Kulanite Cooper M A, Hawthorne F C The Canadian Mineralogist 32 (1994) 15-19 Refinement of the crystal structure of kulanite Note: occupancies of M1 and M2 have been switched, as noted by authors, 2006 Locality: Rapid Creek, Yukon, Canada _database_code_amcsd 0005343 CELL PARAMETERS: 9.0140 12.0740 4.9260 90.000 100.480 90.000 SPACE GROUP: P2_1/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 527.178 Density (g/cm3): 3.880 MAX. ABS. INTENSITY / VOLUME**2: 15.34336688 RIR: 1.287 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.98 58.27 8.8636 1 0 0 2 12.39 2.03 7.1450 1 1 0 4 14.67 11.05 6.0370 0 2 0 2 17.78 29.32 4.9896 1 2 0 4 18.32 1.15 4.8438 0 0 1 2 19.22 15.86 4.6187 -1 0 1 2 19.75 36.94 4.4956 0 1 1 4 20.59 5.50 4.3139 -1 1 1 4 21.36 9.51 4.1604 2 1 0 4 23.55 1.12 3.7780 0 2 1 4 24.29 2.45 3.6646 1 3 0 4 24.92 27.06 3.5725 2 2 0 4 25.74 13.59 3.4617 -2 1 1 4 26.93 7.82 3.3102 1 2 1 4 28.79 41.25 3.1005 -2 2 1 4 28.84 100.00 3.0956 0 3 1 4 29.44 52.67 3.0343 -1 3 1 4 29.99 18.99 2.9794 2 3 0 4 30.62 53.73 2.9193 2 1 1 4 31.16 24.75 2.8699 3 1 0 4 31.30 15.03 2.8574 1 4 0 4 31.71 30.79 2.8221 1 3 1 4 32.50 1.44 2.7549 -3 0 1 2 33.27 30.56 2.6927 2 2 1 4 33.36 40.71 2.6859 -3 1 1 4 33.78 40.27 2.6538 3 2 0 4 35.53 3.32 2.5268 -1 4 1 4 35.83 7.59 2.5063 -3 2 1 4 36.00 5.14 2.4948 2 4 0 4 36.64 23.59 2.4524 -1 0 2 2 37.12 22.36 2.4219 0 0 2 2 37.32 1.29 2.4097 2 3 1 4 37.47 6.03 2.4002 1 4 1 4 37.77 10.27 2.3817 3 3 0 4 37.89 1.95 2.3746 0 1 2 4 38.64 2.09 2.3299 1 5 0 4 38.88 5.93 2.3166 -2 4 1 4 39.00 4.25 2.3094 -2 0 2 2 39.21 3.64 2.2974 3 1 1 4 39.67 2.16 2.2721 -1 2 2 4 39.74 10.42 2.2683 -2 1 2 4 40.12 3.53 2.2478 0 2 2 4 40.72 1.10 2.2159 4 0 0 2 41.07 1.72 2.1978 1 1 2 4 41.43 14.79 2.1795 4 1 0 4 41.80 5.48 2.1611 0 5 1 4 41.88 2.08 2.1569 -2 2 2 4 42.23 28.71 2.1400 -1 5 1 4 42.64 6.17 2.1205 2 5 0 4 42.83 8.37 2.1114 3 4 0 4 43.16 13.00 2.0961 1 2 2 4 43.20 1.68 2.0943 -1 3 2 4 43.51 1.55 2.0802 4 2 0 4 43.81 2.05 2.0664 -3 0 2 2 43.92 5.45 2.0615 1 5 1 4 44.36 11.62 2.0420 -4 2 1 4 44.48 6.12 2.0367 -3 1 2 4 44.53 10.32 2.0348 -3 4 1 4 44.80 1.56 2.0231 3 3 1 4 45.05 24.69 2.0123 0 6 0 2 45.16 2.42 2.0077 -2 5 1 4 45.27 6.65 2.0030 -2 3 2 4 45.85 5.56 1.9792 2 0 2 2 46.26 3.25 1.9624 1 6 0 4 46.45 4.27 1.9550 -3 2 2 4 46.47 7.50 1.9541 1 3 2 4 46.50 4.82 1.9531 2 1 2 4 46.80 1.08 1.9411 4 3 0 4 47.61 4.94 1.9100 -4 3 1 4 48.33 3.74 1.8832 2 5 1 4 48.40 9.12 1.8807 2 2 2 4 48.70 1.59 1.8697 3 5 0 4 49.27 6.72 1.8495 3 4 1 4 49.40 3.60 1.8448 -1 6 1 4 49.71 5.18 1.8341 -2 4 2 4 50.24 3.96 1.8159 -3 5 1 4 50.52 2.78 1.8067 -4 0 2 2 50.63 1.29 1.8030 4 2 1 4 50.83 6.04 1.7963 1 4 2 4 51.12 8.32 1.7868 -4 1 2 4 51.56 5.18 1.7727 5 0 0 2 51.58 1.33 1.7720 -5 0 1 2 51.90 6.66 1.7619 -4 4 1 4 52.15 3.78 1.7539 5 1 0 4 52.90 3.17 1.7309 -4 2 2 4 53.08 1.50 1.7255 3 0 2 2 53.24 1.45 1.7207 -1 5 2 4 53.59 1.03 1.7102 4 3 1 4 53.66 2.40 1.7081 3 1 2 4 53.76 3.34 1.7051 -3 4 2 4 53.92 1.48 1.7003 -5 2 1 4 54.61 9.48 1.6805 3 5 1 4 55.02 6.87 1.6690 -2 5 2 4 55.38 6.20 1.6590 3 2 2 4 55.52 2.77 1.6551 2 4 2 4 56.07 1.59 1.6403 1 5 2 4 56.57 1.39 1.6270 -1 1 3 4 56.64 3.49 1.6250 -3 6 1 4 56.65 3.63 1.6249 0 7 1 4 56.74 3.50 1.6223 5 3 0 4 57.05 1.94 1.6145 -2 0 3 2 57.06 1.55 1.6140 -4 5 1 4 57.55 9.50 1.6014 4 4 1 4 58.62 9.85 1.5749 5 0 1 2 58.82 1.56 1.5700 -3 5 2 4 59.22 1.94 1.5602 -5 1 2 4 59.25 3.02 1.5596 -2 2 3 4 59.41 6.66 1.5557 -1 6 2 4 59.64 1.25 1.5502 -4 4 2 4 59.75 4.52 1.5478 0 6 2 4 60.48 2.24 1.5307 2 5 2 4 60.57 1.67 1.5286 5 4 0 4 60.59 7.15 1.5282 -5 4 1 4 60.62 1.57 1.5275 1 1 3 4 60.63 4.18 1.5272 -3 1 3 4 60.70 1.87 1.5258 3 6 1 4 60.78 1.08 1.5239 5 2 1 4 60.94 5.97 1.5203 -1 3 3 4 61.43 3.32 1.5093 0 8 0 2 61.66 2.21 1.5043 4 0 2 2 61.92 12.52 1.4985 0 3 3 4 61.93 2.41 1.4984 -2 3 3 4 61.95 3.55 1.4980 3 4 2 4 62.02 7.91 1.4964 2 7 1 4 62.19 2.32 1.4927 4 1 2 4 62.23 4.40 1.4918 -3 2 3 4 62.28 4.60 1.4907 -6 0 1 2 62.33 9.99 1.4896 3 7 0 4 62.42 1.06 1.4878 1 8 0 4 63.43 2.23 1.4666 5 3 1 4 63.44 1.85 1.4663 6 1 0 4 63.48 11.15 1.4654 -5 3 2 4 63.65 6.74 1.4620 -3 7 1 4 64.97 1.23 1.4354 2 0 3 2 65.01 1.23 1.4346 -1 8 1 4 65.30 1.35 1.4290 5 5 0 4 65.48 5.16 1.4254 2 1 3 4 65.57 3.76 1.4237 0 4 3 4 66.23 1.20 1.4111 2 6 2 4 66.28 2.92 1.4102 1 8 1 4 66.34 2.47 1.4091 4 3 2 4 67.03 2.09 1.3962 5 4 1 4 67.08 3.39 1.3952 -5 4 2 4 67.22 3.43 1.3927 -2 8 1 4 67.55 1.81 1.3868 6 3 0 4 68.40 4.12 1.3715 -3 4 3 4 68.57 1.98 1.3686 -6 1 2 4 68.74 1.74 1.3655 1 7 2 4 69.00 2.83 1.3611 4 7 0 4 69.71 4.05 1.3490 2 8 1 4 70.00 3.28 1.3440 3 8 0 4 70.11 1.25 1.3422 0 5 3 4 70.84 1.14 1.3302 5 6 0 4 70.86 2.41 1.3299 -5 6 1 4 71.21 1.64 1.3242 -3 7 2 4 71.43 1.75 1.3206 5 0 2 2 71.84 1.76 1.3141 6 2 1 4 71.93 1.55 1.3127 5 1 2 4 72.53 1.97 1.3033 -6 3 2 4 72.85 2.29 1.2983 1 5 3 4 72.86 1.17 1.2982 -3 5 3 4 73.00 1.74 1.2961 -4 4 3 4 73.21 1.75 1.2929 0 9 1 4 73.48 1.34 1.2887 -5 2 3 4 73.71 1.37 1.2854 -1 8 2 4 73.80 1.39 1.2840 2 9 0 4 74.01 1.51 1.2809 0 8 2 4 75.43 2.29 1.2602 6 5 0 4 75.77 1.00 1.2555 -7 2 1 4 75.82 3.78 1.2548 5 3 2 4 75.89 1.21 1.2538 3 3 3 4 76.10 1.72 1.2508 1 8 2 4 76.33 3.12 1.2476 -4 7 2 4 76.87 6.74 1.2402 5 6 1 4 76.94 1.28 1.2393 7 2 0 4 77.16 2.06 1.2362 5 7 0 4 77.35 1.84 1.2337 -4 5 3 4 77.61 4.83 1.2302 -1 0 4 2 78.39 1.22 1.2199 3 7 2 4 79.23 1.14 1.2090 3 4 3 4 79.26 4.43 1.2087 -5 4 3 4 79.32 1.32 1.2079 7 3 0 4 79.36 1.35 1.2074 0 10 0 2 79.56 1.01 1.2049 0 1 4 4 79.59 1.97 1.2045 -6 0 3 2 79.94 2.12 1.2001 2 8 2 4 80.12 2.69 1.1978 -6 6 1 4 80.24 1.24 1.1964 1 10 0 4 80.82 1.71 1.1893 -1 7 3 4 80.98 1.04 1.1873 0 2 4 4 82.59 1.02 1.1681 -1 10 1 4 83.09 2.26 1.1624 -5 7 2 4 83.30 1.42 1.1600 -2 9 2 4 83.42 1.24 1.1586 5 5 2 4 83.49 2.18 1.1579 3 5 3 4 84.22 1.97 1.1497 -3 3 4 4 84.24 2.34 1.1494 -4 1 4 4 84.41 1.45 1.1476 4 9 0 4 85.72 2.62 1.1334 -7 5 1 4 86.32 2.15 1.1270 7 3 1 4 86.86 1.03 1.1214 7 5 0 4 88.34 1.13 1.1064 -8 2 1 4 88.65 2.36 1.1033 2 7 3 4 88.65 2.81 1.1033 8 1 0 4 88.73 2.73 1.1025 -2 8 3 4 89.10 2.10 1.0989 2 2 4 4 89.16 1.03 1.0984 5 0 3 2 89.74 1.25 1.0927 -5 1 4 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.