 2 61.40 2.93 1.5101 -3 7 1 2 61.40 2.60 1.5100 -1 3 4 2 61.71 3.66 1.5032 -4 6 1 2 61.90 2.29 1.4991 2 -7 2 2 61.96 2.86 1.4977 -4 2 3 2 62.18 1.49 1.4929 0 -7 2 2 62.50 1.89 1.4860 0 -4 4 2 63.13 12.75 1.4726 -3 5 3 2 63.74 1.32 1.4602 2 -6 3 2 63.87 2.92 1.4575 -1 7 2 2 64.24 1.21 1.4500 -3 1 4 2 64.34 2.12 1.4478 -5 4 1 2 64.35 4.71 1.4477 2 5 2 2 64.58 1.33 1.4431 -3 0 4 2 64.60 2.25 1.4426 1 -8 1 2 64.74 1.21 1.4399 -1 -4 4 2 64.79 3.79 1.4390 -5 0 1 2 64.81 1.35 1.4386 5 0 0 2 65.11 6.21 1.4326 -4 -1 3 2 65.28 2.79 1.4294 -2 -3 4 2 65.61 7.91 1.4229 -2 -6 2 2 66.31 3.29 1.4097 -2 8 1 2 66.44 18.64 1.4071 5 -4 1 2 66.48 16.35 1.4064 2 1 4 2 66.52 1.73 1.4056 -5 3 2 2 66.82 1.51 1.4001 0 7 2 2 67.38 10.37 1.3899 1 -5 4 2 67.53 1.98 1.3871 -3 -5 2 2 67.64 1.60 1.3852 3 4 2 2 68.17 1.34 1.3756 0 6 3 2 68.66 1.61 1.3670 1 -8 2 2 69.72 2.21 1.3488 4 4 0 2 69.77 1.33 1.3479 -2 -4 4 2 69.85 1.86 1.3465 2 -7 3 2 70.05 1.29 1.3432 4 -4 3 2 71.25 3.08 1.3235 3 -3 4 2 72.13 1.42 1.3095 -3 -6 1 2 72.33 1.64 1.3064 -4 -4 2 2 72.39 2.06 1.3055 5 -4 2 2 72.49 1.68 1.3039 1 7 2 2 72.59 1.68 1.3024 3 0 4 2 72.75 1.52 1.2998 -5 2 3 2 72.93 4.15 1.2971 -1 7 3 2 73.25 1.01 1.2922 -1 9 0 2 73.43 2.20 1.2895 -1 -7 3 2 73.53 5.97 1.2880 -5 3 3 2 73.83 2.76 1.2836 -2 -7 2 2 74.03 1.30 1.2806 4 1 3 2 74.59 1.00 1.2722 -5 0 3 2 74.95 2.49 1.2671 2 -6 4 2 75.08 1.07 1.2652 -4 -1 4 2 76.26 1.34 1.2486 -6 3 1 2 76.82 1.26 1.2408 4 5 0 2 77.18 1.69 1.2360 -3 9 1 2 77.33 2.95 1.2340 -6 4 1 2 78.05 1.70 1.2243 -3 1 5 2 78.69 5.36 1.2159 1 5 4 2 80.73 1.28 1.1903 -6 4 2 2 81.22 1.94 1.1844 5 3 1 2 81.82 2.13 1.1772 4 -4 4 2 83.04 2.90 1.1630 -1 -7 4 2 84.74 1.45 1.1440 2 -9 3 2 87.59 1.43 1.1139 -1 -1 6 2 88.32 1.35 1.1066 -3 5 5 2 88.80 1.31 1.1019 -1 -2 6 2 89.55 1.59 1.0946 -2 0 6 2 89.83 1.44 1.0919 0 10 1 2 89.83 4.37 1.0919 4 -10 1 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.