Jamesite Cooper M A, Hawthorne F C The Canadian Mineralogist 37 (1999) 53-60 Local Pb-_ disorder in the crystal structure of jamesite, Pb2ZnFe2(Fe2.8Zn1.2)(AsO4)4(OH)8[(OH)1.2O.8], and revision of the chemical formula _database_code_amcsd 0005590 CELL PARAMETERS: 5.5830 9.5420 10.2190 109.810 90.570 97.710 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 506.653 Density (g/cm3): 6.411 MAX. ABS. INTENSITY / VOLUME**2: 108.6710313 RIR: 5.519 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.21 100.00 9.5973 0 0 1 2 9.96 1.43 8.8809 0 1 0 2 11.01 21.50 8.0376 0 -1 1 2 15.75 8.35 5.6261 0 1 1 2 16.05 15.39 5.5227 1 0 0 2 17.63 19.46 5.0313 -1 1 0 2 17.74 16.21 5.0005 0 -1 2 2 18.05 14.44 4.9147 -1 0 1 2 18.92 40.20 4.6902 0 -2 1 2 19.01 21.57 4.6683 1 0 1 2 20.00 12.44 4.4404 0 2 0 2 20.14 7.54 4.4097 1 1 0 2 20.25 20.94 4.3860 -1 -1 1 2 21.06 10.00 4.2192 -1 1 1 2 23.29 20.99 3.8190 1 -2 1 2 23.76 3.54 3.7449 1 -1 2 2 23.81 5.93 3.7377 -1 2 0 2 23.83 1.14 3.7338 -1 0 2 2 23.91 29.66 3.7211 0 1 2 2 23.97 2.63 3.7118 1 1 1 2 24.25 19.07 3.6698 -1 -1 2 2 24.82 18.52 3.5878 0 2 1 2 25.30 16.89 3.5202 1 0 2 2 26.17 10.69 3.4056 0 -1 3 2 26.33 44.39 3.3852 1 -2 2 2 26.43 3.09 3.3724 -1 -2 1 2 27.43 15.28 3.2520 -1 1 2 2 27.55 40.49 3.2372 1 2 0 2 27.68 1.55 3.2223 -1 2 1 2 28.23 1.18 3.1609 0 -2 3 2 28.53 4.04 3.1290 -1 -2 2 2 29.52 20.46 3.0262 0 -3 2 2 30.19 1.09 2.9603 0 3 0 2 30.37 6.76 2.9430 1 1 2 2 30.74 21.16 2.9082 -1 -1 3 2 30.95 15.43 2.8895 1 -1 3 2 31.47 12.62 2.8424 -1 0 3 2 31.59 15.43 2.8325 1 2 1 2 31.98 7.11 2.7986 1 -2 3 2 32.10 7.35 2.7887 1 -3 2 2 32.15 10.62 2.7841 -1 3 0 2 32.52 20.50 2.7534 -2 1 0 2 32.85 26.17 2.7261 0 1 3 2 33.19 3.11 2.6995 1 0 3 2 33.22 2.12 2.6966 -2 0 1 2 33.29 2.54 2.6913 -1 -2 3 2 33.45 10.41 2.6792 0 -3 3 2 34.30 12.92 2.6142 -2 1 1 2 34.32 3.24 2.6128 2 0 1 2 34.64 1.39 2.5894 0 3 1 2 34.65 1.04 2.5887 -1 -3 1 2 35.23 4.28 2.5477 -2 -1 1 2 35.24 2.86 2.5469 0 -1 4 2 35.30 2.52 2.5428 -1 1 3 2 35.38 1.59 2.5369 -1 -3 2 2 35.42 4.16 2.5339 2 1 0 2 35.60 8.11 2.5218 2 -2 1 2 35.92 2.38 2.5002 0 -2 4 2 36.13 21.50 2.4861 -1 3 1 2 36.47 3.23 2.4635 1 3 0 2 37.53 2.41 2.3967 -2 -1 2 2 37.98 2.45 2.3690 2 -2 2 2 38.09 2.61 2.3626 2 1 1 2 38.19 1.36 2.3568 1 1 3 2 38.24 2.01 2.3537 -2 2 1 2 38.35 4.12 2.3473 0 -4 1 2 38.38 4.87 2.3451 0 -4 2 2 38.54 2.03 2.3360 -1 -3 3 2 38.57 11.86 2.3342 2 0 2 2 39.27 5.59 2.2944 1 -1 4 2 39.39 2.12 2.2873 0 -3 4 2 39.56 3.73 2.2782 1 -4 1 2 39.83 3.21 2.2630 1 -4 2 2 39.88 2.11 2.2605 -1 -2 4 2 40.07 3.05 2.2500 -1 0 4 2 40.40 4.52 2.2324 2 -3 1 2 40.64 5.64 2.2202 0 4 0 2 40.95 6.83 2.2039 0 3 2 2 41.16 3.54 2.1930 -2 -2 2 2 41.47 1.83 2.1775 -1 2 3 2 41.56 1.71 2.1729 -1 4 0 2 41.89 2.79 2.1566 1 -3 4 2 41.93 1.30 2.1547 -2 0 3 2 42.02 1.27 2.1502 -1 3 2 2 42.26 1.21 2.1387 0 1 4 2 42.35 3.71 2.1341 1 -4 3 2 42.48 4.42 2.1279 2 -2 3 2 42.87 3.11 2.1096 -2 2 2 2 43.68 3.45 2.0724 -1 -3 4 2 44.38 3.03 2.0411 -2 3 1 2 44.53 6.37 2.0346 0 -2 5 2 44.54 1.09 2.0344 -2 -2 3 2 44.60 3.34 2.0315 2 0 3 2 44.96 1.77 2.0164 0 4 1 2 45.12 1.24 2.0094 0 -4 4 2 46.25 1.87 1.9631 1 4 0 2 46.73 1.22 1.9437 0 -3 5 2 46.89 3.97 1.9377 1 1 4 2 46.96 1.62 1.9348 -2 -3 2 2 47.36 2.56 1.9195 0 0 5 2 47.62 5.60 1.9095 2 -4 2 2 48.13 2.13 1.8904 0 -5 2 2 48.24 1.45 1.8864 2 3 0 2 48.32 5.14 1.8836 1 -1 5 2 48.55 2.73 1.8754 0 3 3 2 48.78 1.64 1.8669 -2 0 4 2 48.96 2.17 1.8605 0 2 4 2 49.09 1.87 1.8559 2 2 2 2 49.11 2.93 1.8550 -2 2 3 2 49.13 1.01 1.8544 1 -3 5 2 49.26 1.34 1.8497 -2 3 2 2 49.33 1.65 1.8474 -1 0 5 2 49.54 1.04 1.8401 -1 -4 4 2 50.02 2.33 1.8234 -1 2 4 2 50.27 1.05 1.8151 1 -5 3 2 50.35 1.75 1.8123 2 -3 4 2 51.11 1.56 1.7870 0 -4 5 2 51.31 2.28 1.7805 1 0 5 2 51.71 1.78 1.7679 -1 5 0 2 51.86 2.34 1.7631 -3 -1 1 2 52.20 1.67 1.7524 3 1 0 2 52.63 2.07 1.7391 3 -1 2 2 53.25 2.60 1.7202 -1 -5 2 2 53.43 1.29 1.7150 -1 1 5 2 53.55 2.04 1.7112 1 -5 4 2 53.57 6.72 1.7106 1 3 3 2 53.84 2.70 1.7028 0 -2 6 2 54.18 4.14 1.6928 3 -3 1 2 54.19 2.41 1.6926 2 -4 4 2 54.24 1.49 1.6910 -1 -5 3 2 54.98 2.65 1.6700 -1 -4 5 2 55.13 2.29 1.6659 2 -5 2 2 55.40 3.05 1.6585 2 -5 1 2 55.44 2.49 1.6573 3 -3 2 2 55.47 1.06 1.6564 -2 -1 5 2 55.54 1.62 1.6547 2 2 3 2 55.78 3.46 1.6482 0 5 1 2 55.87 1.23 1.6456 -2 -4 3 2 56.11 1.30 1.6391 -3 2 2 2 56.14 1.28 1.6382 -3 0 3 2 56.29 1.03 1.6344 1 1 5 2 56.43 1.07 1.6305 -1 -2 6 2 56.60 2.47 1.6260 -2 2 4 2 56.71 1.93 1.6231 3 -2 3 2 56.72 1.99 1.6230 2 1 4 2 56.76 1.09 1.6219 -2 0 5 2 56.89 2.46 1.6186 2 4 0 2 56.95 2.54 1.6169 2 -3 5 2 57.19 1.47 1.6107 2 -1 5 2 57.42 1.04 1.6048 1 -3 6 2 57.69 1.83 1.5981 -3 1 3 2 58.32 2.29 1.5822 -1 4 3 2 58.46 3.35 1.5788 1 -5 5 2 58.74 2.35 1.5719 1 -6 2 2 59.17 1.16 1.5614 -1 0 6 2 59.35 1.41 1.5573 -1 2 5 2 59.81 1.42 1.5463 1 -6 1 2 59.87 1.52 1.5448 2 -5 4 2 61.28 1.52 1.5126 1 0 6 2 61.47 1.32 1.5085 -1 5 2 2 61.99 1.19 1.4971 3 -2 4 2 63.26 2.41 1.4700 -3 4 1 2 63.45 1.19 1.4661 -1 1 6 2 63.86 1.13 1.4576 3 2 2 2 64.50 1.06 1.4447 2 -2 6 2 64.80 1.77 1.4388 2 -6 1 2 65.31 1.76 1.4287 2 1 5 2 66.47 1.75 1.4066 -1 4 4 2 66.64 1.01 1.4034 2 5 0 2 67.93 1.26 1.3799 4 -1 1 2 68.57 1.01 1.3686 1 -4 7 2 68.89 1.46 1.3630 0 2 6 2 71.12 1.21 1.3257 1 -7 1 2 71.24 1.34 1.3236 -2 6 1 2 76.66 1.11 1.2430 -2 6 2 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.