Muscovite Liang J, Hawthorne F C The Canadian Mineralogist 34 (1996) 115-122 Rietveld refinement of micaceous materials: muscovite-2M1, a comparison with single-crystal structure refinement Sample: Rietveld refinement (reflection mode) _database_code_amcsd 0005484 CELL PARAMETERS: 5.1805 8.9940 20.0860 90.000 95.740 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 931.183 Density (g/cm3): 2.770 MAX. ABS. INTENSITY / VOLUME**2: 3.246375402 RIR: 0.382 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.85 100.00 9.9926 0 0 2 2 17.75 31.64 4.9963 0 0 4 2 19.74 3.07 4.4970 0 2 0 2 19.85 39.57 4.4721 1 1 0 4 19.97 97.03 4.4472 -1 1 1 4 20.24 9.49 4.3873 0 2 1 4 20.73 26.70 4.2857 1 1 1 4 21.67 24.38 4.1009 0 2 2 4 22.47 9.06 3.9560 1 1 2 4 22.97 60.49 3.8718 -1 1 3 4 23.87 58.17 3.7273 0 2 3 4 24.92 5.49 3.5724 1 1 3 4 25.55 86.54 3.4860 -1 1 4 4 26.67 67.68 3.3425 0 2 4 4 26.76 77.94 3.3309 0 0 6 2 27.91 83.62 3.1972 1 1 4 4 28.63 10.89 3.1177 -1 1 5 4 29.91 84.17 2.9875 0 2 5 4 31.28 57.55 2.8595 1 1 5 4 32.08 43.44 2.7898 -1 1 6 4 34.61 5.25 2.5915 1 3 0 4 34.68 37.73 2.5867 -1 3 1 4 34.81 18.29 2.5773 2 0 0 2 34.96 10.24 2.5668 1 1 6 4 35.08 57.81 2.5582 -2 0 2 2 35.14 93.34 2.5537 1 3 1 4 35.82 5.63 2.5072 -1 1 7 4 35.95 10.27 2.4982 0 0 8 2 36.24 1.13 2.4784 1 3 2 4 36.57 33.60 2.4573 -1 3 3 4 36.88 16.72 2.4373 2 0 2 2 37.31 4.52 2.4103 0 2 7 4 37.64 11.82 2.3899 -2 0 4 2 37.88 33.55 2.3752 1 3 3 4 40.10 1.40 2.2485 0 4 0 2 40.19 12.07 2.2438 -2 2 1 4 40.33 4.28 2.2361 2 2 0 4 40.37 3.32 2.2344 0 4 1 4 40.52 7.10 2.2262 -1 3 5 4 40.98 2.69 2.2025 2 0 4 2 41.00 10.12 2.2012 2 2 1 4 41.15 7.68 2.1937 0 4 2 4 41.47 10.09 2.1776 -2 2 3 4 42.13 20.48 2.1448 -2 0 6 2 42.17 4.03 2.1428 2 2 2 4 42.43 4.61 2.1304 0 4 3 4 42.52 47.78 2.1262 1 3 5 4 43.14 1.00 2.0971 -1 3 6 4 43.81 6.07 2.0664 2 2 3 4 44.17 11.68 2.0504 0 4 4 4 44.69 3.18 2.0279 -2 2 5 4 45.38 39.85 1.9985 0 0 10 2 45.88 1.77 1.9780 2 2 4 4 46.10 24.24 1.9688 -1 3 7 4 46.67 12.23 1.9463 2 0 6 2 46.93 2.61 1.9359 -2 2 6 4 48.12 2.39 1.8908 -2 0 8 2 48.62 3.51 1.8726 1 3 7 4 48.87 2.39 1.8636 0 4 6 4 49.38 1.88 1.8455 -1 3 8 4 49.94 1.69 1.8263 0 2 10 4 51.75 1.38 1.7665 0 4 7 4 52.50 5.13 1.7430 -2 2 8 4 52.71 1.44 1.7366 -1 1 11 4 52.93 18.33 1.7298 -1 3 9 4 53.58 7.91 1.7103 2 0 8 2 54.01 1.41 1.6977 -2 4 1 4 54.04 2.87 1.6970 -1 5 1 4 54.13 2.39 1.6943 2 4 0 4 54.26 2.34 1.6906 2 2 7 4 54.67 1.03 1.6790 2 4 1 4 54.78 6.29 1.6756 -3 1 3 4 55.04 3.48 1.6685 -2 4 3 4 55.06 1.83 1.6680 3 1 1 4 55.28 18.55 1.6619 -2 0 10 2 55.61 5.79 1.6527 2 4 2 4 55.86 38.65 1.6458 1 3 9 4 56.16 6.83 1.6379 3 1 2 4 56.17 6.28 1.6377 -2 4 4 4 56.34 3.19 1.6329 1 5 3 4 56.67 11.60 1.6244 -1 5 4 4 56.95 1.54 1.6168 2 4 3 4 57.12 11.24 1.6126 -3 1 5 4 57.65 5.16 1.5990 3 1 3 4 57.66 3.88 1.5986 2 2 8 4 57.68 8.01 1.5982 -2 4 5 4 57.92 5.78 1.5921 1 5 4 4 58.86 3.52 1.5689 -3 1 6 4 59.16 1.32 1.5618 0 2 12 4 59.28 3.72 1.5588 -2 2 10 4 59.51 8.49 1.5533 3 1 4 4 59.57 6.13 1.5520 -2 4 6 4 59.87 2.49 1.5449 1 5 5 4 60.35 5.19 1.5336 -1 5 6 4 60.76 2.82 1.5244 2 4 5 4 60.77 18.74 1.5241 -1 3 11 4 61.03 2.87 1.5182 1 1 12 4 61.49 8.33 1.5080 2 0 10 2 61.90 25.05 1.4990 0 6 0 2 62.03 49.67 1.4962 -3 3 1 4 62.09 2.07 1.4948 0 6 1 4 62.16 2.93 1.4932 1 5 6 4 62.67 2.88 1.4824 0 6 2 4 62.67 1.28 1.4824 -3 3 3 4 62.92 2.91 1.4771 3 3 1 4 63.07 1.75 1.4741 -2 2 11 4 63.18 3.63 1.4716 2 4 6 4 63.39 2.71 1.4673 -2 0 12 2 64.01 3.15 1.4547 0 2 13 4 64.05 6.95 1.4537 1 3 11 4 64.79 2.49 1.4389 1 5 7 4 65.26 6.62 1.4297 2 2 10 4 65.37 1.78 1.4275 0 0 14 2 65.94 1.72 1.4165 1 1 13 4 66.12 1.89 1.4132 0 4 11 4 66.18 1.74 1.4121 -3 1 9 4 67.07 2.63 1.3954 -1 1 14 4 67.27 1.69 1.3919 -2 4 9 4 68.42 2.57 1.3711 -3 3 7 4 68.66 1.98 1.3670 0 6 6 4 69.43 4.18 1.3537 2 2 11 4 69.51 29.30 1.3524 -1 3 13 4 70.30 13.26 1.3391 2 0 12 2 70.34 9.27 1.3383 0 4 12 4 71.04 1.48 1.3270 1 1 14 4 71.38 6.38 1.3215 -2 2 13 4 72.21 1.49 1.3083 -1 1 15 4 72.92 1.91 1.2973 -2 6 1 4 73.02 5.97 1.2958 2 6 0 4 73.10 3.68 1.2946 -4 0 2 2 73.14 1.58 1.2940 1 3 13 4 73.18 12.94 1.2933 -2 6 2 4 73.36 8.19 1.2906 -3 3 9 4 73.49 6.51 1.2886 4 0 0 2 73.71 5.50 1.2854 0 6 8 4 74.24 1.32 1.2775 0 2 15 4 74.29 8.10 1.2768 3 3 7 4 74.76 7.46 1.2699 -2 6 4 4 74.81 2.99 1.2691 0 4 13 4 75.30 3.80 1.2621 4 0 2 2 75.90 2.68 1.2536 -2 2 14 4 75.98 1.52 1.2524 2 4 10 4 76.22 3.30 1.2491 0 0 16 2 76.43 4.42 1.2462 -1 7 1 4 76.56 3.19 1.2444 -4 0 6 2 76.59 1.90 1.2441 -4 2 2 4 76.59 1.01 1.2440 -3 5 2 4 76.71 1.84 1.2424 0 6 9 4 76.82 1.05 1.2408 -1 7 2 4 76.94 5.48 1.2392 2 6 4 4 76.97 1.50 1.2388 4 2 0 4 77.06 5.48 1.2376 -3 5 3 4 77.56 1.48 1.2308 -1 7 3 4 78.21 3.86 1.2222 3 5 2 4 78.37 4.27 1.2201 1 7 3 4 78.50 4.51 1.2184 2 2 13 4 78.63 5.90 1.2168 -4 2 5 4 79.03 1.73 1.2116 -3 5 5 4 79.54 1.23 1.2052 0 4 14 4 79.56 3.19 1.2048 -3 3 11 4 79.72 2.69 1.2028 1 7 4 4 80.00 1.43 1.1994 -4 2 6 4 80.01 2.35 1.1992 0 6 10 4 80.03 1.05 1.1990 2 0 14 2 80.16 1.60 1.1974 4 2 3 4 80.54 2.51 1.1927 -3 5 6 4 80.68 1.49 1.1909 -2 2 15 4 80.69 2.37 1.1908 3 3 9 4 81.10 4.86 1.1858 3 5 4 4 81.41 2.28 1.1821 1 7 5 4 81.58 3.62 1.1800 3 1 11 4 81.71 2.08 1.1785 -4 2 7 4 81.78 1.52 1.1777 -2 4 13 4 81.90 1.68 1.1762 4 2 4 4 83.12 1.51 1.1620 -1 1 17 4 83.18 1.66 1.1614 1 3 15 4 83.94 2.75 1.1528 -1 7 7 4 83.98 1.11 1.1523 4 2 5 4 85.47 1.39 1.1360 -4 0 10 2 86.14 3.73 1.1289 -2 4 14 4 86.29 1.78 1.1273 2 6 8 4 87.19 1.55 1.1180 4 4 0 4 87.27 1.14 1.1172 0 8 2 4 87.67 10.39 1.1131 -2 6 10 4 87.88 2.06 1.1110 -1 5 14 4 88.68 1.22 1.1030 2 4 13 4 88.86 5.33 1.1012 4 0 8 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.