Kaliborite Burns P C, Hawthorne F C The Canadian Mineralogist 32 (1994) 885-894 Kaliborite: An example of a crystallographically symmetrical hydrogen bond _database_code_amcsd 0005415 CELL PARAMETERS: 18.5720 8.4660 14.6890 90.000 100.020 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 2274.332 Density (g/cm3): 2.092 MAX. ABS. INTENSITY / VOLUME**2: 1.961434355 RIR: 0.305 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.67 3.96 9.1444 2 0 0 2 11.52 4.78 7.6828 1 1 0 4 12.24 100.00 7.2325 0 0 2 2 12.65 11.48 7.0004 -1 1 1 4 13.44 18.10 6.5886 1 1 1 4 14.23 99.91 6.2240 -2 0 2 2 16.21 59.59 5.4694 -1 1 2 4 16.90 3.87 5.2459 2 0 2 2 17.44 17.39 5.0839 1 1 2 4 18.11 2.09 4.8974 -3 1 1 4 19.77 2.59 4.4908 3 1 1 4 20.27 1.36 4.3817 -3 1 2 4 20.99 9.25 4.2330 0 2 0 2 21.10 12.64 4.2096 -4 0 2 2 21.88 1.35 4.0626 0 2 1 4 22.48 8.22 3.9559 1 1 3 4 23.15 72.42 3.8414 2 2 0 4 23.17 5.55 3.8385 3 1 2 4 23.52 93.59 3.7819 -2 2 1 4 23.88 10.39 3.7259 -3 1 3 4 24.36 27.06 3.6533 0 2 2 4 24.62 6.18 3.6162 0 0 4 2 24.85 15.77 3.5828 -2 0 4 2 25.45 53.31 3.5002 -2 2 2 4 26.27 3.70 3.3923 -5 1 1 4 26.46 53.04 3.3681 -1 1 4 4 27.07 5.40 3.2943 2 2 2 4 27.44 17.90 3.2503 -5 1 2 4 27.60 9.32 3.2323 3 1 3 4 28.03 2.22 3.1835 1 1 4 4 28.07 1.91 3.1790 2 0 4 2 28.23 2.63 3.1615 5 1 1 4 28.44 4.83 3.1381 -3 1 4 4 28.63 18.76 3.1176 -2 2 3 4 28.67 74.69 3.1134 -4 2 1 4 28.69 10.65 3.1120 -4 0 4 2 29.76 12.92 3.0020 -6 0 2 2 29.94 3.27 2.9849 -4 2 2 4 30.13 11.98 2.9658 4 2 1 4 30.80 1.08 2.9028 2 2 3 4 31.11 30.20 2.8752 5 1 2 4 32.09 3.44 2.7890 1 3 0 4 32.26 1.89 2.7751 -1 1 5 4 32.39 10.25 2.7642 -4 2 3 4 32.53 11.07 2.7522 -1 3 1 4 32.57 3.63 2.7495 0 2 4 4 32.67 22.39 2.7409 3 1 4 4 32.69 2.85 2.7391 4 2 2 4 32.87 13.14 2.7251 1 3 1 4 33.61 30.64 2.6668 -3 1 5 4 33.90 1.12 2.6444 1 1 5 4 34.15 9.29 2.6257 -1 3 2 4 34.18 12.18 2.6230 4 0 4 2 34.78 3.91 2.5793 1 3 2 4 34.92 9.96 2.5697 5 1 3 4 35.14 1.03 2.5540 -3 3 1 4 35.31 2.42 2.5420 2 2 4 4 35.46 1.06 2.5317 -7 1 1 4 35.81 7.26 2.5073 -4 2 4 4 35.96 4.68 2.4975 -6 2 1 4 35.97 10.65 2.4965 7 1 0 4 36.06 28.32 2.4911 -7 1 2 4 36.20 10.32 2.4811 4 2 3 4 36.32 1.21 2.4736 6 2 0 4 36.35 2.04 2.4716 -3 3 2 4 36.70 7.70 2.4487 -6 2 2 4 37.30 7.71 2.4108 0 0 6 2 37.53 3.37 2.3966 -2 2 5 4 37.57 1.33 2.3943 7 1 1 4 37.66 4.52 2.3885 0 2 5 4 37.66 6.10 2.3885 -5 1 5 4 37.69 7.94 2.3869 1 3 3 4 37.72 4.69 2.3847 -7 1 3 4 37.75 7.03 2.3829 6 2 1 4 38.13 31.53 2.3604 3 3 2 4 38.19 4.48 2.3565 3 1 5 4 38.30 30.04 2.3498 -1 1 6 4 38.49 10.48 2.3391 -6 2 3 4 39.09 9.40 2.3044 -4 0 6 2 39.19 5.29 2.2988 -3 1 6 4 39.42 10.31 2.2861 8 0 0 2 39.43 1.36 2.2853 5 1 4 4 40.12 8.20 2.2474 7 1 2 4 40.18 9.74 2.2444 -5 3 1 4 40.31 4.80 2.2374 -1 3 4 4 40.31 1.40 2.2372 2 0 6 2 40.37 2.47 2.2343 5 3 0 4 40.38 10.86 2.2338 2 2 5 4 40.46 3.65 2.2296 4 2 4 4 41.10 1.24 2.1962 3 3 3 4 41.41 3.75 2.1807 1 3 4 4 41.96 2.55 2.1533 6 0 4 2 42.72 2.86 2.1165 0 4 0 2 42.80 3.48 2.1127 -2 2 6 4 43.18 2.55 2.0949 0 2 6 4 43.20 10.10 2.0942 0 4 1 4 43.41 13.34 2.0846 6 2 3 4 43.55 18.98 2.0783 8 0 2 2 43.63 5.70 2.0747 -6 0 6 2 44.05 5.60 2.0559 3 1 6 4 44.12 3.46 2.0526 -2 4 1 4 44.52 10.84 2.0353 -8 2 1 4 44.57 3.90 2.0331 -1 1 7 4 44.61 17.02 2.0313 0 4 2 4 44.63 1.69 2.0303 2 4 1 4 44.72 7.12 2.0267 -6 2 5 4 44.78 10.60 2.0239 -4 2 6 4 44.89 2.52 2.0194 -8 2 2 4 45.10 12.22 2.0104 -3 1 7 4 45.25 4.93 2.0038 -9 1 1 4 45.29 2.12 2.0023 4 2 5 4 45.39 2.63 1.9981 -5 3 4 4 45.49 4.33 1.9938 -9 1 2 4 45.79 7.37 1.9818 1 3 5 4 45.93 4.09 1.9760 9 1 0 4 46.25 3.64 1.9628 2 4 2 4 46.53 6.50 1.9520 8 2 1 4 46.63 2.39 1.9477 -9 1 3 4 46.88 1.48 1.9380 0 4 3 4 47.01 1.19 1.9330 -7 3 1 4 47.28 2.03 1.9224 -4 4 1 4 47.33 8.10 1.9207 4 4 0 4 47.37 2.72 1.9193 6 2 4 4 47.58 3.95 1.9113 7 1 4 4 47.86 1.33 1.9006 -5 1 7 4 47.90 1.03 1.8991 -7 1 6 4 48.12 11.72 1.8910 -4 4 2 4 48.25 1.43 1.8861 4 4 1 4 48.47 1.47 1.8780 -2 2 7 4 48.63 5.51 1.8724 -9 1 4 4 48.70 7.22 1.8697 7 3 1 4 48.71 1.46 1.8696 2 4 3 4 48.78 4.02 1.8669 -5 3 5 4 48.82 3.89 1.8656 8 2 2 4 48.89 2.35 1.8629 -6 2 6 4 49.06 8.15 1.8570 0 2 7 4 49.21 4.51 1.8516 3 3 5 4 49.22 1.57 1.8513 -10 0 2 2 49.30 4.06 1.8483 -1 3 6 4 49.67 7.28 1.8356 -2 0 8 2 49.80 1.48 1.8309 -4 4 3 4 49.93 1.47 1.8266 0 4 4 4 49.97 1.07 1.8251 5 1 6 4 49.98 1.80 1.8250 -8 0 6 2 50.02 1.75 1.8236 4 4 2 4 50.04 1.65 1.8227 -4 2 7 4 50.83 1.25 1.7963 8 0 4 2 51.29 6.24 1.7813 -3 1 8 4 51.40 1.27 1.7778 -9 1 5 4 51.74 1.57 1.7667 2 2 7 4 52.23 3.17 1.7515 7 1 5 4 52.38 1.69 1.7467 -6 4 1 4 52.82 1.80 1.7332 -5 3 6 4 52.93 4.59 1.7298 -6 4 2 4 52.97 1.84 1.7286 9 1 3 4 53.55 1.27 1.7112 -2 4 5 4 53.63 2.33 1.7090 -6 2 7 4 53.80 2.70 1.7040 10 0 2 2 54.07 1.35 1.6962 -10 2 2 4 54.42 1.22 1.6860 1 5 0 4 54.49 5.58 1.6841 -2 2 8 4 54.49 1.52 1.6839 5 3 5 4 54.57 2.96 1.6818 -1 3 7 4 54.97 1.85 1.6705 -10 2 3 4 55.37 5.03 1.6594 -9 3 2 4 55.46 3.13 1.6569 -4 4 5 4 55.72 1.57 1.6497 -4 2 8 4 55.84 3.71 1.6464 5 1 7 4 56.09 6.01 1.6397 1 3 7 4 56.15 3.33 1.6380 10 2 1 4 56.37 1.94 1.6323 -11 1 3 4 56.40 1.34 1.6314 11 1 0 4 56.40 1.75 1.6314 3 5 0 4 56.47 2.00 1.6296 -3 5 1 4 56.74 1.33 1.6223 9 1 4 4 57.10 1.45 1.6130 9 3 1 4 57.18 1.87 1.6109 7 3 4 4 57.43 3.12 1.6045 -5 3 7 4 57.63 4.50 1.5995 -1 5 3 4 57.68 4.68 1.5983 -2 4 6 4 57.73 5.19 1.5970 -10 0 6 2 57.77 4.62 1.5958 -7 1 8 4 57.98 2.16 1.5905 0 4 6 4 58.03 1.13 1.5895 4 0 8 2 58.38 1.66 1.5807 10 2 2 4 59.37 3.80 1.5567 -8 4 2 4 59.52 1.36 1.5531 8 4 0 4 59.80 1.41 1.5466 -12 0 2 2 60.17 1.20 1.5378 -11 1 5 4 60.18 3.27 1.5375 -1 5 4 4 60.23 2.64 1.5366 5 5 0 4 60.26 1.96 1.5359 -1 3 8 4 60.42 1.22 1.5321 -8 4 3 4 60.48 1.17 1.5307 -3 3 8 4 60.72 1.22 1.5252 8 4 1 4 60.83 1.53 1.5228 -2 2 9 4 61.11 4.63 1.5164 5 5 1 4 61.32 1.36 1.5117 7 3 5 4 61.74 1.56 1.5026 0 2 9 4 61.77 1.11 1.5017 -4 2 9 4 61.81 3.21 1.5010 -12 0 4 2 61.99 4.09 1.4969 9 3 3 4 62.04 1.64 1.4960 -5 5 3 4 62.12 1.92 1.4942 -10 2 6 4 62.41 2.60 1.4880 4 2 8 4 62.65 1.53 1.4829 8 4 2 4 62.73 2.40 1.4812 5 5 2 4 63.12 1.38 1.4729 -11 1 6 4 63.72 1.02 1.4606 -9 3 6 4 64.61 1.44 1.4426 5 3 7 4 64.74 1.15 1.4399 8 2 6 4 65.77 1.07 1.4199 -7 5 2 4 66.01 1.48 1.4153 9 1 6 4 66.04 1.71 1.4148 -10 0 8 2 66.04 1.14 1.4147 -12 2 4 4 66.58 4.25 1.4046 12 2 1 4 66.79 3.38 1.4005 -6 4 7 4 67.25 1.02 1.3922 -1 5 6 4 68.01 1.76 1.3784 5 5 4 4 68.64 1.49 1.3674 -4 4 8 4 68.65 1.63 1.3672 5 1 9 4 68.68 1.73 1.3667 11 3 2 4 68.80 1.10 1.3646 12 2 2 4 69.46 1.79 1.3533 -10 4 4 4 69.48 1.94 1.3528 9 3 5 4 69.72 1.42 1.3488 -4 6 1 4 70.34 3.63 1.3384 3 1 10 4 71.96 1.55 1.3122 -1 1 11 4 73.42 1.17 1.2897 2 6 4 4 73.81 1.10 1.2837 -6 6 1 4 74.02 1.50 1.2807 1 1 11 4 74.42 2.18 1.2748 -10 4 6 4 74.76 1.34 1.2699 -9 5 4 4 74.79 1.20 1.2694 -2 6 5 4 75.40 1.15 1.2606 -6 6 3 4 76.62 3.60 1.2436 5 3 9 4 77.86 1.16 1.2269 -10 4 7 4 78.20 1.03 1.2224 -14 2 5 4 78.77 1.17 1.2150 -11 3 8 4 78.89 1.82 1.2134 11 3 5 4 79.07 1.08 1.2111 -3 1 12 4 79.41 1.55 1.2068 15 1 0 4 79.49 1.01 1.2057 -8 6 1 4 79.63 1.58 1.2039 -6 6 5 4 82.33 1.51 1.1712 8 2 9 4 83.36 1.10 1.1593 5 3 10 4 84.92 1.05 1.1420 2 6 7 4 85.11 1.36 1.1399 9 5 5 4 86.43 1.40 1.1259 15 1 3 4 88.63 1.19 1.1036 4 6 7 4 88.97 1.19 1.1002 -13 1 10 4 89.13 1.24 1.0986 6 2 11 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.