Sidpietersite Cooper M A, Hawthorne F C The Canadian Mineralogist 37 (1999) 1275-1282 The structure topology of sidpietersite, Pb4(SO3S)O2(OH)2, a novel thiosulfate structure _database_code_amcsd 0005630 CELL PARAMETERS: 7.4550 6.4960 11.2070 114.330 89.650 88.690 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 494.327 Density (g/cm3): 6.751 MAX. ABS. INTENSITY / VOLUME**2: 95.43486225 RIR: 4.603 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.66 100.00 10.2102 0 0 1 2 13.86 20.81 6.3876 0 -1 1 2 14.97 52.17 5.9168 0 1 0 2 17.66 20.17 5.0227 0 -1 2 2 18.47 5.61 4.8039 1 -1 1 2 18.89 1.69 4.6979 1 1 0 2 20.21 22.68 4.3935 0 1 1 2 20.92 1.27 4.2455 1 0 2 2 21.40 4.82 4.1518 1 -1 2 2 24.20 8.89 3.6772 0 -1 3 2 25.31 23.12 3.5196 2 0 1 2 25.59 17.20 3.4811 -2 0 1 2 26.18 88.19 3.4034 0 0 3 2 27.03 1.27 3.2991 1 -1 3 2 27.38 3.37 3.2576 0 1 2 2 27.94 71.58 3.1938 0 -2 2 2 27.94 44.63 3.1933 2 1 0 2 28.67 57.76 3.1140 -2 1 0 2 29.44 1.70 3.0344 2 0 2 2 29.76 18.59 3.0024 -2 -1 2 2 29.93 4.38 2.9855 -2 0 2 2 29.96 8.53 2.9827 2 -1 2 2 30.21 14.81 2.9584 0 2 0 2 30.23 2.36 2.9564 -1 -2 2 2 30.81 19.10 2.9025 0 -2 3 2 31.03 48.61 2.8818 2 1 1 2 31.93 32.72 2.8032 -2 1 1 2 31.95 18.11 2.8011 0 -1 4 2 32.24 1.08 2.7763 1 2 0 2 33.27 1.42 2.6929 1 -2 3 2 34.24 43.07 2.6187 2 -1 3 2 34.28 39.52 2.6158 -2 -1 3 2 34.88 38.22 2.5722 0 2 1 2 35.16 12.14 2.5525 0 0 4 2 35.44 5.68 2.5331 0 1 3 2 36.04 1.47 2.4918 -2 0 3 2 36.43 4.47 2.4661 -2 -2 1 2 36.70 1.21 2.4485 -2 -2 2 2 37.03 1.85 2.4275 1 0 4 2 37.38 1.02 2.4060 2 -2 1 2 37.44 3.82 2.4020 2 -2 2 2 38.32 7.89 2.3490 2 2 0 2 39.10 13.99 2.3041 -2 -2 3 2 39.42 8.24 2.2861 -2 2 0 2 39.60 9.78 2.2757 2 -2 3 2 40.35 1.65 2.2353 0 -1 5 2 41.74 1.57 2.1639 0 -3 2 2 42.15 14.34 2.1438 0 -2 5 2 42.45 6.89 2.1292 0 -3 3 2 42.59 11.24 2.1227 2 0 4 2 42.66 7.05 2.1192 2 1 3 2 42.97 3.19 2.1048 0 -3 1 2 43.31 10.12 2.0893 -2 0 4 2 43.60 1.57 2.0759 2 -2 4 2 43.70 11.22 2.0713 -2 1 3 2 43.97 1.50 2.0594 3 -1 3 2 44.05 5.56 2.0557 0 1 4 2 46.76 1.14 1.9426 3 -2 2 2 47.45 4.67 1.9160 2 2 2 2 47.61 1.13 1.9100 -2 -1 5 2 48.13 15.64 1.8905 -2 -3 2 2 48.71 2.86 1.8696 -2 2 2 2 48.89 20.01 1.8630 4 0 0 2 49.15 5.15 1.8535 -2 -3 1 2 49.18 14.40 1.8525 2 -3 2 2 49.58 7.44 1.8386 0 -2 6 2 49.59 4.16 1.8383 4 0 1 2 49.73 1.59 1.8334 2 -3 3 2 50.18 13.69 1.8180 2 1 4 2 50.35 2.54 1.8124 2 -3 1 2 50.63 1.10 1.8030 0 3 1 2 50.98 3.23 1.7913 4 1 0 2 51.16 1.93 1.7855 1 -2 6 2 51.26 11.20 1.7824 -2 1 4 2 51.35 1.73 1.7792 4 -1 1 2 52.25 1.05 1.7506 -4 -1 2 2 52.51 1.02 1.7428 4 -1 2 2 52.84 1.17 1.7327 4 1 1 2 53.14 3.56 1.7236 0 1 5 2 53.88 3.74 1.7017 0 0 6 2 54.00 2.06 1.6982 -4 1 1 2 54.83 6.08 1.6742 0 -3 6 2 55.20 9.09 1.6641 -2 -3 5 2 55.20 8.28 1.6639 2 -1 6 2 55.30 2.18 1.6611 -4 -1 3 2 55.67 9.36 1.6509 -2 -1 6 2 55.71 7.24 1.6500 2 -3 5 2 55.73 2.26 1.6495 2 -2 6 2 55.78 3.89 1.6481 -2 -2 6 2 55.85 6.20 1.6460 4 0 3 2 56.03 7.75 1.6414 2 3 1 2 56.50 9.10 1.6288 0 2 4 2 56.53 3.05 1.6279 0 3 2 2 56.72 9.41 1.6230 -4 -2 2 2 56.73 9.89 1.6226 -4 0 3 2 57.25 5.32 1.6091 0 -4 2 2 57.41 8.58 1.6051 -2 3 1 2 57.73 2.82 1.5969 0 -4 4 2 57.78 5.24 1.5958 4 -2 2 2 58.53 1.70 1.5770 -4 -2 3 2 58.61 4.54 1.5751 0 -1 7 2 59.28 3.78 1.5588 4 -2 3 2 59.32 5.52 1.5579 0 -4 1 2 59.36 2.79 1.5570 -4 2 0 2 59.43 2.73 1.5552 4 -1 4 2 59.77 1.42 1.5473 -4 -1 4 2 60.25 4.55 1.5359 0 -4 5 2 60.53 7.11 1.5297 4 2 1 2 60.81 1.01 1.5232 2 -3 6 2 61.08 3.63 1.5172 4 0 4 2 61.51 3.93 1.5076 2 3 2 2 62.28 2.24 1.4908 -2 -4 2 2 62.37 5.05 1.4888 -4 2 1 2 62.95 2.15 1.4764 -2 3 2 2 63.36 2.20 1.4680 2 -2 7 2 63.54 1.45 1.4642 -2 -2 7 2 63.55 1.30 1.4640 2 -4 2 2 63.81 2.28 1.4586 0 0 7 2 65.34 2.11 1.4281 -2 -4 5 2 65.99 1.07 1.4157 -4 -3 3 2 66.18 1.14 1.4120 2 -4 5 2 66.41 4.00 1.4078 -4 -2 5 2 66.58 1.51 1.4046 4 -2 5 2 67.44 1.66 1.3888 4 -3 3 2 67.64 1.48 1.3851 0 4 1 2 68.71 2.06 1.3662 2 0 7 2 68.79 1.74 1.3646 -4 1 4 2 69.62 2.56 1.3504 -2 0 7 2 69.96 1.89 1.3447 2 2 5 2 71.34 1.68 1.3221 -2 2 5 2 72.14 2.64 1.3094 4 -2 6 2 72.23 1.38 1.3079 -4 -2 6 2 73.66 3.57 1.2861 0 4 2 2 74.09 1.41 1.2796 4 1 5 2 74.24 1.25 1.2775 0 -5 5 2 74.40 1.92 1.2751 -2 -3 8 2 74.46 1.13 1.2742 2 -3 8 2 75.75 1.66 1.2557 0 -4 8 2 75.82 1.13 1.2547 2 3 4 2 76.19 1.76 1.2495 -4 -3 6 2 76.45 1.76 1.2459 -4 0 6 2 76.55 1.79 1.2446 0 -2 9 2 76.70 2.73 1.2425 4 2 4 2 76.81 1.44 1.2410 4 -3 6 2 77.37 2.15 1.2334 2 1 7 2 77.38 1.85 1.2332 -2 3 4 2 77.39 2.38 1.2331 -2 -5 4 2 77.40 1.10 1.2331 -4 -4 2 2 77.94 1.63 1.2257 0 -3 9 2 78.06 1.60 1.2242 -4 -4 4 2 78.20 1.10 1.2224 6 1 0 2 78.60 1.92 1.2172 -2 1 7 2 78.65 1.73 1.2165 2 -5 4 2 79.07 2.62 1.2111 -4 -4 1 2 79.11 2.74 1.2106 -4 2 4 2 79.20 1.29 1.2094 4 -1 7 2 79.25 2.77 1.2088 -6 1 0 2 79.34 1.64 1.2076 -6 -1 2 2 79.63 2.71 1.2040 6 1 1 2 79.71 1.96 1.2030 4 -4 2 2 80.24 1.34 1.1964 -4 -1 7 2 80.38 1.33 1.1946 -4 -4 5 2 81.42 2.51 1.1820 -2 -5 1 2 81.61 1.29 1.1797 4 -4 1 2 81.83 2.39 1.1771 6 -1 3 2 81.90 1.55 1.1763 -6 -1 3 2 81.93 1.52 1.1758 4 -4 5 2 83.03 2.15 1.1631 2 -5 1 2 83.47 1.13 1.1581 4 0 7 2 83.88 1.37 1.1534 0 1 8 2 84.47 1.35 1.1469 -2 -1 9 2 84.56 1.59 1.1459 2 3 5 2 85.28 1.04 1.1380 -2 -5 7 2 85.50 1.45 1.1357 0 2 7 2 85.97 1.07 1.1307 0 -5 8 2 86.21 1.04 1.1282 -2 3 5 2 88.53 1.39 1.1045 -6 1 3 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.