Vuonnemite Ercit T S, Cooper M A, Hawthorne F C The Canadian Mineralogist 36 (1998) 1311-1320 The crystal structure of vuonnemite, Na11TiNb2(Si2O7)2(PO4)2O3(F,OH), a phosphate-bearing sorosilicate of the lomonosovite group Locality: Lovozero, Kola Peninsula, Russia _database_code_amcsd 0005582 CELL PARAMETERS: 5.4970 7.1630 14.4370 92.550 95.300 90.610 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 565.404 Density (g/cm3): 3.303 MAX. ABS. INTENSITY / VOLUME**2: 9.300136166 RIR: 0.917 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 6.15 100.00 14.3603 0 0 1 2 12.33 17.92 7.1801 0 0 2 2 12.37 3.84 7.1551 0 1 0 2 13.57 1.87 6.5242 0 -1 1 2 14.08 18.61 6.2905 0 1 1 2 16.20 5.37 5.4729 1 0 0 2 17.09 66.63 5.1881 0 -1 2 2 17.87 33.69 4.9629 1 0 1 2 17.90 32.16 4.9563 0 1 2 2 18.54 5.95 4.7868 0 0 3 2 19.46 10.43 4.5618 -1 0 2 2 20.28 29.29 4.3785 -1 1 0 2 20.58 6.76 4.3163 1 1 0 2 20.88 78.09 4.2535 -1 -1 1 2 20.93 23.95 4.2434 -1 1 1 2 21.31 1.23 4.1698 1 0 2 2 21.49 6.08 4.1350 1 -1 1 2 21.86 3.06 4.0653 0 -1 3 2 22.09 3.38 4.0232 1 1 1 2 22.82 18.44 3.8971 0 1 3 2 22.95 3.12 3.8759 -1 -1 2 2 23.30 14.04 3.8179 -1 1 2 2 23.53 8.82 3.7814 -1 0 3 2 24.30 3.41 3.6635 1 -1 2 2 24.80 30.92 3.5901 0 0 4 2 24.89 4.19 3.5776 0 2 0 2 25.38 6.40 3.5093 0 -2 1 2 25.84 1.68 3.4478 1 0 3 2 25.94 7.17 3.4348 0 2 1 2 26.95 7.87 3.3081 -1 1 3 2 27.28 1.57 3.2692 0 -1 4 2 27.34 3.32 3.2621 0 -2 2 2 28.25 6.31 3.1586 1 -1 3 2 28.32 1.74 3.1516 0 1 4 2 28.38 4.17 3.1453 0 2 2 2 28.44 2.21 3.1386 -1 0 4 2 29.22 3.06 3.0559 1 1 3 2 30.04 3.10 2.9744 1 2 0 2 30.14 11.99 2.9651 -1 -2 1 2 30.21 12.66 2.9583 -1 2 1 2 30.37 22.08 2.9432 1 -2 1 2 30.50 5.64 2.9305 0 -2 3 2 30.75 8.70 2.9081 -1 -1 4 2 31.04 1.05 2.8815 1 0 4 2 31.14 74.13 2.8721 0 0 5 2 31.25 18.69 2.8627 1 2 1 2 31.52 1.55 2.8382 -1 -2 2 2 31.91 9.87 2.8049 0 2 3 2 32.05 1.33 2.7926 -1 2 2 2 32.35 69.94 2.7674 1 -2 2 2 32.73 20.73 2.7364 2 0 0 2 32.74 39.55 2.7352 -2 0 1 2 32.99 8.01 2.7151 1 -1 4 2 33.62 53.10 2.6658 1 2 2 2 33.87 2.56 2.6464 -1 0 5 2 33.96 14.05 2.6400 -2 0 2 2 34.05 24.45 2.6330 -1 -2 3 2 34.05 14.13 2.6327 1 1 4 2 34.97 32.32 2.5659 -1 2 3 2 35.29 1.30 2.5433 2 1 0 2 35.76 9.36 2.5107 -1 -1 5 2 35.95 1.35 2.4980 2 -1 1 2 36.20 2.04 2.4814 2 0 2 2 36.27 12.76 2.4769 -2 0 3 2 36.51 1.37 2.4614 2 1 1 2 36.61 2.16 2.4543 -1 1 5 2 36.66 5.21 2.4511 1 0 5 2 37.52 4.35 2.3970 -1 -2 4 2 37.58 7.02 2.3934 0 0 6 2 37.96 2.42 2.3704 0 -3 1 2 38.27 1.10 2.3520 1 -1 5 2 38.33 1.18 2.3481 -2 -1 3 2 38.76 2.15 2.3234 -1 2 4 2 39.26 4.04 2.2950 0 -3 2 2 39.32 1.66 2.2913 0 -2 5 2 39.42 4.01 2.2859 2 0 3 2 39.51 1.45 2.2809 -2 0 4 2 41.06 1.93 2.1984 -1 3 0 2 41.20 3.18 2.1913 0 2 5 2 41.24 2.89 2.1893 -2 2 0 2 41.24 1.64 2.1888 -1 -1 6 2 41.35 1.20 2.1837 -2 -1 4 2 41.43 2.55 2.1794 -2 2 1 2 41.52 1.86 2.1747 0 -3 3 2 41.59 2.53 2.1716 -1 3 1 2 41.69 2.83 2.1665 -2 -2 1 2 41.86 3.47 2.1581 2 2 0 2 42.04 1.51 2.1494 2 -2 1 2 42.18 3.64 2.1424 -1 1 6 2 42.48 1.46 2.1282 -1 -3 2 2 42.51 9.37 2.1268 -2 -2 2 2 42.61 4.64 2.1217 -2 2 2 2 42.61 2.82 2.1217 1 0 6 2 43.01 1.48 2.1032 2 2 1 2 43.14 1.84 2.0968 0 3 3 2 43.40 10.50 2.0849 2 0 4 2 43.79 7.49 2.0675 2 -2 2 2 43.81 5.28 2.0665 1 -2 5 2 43.95 2.61 2.0603 1 -1 6 2 44.15 4.41 2.0515 0 0 7 2 44.38 2.34 2.0412 -1 -3 3 2 44.64 1.39 2.0298 0 -3 4 2 44.71 1.08 2.0268 -2 2 3 2 45.07 10.09 2.0116 2 2 2 2 45.13 1.44 2.0092 -2 -1 5 2 45.31 2.23 2.0014 1 -3 3 2 45.43 2.97 1.9963 0 -1 7 2 45.69 1.44 1.9858 -2 1 5 2 45.77 2.23 1.9825 -1 0 7 2 45.82 5.18 1.9804 1 2 5 2 46.40 3.37 1.9569 2 -2 3 2 46.61 6.46 1.9486 0 1 7 2 46.67 1.12 1.9461 0 3 4 2 46.88 1.69 1.9380 -2 -2 4 2 47.25 2.48 1.9238 1 3 3 2 47.96 1.28 1.8970 2 2 3 2 48.01 1.71 1.8952 2 0 5 2 48.13 11.50 1.8907 -2 0 6 2 48.45 4.40 1.8788 1 -3 4 2 48.89 6.97 1.8631 1 -2 6 2 49.80 2.50 1.8312 -3 0 1 2 50.25 1.80 1.8158 0 -2 7 2 50.30 1.27 1.8139 2 1 5 2 50.38 2.68 1.8113 -2 3 0 2 50.76 2.36 1.7985 1 3 4 2 50.99 8.81 1.7911 2 -3 1 2 51.05 8.11 1.7890 1 2 6 2 51.06 28.27 1.7888 0 4 0 2 51.18 4.52 1.7849 2 3 0 2 51.51 1.57 1.7741 -3 1 0 2 51.58 6.86 1.7720 -2 -3 2 2 51.64 1.34 1.7701 -3 -1 1 2 51.72 1.82 1.7676 -2 3 2 2 51.85 1.21 1.7632 -1 -2 7 2 52.13 1.55 1.7546 -1 0 8 2 52.20 1.42 1.7522 -3 -1 2 2 52.24 2.20 1.7511 2 3 1 2 52.42 2.55 1.7456 0 2 7 2 52.54 4.72 1.7417 -1 3 5 2 52.95 1.89 1.7294 0 -3 6 2 53.26 1.53 1.7201 -1 -1 8 2 53.26 4.88 1.7199 -2 0 7 2 53.59 2.21 1.7100 -3 -1 3 2 53.66 4.13 1.7081 -3 1 3 2 53.72 2.59 1.7062 -1 2 7 2 53.98 1.45 1.6987 1 -4 1 2 54.20 2.74 1.6923 2 -1 6 2 54.23 2.49 1.6914 3 -1 2 2 54.29 5.61 1.6898 -2 -2 6 2 54.41 5.09 1.6862 1 -2 7 2 54.91 1.24 1.6721 3 1 2 2 55.08 1.26 1.6673 1 4 1 2 55.10 1.66 1.6669 1 -4 2 2 55.34 1.14 1.6600 2 1 6 2 55.56 3.86 1.6541 -2 2 6 2 55.76 1.31 1.6486 -3 -1 4 2 56.22 7.31 1.6361 -3 2 1 2 56.26 4.64 1.6350 -3 2 0 2 56.27 1.95 1.6349 -2 3 4 2 56.28 2.11 1.6346 0 -2 8 2 56.33 2.04 1.6334 -1 -4 3 2 56.41 2.08 1.6311 0 -4 4 2 56.68 8.48 1.6241 -3 -2 1 2 56.72 4.20 1.6230 1 2 7 2 56.73 1.54 1.6228 2 3 3 2 57.00 3.90 1.6155 3 2 0 2 57.09 2.41 1.6133 3 -2 1 2 57.25 1.83 1.6091 -3 0 5 2 57.56 1.22 1.6012 1 1 8 2 57.58 7.13 1.6008 -1 -2 8 2 57.78 5.24 1.5956 0 0 9 2 57.94 4.51 1.5916 0 -3 7 2 58.11 1.23 1.5874 3 2 1 2 58.21 1.10 1.5848 -2 -3 5 2 58.38 1.66 1.5808 -3 -2 3 2 58.50 2.20 1.5777 -3 2 3 2 58.58 4.74 1.5758 0 2 8 2 58.65 1.71 1.5741 -3 -1 5 2 58.69 1.61 1.5731 3 -2 2 2 58.70 3.57 1.5728 2 0 7 2 58.71 1.83 1.5726 0 4 4 2 58.88 3.06 1.5686 3 0 4 2 58.90 1.18 1.5679 -2 -2 7 2 59.61 7.76 1.5511 -1 2 8 2 59.63 5.72 1.5505 0 -4 5 2 59.95 1.25 1.5431 -2 -1 8 2 59.97 1.00 1.5425 3 2 2 2 59.97 1.17 1.5424 0 1 9 2 60.36 1.50 1.5335 -3 -2 4 2 60.76 2.39 1.5243 -3 2 4 2 61.23 1.54 1.5139 2 -3 5 2 61.51 1.75 1.5075 -2 4 0 2 61.80 4.97 1.5013 -2 4 1 2 62.18 3.14 1.4929 -2 -4 1 2 62.40 4.89 1.4882 0 4 5 2 62.45 1.77 1.4872 2 4 0 2 62.66 2.06 1.4826 -2 -4 2 2 62.82 2.99 1.4792 -2 4 2 2 62.91 2.16 1.4773 1 -1 9 2 63.18 1.24 1.4716 2 -4 2 2 63.42 1.17 1.4668 0 -3 8 2 63.58 6.42 1.4634 2 -2 7 2 63.70 1.25 1.4609 -1 -2 9 2 63.82 1.18 1.4585 -1 4 5 2 63.88 1.82 1.4572 -2 -4 3 2 63.97 1.67 1.4554 2 3 5 2 64.03 1.93 1.4541 3 -2 4 2 64.04 1.95 1.4540 -2 -2 8 2 64.70 3.99 1.4408 2 0 8 2 64.94 1.54 1.4360 0 0 10 2 65.11 2.07 1.4327 2 -4 3 2 65.18 1.40 1.4313 2 4 2 2 65.45 2.16 1.4260 2 -3 6 2 65.67 1.13 1.4218 -1 0 10 2 65.72 1.77 1.4208 -2 2 8 2 65.79 2.74 1.4196 3 2 4 2 65.88 2.41 1.4178 -3 -3 3 2 65.88 1.03 1.4178 -1 2 9 2 65.89 1.34 1.4176 0 5 1 2 65.91 5.50 1.4172 2 2 7 2 65.98 1.66 1.4159 0 -5 2 2 66.04 2.29 1.4146 -2 -3 7 2 66.05 1.57 1.4145 1 4 5 2 66.40 1.61 1.4079 -3 -2 6 2 66.52 1.86 1.4057 -1 -1 10 2 67.17 1.67 1.3937 1 -3 8 2 67.31 1.83 1.3911 -3 2 6 2 67.39 1.34 1.3895 -1 5 0 2 67.59 1.70 1.3859 2 4 3 2 67.69 1.05 1.3843 3 -2 5 2 67.72 1.31 1.3837 2 -4 4 2 67.72 1.15 1.3837 -1 1 10 2 67.81 3.55 1.3821 -1 -5 1 2 67.90 1.52 1.3803 -1 5 1 2 68.25 1.77 1.3742 3 -1 6 2 68.25 3.44 1.3742 -4 0 1 2 68.59 1.61 1.3682 4 0 0 2 69.16 2.60 1.3584 1 0 10 2 69.63 6.48 1.3503 4 0 1 2 71.10 1.01 1.3260 -3 -1 8 2 71.47 3.41 1.3200 -4 0 4 2 71.61 1.39 1.3178 -1 -5 4 2 71.69 1.76 1.3165 -2 -4 6 2 72.42 1.23 1.3050 1 -5 4 2 73.87 4.33 1.2830 -2 4 6 2 75.48 1.41 1.2596 1 5 4 2 76.16 1.00 1.2499 -2 -3 9 2 78.21 1.05 1.2222 -2 4 7 2 78.48 2.48 1.2187 0 -4 9 2 79.98 1.26 1.1996 -1 3 10 2 80.52 3.07 1.1929 4 0 5 2 80.55 1.16 1.1925 1 -2 11 2 81.31 1.37 1.1833 -4 -3 2 2 82.22 1.36 1.1725 -3 -1 10 2 82.29 1.11 1.1716 0 1 12 2 82.90 1.01 1.1646 0 4 9 2 83.45 1.36 1.1583 1 2 11 2 83.46 2.30 1.1582 1 -6 2 2 83.62 1.89 1.1564 2 4 7 2 84.26 1.45 1.1493 3 0 9 2 84.44 1.44 1.1473 2 -4 8 2 84.57 1.47 1.1458 -1 -6 3 2 84.83 1.27 1.1429 4 0 6 2 85.06 1.85 1.1405 -4 0 8 2 85.54 1.70 1.1353 1 6 2 2 86.13 1.91 1.1290 -1 6 3 2 86.67 1.18 1.1233 -4 1 8 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.