Na3Ca6(UO2)4(CO3)12(H2O)17 Vochten R, Haverbeke L V, Springel K V The Canadian Mineralogist 32 (1994) 553-561 The structure and physicochemical characteristics of a synthetic phase compositionally intermediate between liebigite and andersonite _database_code_amcsd 0005406 CELL PARAMETERS: 18.1500 16.8660 18.4360 90.000 90.000 90.000 SPACE GROUP: Pnnm X-RAY WAVELENGTH: 1.541838 Cell Volume: 5643.589 Density (g/cm3): 2.886 MAX. ABS. INTENSITY / VOLUME**2: 37.09683505 RIR: 4.185 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.10 3.25 12.4442 0 1 1 4 8.62 3.32 10.2635 1 1 1 8 9.59 4.15 9.2180 0 0 2 2 10.49 78.99 8.4330 0 2 0 2 13.69 61.84 6.4670 2 0 2 4 14.34 8.38 6.1775 2 2 0 4 15.05 14.59 5.8858 1 2 2 8 15.35 1.09 5.7740 0 1 3 4 16.11 9.04 5.5023 1 1 3 8 16.29 5.74 5.4410 3 1 1 8 16.48 2.14 5.3775 0 3 1 4 17.28 100.00 5.1317 2 2 2 8 18.05 10.62 4.9158 3 2 0 4 18.21 2.10 4.8715 2 1 3 8 19.26 23.87 4.6090 0 0 4 2 19.56 15.10 4.5375 4 0 0 2 20.48 2.14 4.3376 3 2 2 8 21.07 3.22 4.2165 0 4 0 2 21.42 1.50 4.1481 0 3 3 4 21.64 4.43 4.1071 1 4 0 4 21.98 21.94 4.0444 0 2 4 4 21.98 2.98 4.0438 1 3 3 8 22.12 3.69 4.0193 3 3 1 8 22.25 27.56 3.9958 4 2 0 4 22.52 6.47 3.9476 1 2 4 8 23.20 1.26 3.8344 0 4 2 4 23.58 3.43 3.7726 2 3 3 8 23.72 7.83 3.7516 1 4 2 8 24.09 1.94 3.6941 2 2 4 8 25.21 5.13 3.5332 1 1 5 8 25.21 20.45 3.5321 2 4 2 8 25.69 4.34 3.4679 4 3 1 8 25.75 10.80 3.4593 3 4 0 4 26.62 1.04 3.3480 2 1 5 8 26.87 2.24 3.3181 0 5 1 4 27.54 4.22 3.2387 3 4 2 8 27.59 7.75 3.2335 4 0 4 4 28.65 1.25 3.1163 2 5 1 8 28.69 4.25 3.1110 0 4 4 4 28.85 4.01 3.0951 3 1 5 8 28.91 8.58 3.0888 4 4 0 4 29.06 5.57 3.0731 5 1 3 8 29.06 2.05 3.0727 0 0 6 2 29.12 7.58 3.0663 1 4 4 8 29.38 2.26 3.0397 1 3 5 8 29.53 2.71 3.0250 6 0 0 2 29.59 9.53 3.0191 4 2 4 8 30.72 9.62 2.9104 2 0 6 4 31.12 9.22 2.8742 6 0 2 4 31.37 3.56 2.8512 1 2 6 8 31.72 1.40 2.8212 4 1 5 8 31.83 7.20 2.8115 2 5 3 8 32.22 1.60 2.7779 1 6 0 4 32.36 1.62 2.7667 3 4 4 8 32.55 12.25 2.7511 2 2 6 8 32.60 1.35 2.7471 3 3 5 8 32.78 1.89 2.7317 5 3 3 8 32.92 15.78 2.7205 6 2 2 8 33.16 1.72 2.7015 5 2 4 8 33.32 1.91 2.6888 0 6 2 4 33.46 2.37 2.6784 4 5 1 8 33.70 2.32 2.6597 1 6 2 8 33.74 2.93 2.6567 3 5 3 8 34.01 2.96 2.6361 5 4 2 8 34.80 1.81 2.5780 2 6 2 8 34.83 1.07 2.5758 1 1 7 8 34.97 10.89 2.5659 4 4 4 8 35.19 1.53 2.5502 4 3 5 8 35.20 2.90 2.5493 3 6 0 4 35.28 1.02 2.5442 4 0 6 4 35.36 2.52 2.5383 7 1 1 8 35.90 1.32 2.5014 2 1 7 8 36.09 2.18 2.4888 0 5 5 4 36.57 3.56 2.4570 3 6 2 8 36.77 3.06 2.4441 6 3 3 8 37.48 1.36 2.3999 0 6 4 4 37.55 3.99 2.3952 2 4 6 8 37.64 1.29 2.3896 4 6 0 4 37.81 1.23 2.3792 1 6 4 8 37.88 3.63 2.3749 6 4 2 8 37.99 1.15 2.3687 1 7 1 8 38.05 6.04 2.3647 1 3 7 8 38.98 1.42 2.3104 2 7 1 8 39.05 3.54 2.3067 2 3 7 8 39.09 1.39 2.3045 0 0 8 2 39.73 1.06 2.2687 8 0 0 2 40.35 1.30 2.2355 6 5 1 8 40.43 1.85 2.2308 3 6 4 8 40.58 1.90 2.2230 0 2 8 4 40.86 4.22 2.2087 7 4 0 4 41.20 2.29 2.1908 8 2 0 4 41.38 3.41 2.1821 4 5 5 8 41.45 1.43 2.1784 4 4 6 8 41.47 2.68 2.1776 2 7 3 8 41.81 3.82 2.1606 5 6 2 8 41.84 1.34 2.1592 2 2 8 8 41.91 1.51 2.1557 6 0 6 4 42.07 2.09 2.1479 7 4 2 8 42.76 3.93 2.1149 5 1 7 8 42.76 1.21 2.1146 6 5 3 8 42.78 2.12 2.1140 4 7 1 8 42.98 2.97 2.1044 7 1 5 8 43.20 1.91 2.0942 1 8 0 4 43.32 4.88 2.0885 6 2 6 8 43.94 2.67 2.0606 1 6 6 8 43.97 1.27 2.0592 6 6 0 4 44.07 2.22 2.0547 4 0 8 4 44.19 2.03 2.0496 5 4 6 8 44.34 3.08 2.0431 7 5 1 8 44.36 4.14 2.0421 1 8 2 8 44.51 1.75 2.0355 8 0 4 4 44.79 6.19 2.0236 2 5 7 8 44.82 2.17 2.0222 0 4 8 4 44.94 2.65 2.0170 0 7 5 4 45.11 1.76 2.0097 1 4 8 8 45.39 3.03 1.9979 8 4 0 4 45.43 2.64 1.9963 4 2 8 8 45.45 1.22 1.9957 5 7 1 8 45.51 3.55 1.9933 5 3 7 8 45.54 1.67 1.9918 7 4 4 8 45.72 1.10 1.9844 7 3 5 8 45.86 4.81 1.9787 8 2 4 8 45.98 1.36 1.9738 2 4 8 8 47.15 3.86 1.9275 3 1 9 8 47.22 1.13 1.9247 0 3 9 4 47.36 1.11 1.9194 6 4 6 8 47.39 1.40 1.9184 9 2 2 8 47.70 1.32 1.9066 1 8 4 8 47.72 3.79 1.9059 7 6 0 4 47.77 1.44 1.9039 9 1 3 8 48.19 1.54 1.8883 9 3 1 8 48.61 1.25 1.8729 6 3 7 8 48.62 1.40 1.8728 8 5 1 8 48.63 1.20 1.8721 4 8 2 8 48.85 1.10 1.8644 0 9 1 4 49.34 1.94 1.8471 4 4 8 8 49.45 2.86 1.8431 4 7 5 8 49.71 1.34 1.8341 3 3 9 8 49.74 1.91 1.8331 8 4 4 8 49.90 1.85 1.8276 3 8 4 8 49.91 2.42 1.8274 8 3 5 8 49.94 1.10 1.8263 2 9 1 8 50.31 1.17 1.8137 9 3 3 8 50.66 1.21 1.8018 6 7 3 8 50.69 1.76 1.8008 5 6 6 8 50.85 1.30 1.7955 7 5 5 8 51.07 1.64 1.7884 5 8 2 8 51.18 2.00 1.7849 9 4 2 8 51.30 1.28 1.7808 10 0 2 4 51.58 2.45 1.7719 4 3 9 8 51.75 2.56 1.7666 2 2 10 8 51.86 1.38 1.7631 5 7 5 8 51.92 2.71 1.7612 7 6 4 8 52.00 1.06 1.7585 2 9 3 8 52.25 2.99 1.7509 0 5 9 4 52.45 2.60 1.7446 2 7 7 8 52.52 2.73 1.7424 10 2 2 8 53.11 1.26 1.7245 4 9 1 8 53.54 1.28 1.7116 6 5 7 8 54.75 1.48 1.6767 8 5 5 8 54.96 1.00 1.6706 0 9 5 4 56.24 1.58 1.6357 11 1 1 8 56.32 1.53 1.6335 4 5 9 8 56.96 1.67 1.6167 8 0 8 4 57.09 2.46 1.6133 9 6 2 8 57.61 3.52 1.6001 7 1 9 8 57.85 2.27 1.5940 9 1 7 8 58.09 1.26 1.5878 8 2 8 8 58.91 1.08 1.5677 4 9 5 8 59.20 1.40 1.5607 0 7 9 4 59.85 1.06 1.5454 7 3 9 8 60.01 1.40 1.5416 7 8 4 8 60.08 1.23 1.5399 9 3 7 8 60.40 1.77 1.5327 6 7 7 8 61.15 1.19 1.5155 5 1 11 8 61.45 1.26 1.5089 5 10 2 8 61.52 1.12 1.5074 8 7 5 8 61.59 1.64 1.5058 2 9 7 8 61.85 1.66 1.5001 11 1 5 8 62.75 1.48 1.4808 2 5 11 8 62.98 1.57 1.4758 4 7 9 8 68.14 1.04 1.3761 3 1 13 8 68.88 1.26 1.3631 6 9 7 8 69.04 1.10 1.3603 2 7 11 8 69.97 1.16 1.3445 6 5 11 8 71.30 1.00 1.3226 4 9 9 8 73.72 1.23 1.2852 9 1 11 8 76.82 1.14 1.2408 7 1 13 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.