Cu1.6Pb1.6Bi6.4S12 Topa D, Balic-Zunic T, Makovicky E The Canadian Mineralogist 38 (2000) 611-616 The crystal structure of Cu1.6Pb1.6Bi6.4S12, a new 44.8 Angstrom derivative of the bismuthinite-aikinite solid-solution series _database_code_amcsd 0005646 CELL PARAMETERS: 4.0074 44.8100 11.5130 90.000 90.000 90.000 SPACE GROUP: Pmc2_1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 2067.408 Density (g/cm3): 6.891 MAX. ABS. INTENSITY / VOLUME**2: 75.65648314 RIR: 3.575 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 1.97 3.12 44.8100 0 1 0 2 11.02 3.05 8.0289 0 4 1 2 15.39 16.68 5.7565 0 0 2 1 15.82 3.16 5.6013 0 8 0 2 16.50 1.62 5.3714 0 3 2 2 17.32 20.14 5.1201 0 4 2 2 21.82 3.46 4.0736 0 11 0 2 22.14 57.25 4.0144 0 8 2 2 23.16 3.91 3.8403 0 11 1 2 23.58 28.92 3.7732 1 4 0 4 23.63 1.50 3.7658 0 9 2 2 23.94 3.23 3.7169 0 3 3 2 24.52 100.00 3.6305 0 4 3 2 24.83 55.19 3.5856 1 4 1 4 25.07 85.70 3.5520 0 12 1 2 25.24 1.38 3.5278 0 5 3 2 25.85 3.96 3.4469 0 13 0 2 27.09 1.65 3.2915 0 7 3 2 27.11 18.82 3.2889 1 0 2 2 27.19 3.09 3.2801 1 1 2 4 27.77 1.43 3.2120 1 3 2 4 28.19 8.59 3.1659 0 8 3 2 28.28 56.94 3.1557 1 4 2 4 28.46 92.83 3.1359 1 8 1 4 28.49 7.15 3.1328 0 12 2 2 28.92 2.20 3.0876 1 5 2 4 29.38 1.73 3.0395 0 9 3 2 29.65 2.33 3.0130 1 9 1 4 31.07 3.69 2.8782 0 0 4 1 31.55 93.28 2.8361 1 8 2 4 31.96 3.59 2.8006 0 16 0 2 32.11 1.02 2.7877 0 4 4 2 32.78 21.11 2.7319 1 12 0 4 32.91 3.41 2.7213 0 16 1 2 33.48 1.36 2.6763 0 12 3 2 33.72 36.61 2.6581 1 12 1 4 34.16 2.90 2.6251 0 7 4 2 35.05 42.87 2.5600 0 8 4 2 35.07 1.03 2.5590 1 11 2 4 35.65 15.59 2.5184 0 16 2 2 36.04 1.97 2.4918 0 9 4 2 36.16 21.38 2.4842 1 8 3 4 36.40 1.63 2.4681 1 12 2 4 38.51 23.75 2.3378 1 0 4 2 38.56 3.98 2.3346 1 1 4 4 39.37 30.16 2.2885 1 4 4 4 39.53 2.90 2.2797 0 12 4 2 39.85 3.14 2.2623 0 16 3 2 40.05 21.50 2.2513 1 16 1 4 40.53 6.03 2.2256 1 12 3 4 40.81 4.11 2.2113 1 15 2 4 41.04 3.46 2.1992 0 20 1 2 41.56 2.03 2.1727 0 17 3 2 41.76 1.90 2.1630 1 17 1 4 41.87 9.26 2.1574 1 8 4 4 42.39 14.97 2.1323 1 16 2 4 42.44 7.91 2.1297 0 8 5 2 43.34 4.30 2.0879 0 20 2 2 43.67 1.04 2.0727 0 15 4 2 44.03 1.19 2.0568 1 17 2 4 44.60 1.41 2.0318 1 15 3 4 45.17 3.49 2.0072 0 16 4 2 45.26 36.97 2.0037 2 0 0 2 45.79 1.20 1.9815 1 12 4 4 46.07 36.32 1.9700 1 16 3 4 46.19 7.97 1.9655 1 4 5 4 46.32 10.47 1.9599 0 12 5 2 46.43 16.08 1.9556 1 20 0 4 46.61 1.14 1.9487 1 5 5 4 46.96 22.06 1.9349 0 20 3 2 47.14 3.11 1.9280 1 20 1 4 47.38 9.79 1.9188 0 0 6 1 47.42 1.42 1.9171 0 1 6 2 47.61 1.12 1.9101 1 17 3 4 47.72 1.13 1.9059 1 7 5 4 48.08 1.66 1.8923 2 0 2 2 48.11 1.19 1.8913 0 4 6 2 48.40 8.79 1.8806 1 8 5 4 48.77 7.87 1.8671 0 24 0 2 48.81 2.09 1.8659 2 4 2 4 49.21 1.61 1.8517 1 20 2 4 49.45 1.27 1.8430 0 24 1 2 50.00 1.28 1.8242 0 19 4 2 50.26 1.16 1.8153 0 8 6 2 50.83 1.66 1.7962 1 19 3 4 50.88 1.23 1.7947 1 16 4 4 50.94 10.06 1.7928 2 8 2 4 50.94 1.74 1.7928 1 11 5 4 51.02 1.80 1.7901 1 21 2 4 51.45 2.42 1.7760 0 24 2 2 51.61 1.14 1.7711 0 25 1 2 51.70 1.26 1.7680 0 20 4 2 51.94 11.28 1.7606 1 12 5 4 52.14 20.24 1.7543 2 4 3 4 52.21 1.28 1.7522 1 23 0 4 52.43 18.82 1.7452 2 12 1 4 52.52 3.59 1.7424 1 20 3 4 52.90 10.34 1.7307 1 0 6 2 53.58 4.49 1.7104 1 4 6 4 53.71 1.97 1.7067 0 12 6 2 54.17 1.90 1.6931 2 8 3 4 54.35 1.72 1.6880 2 12 2 4 54.83 3.09 1.6744 1 24 1 4 55.58 1.77 1.6535 1 8 6 4 55.91 1.14 1.6445 2 0 4 2 55.98 1.25 1.6427 0 27 1 2 56.47 1.04 1.6296 2 16 0 4 56.62 3.93 1.6257 1 16 5 4 56.84 1.29 1.6199 1 25 1 4 57.08 1.20 1.6135 2 16 1 4 58.49 1.04 1.5781 0 8 7 2 58.50 14.61 1.5779 2 8 4 4 58.81 1.86 1.5702 1 12 6 4 58.90 5.32 1.5680 2 16 2 4 58.97 2.69 1.5664 0 24 4 2 60.00 3.44 1.5419 0 28 2 2 61.23 1.68 1.5137 1 3 7 4 61.50 5.98 1.5077 1 4 7 4 61.62 5.48 1.5052 0 12 7 2 61.63 1.18 1.5050 2 12 4 4 61.85 1.03 1.5001 1 5 7 4 61.86 1.35 1.5000 2 16 3 4 62.73 1.61 1.4811 2 20 1 4 63.07 1.76 1.4740 1 28 1 4 63.34 3.26 1.4683 1 8 7 4 63.78 3.61 1.4593 2 8 5 4 63.80 3.77 1.4589 1 24 4 4 63.87 1.79 1.4574 0 20 6 2 64.22 1.18 1.4502 0 24 5 2 64.45 1.93 1.4457 2 20 2 4 64.79 6.99 1.4390 1 28 2 4 65.38 1.43 1.4274 0 4 8 2 65.56 1.73 1.4239 1 27 3 4 65.85 2.44 1.4182 0 16 7 2 65.86 1.73 1.4181 2 16 4 4 66.76 5.37 1.4011 2 12 5 4 66.81 1.04 1.4003 0 32 0 2 66.90 1.19 1.3985 1 29 2 4 67.27 11.29 1.3919 2 20 3 4 67.60 5.14 1.3859 2 0 6 2 68.51 4.01 1.3696 1 20 6 4 68.72 4.28 1.3660 2 24 0 4 69.03 1.22 1.3606 0 32 2 2 70.35 2.24 1.3381 0 24 6 2 70.62 1.27 1.3338 1 25 5 4 70.91 1.49 1.3291 2 24 2 4 71.43 9.20 1.3206 1 28 4 4 71.61 1.68 1.3177 3 4 1 4 71.69 3.04 1.3165 1 8 8 4 71.89 2.26 1.3133 1 32 1 4 72.79 1.23 1.2993 2 12 6 4 73.14 1.19 1.2939 1 23 6 4 73.23 2.44 1.2925 3 4 2 4 73.32 3.77 1.2912 3 8 1 4 74.68 1.51 1.2710 0 4 9 2 74.92 4.21 1.2675 3 8 2 4 75.53 3.54 1.2587 1 20 7 4 75.60 1.07 1.2577 3 12 0 4 76.13 1.81 1.2503 3 12 1 4 77.07 1.18 1.2375 0 36 1 2 77.32 1.92 1.2341 2 24 4 4 77.36 1.10 1.2336 1 15 8 4 77.57 1.40 1.2307 3 8 3 4 78.23 2.43 1.2220 2 28 2 4 78.43 1.68 1.2193 1 16 8 4 79.02 1.66 1.2117 3 0 4 2 79.58 2.38 1.2046 3 4 4 4 79.67 4.04 1.2035 2 12 7 4 80.02 1.75 1.1991 3 16 1 4 80.86 1.94 1.1887 1 36 0 4 81.58 1.21 1.1801 3 16 2 4 81.63 1.58 1.1795 1 24 7 4 81.70 1.37 1.1786 2 20 6 4 82.99 1.43 1.1636 0 16 9 2 83.08 1.12 1.1626 2 4 8 4 83.38 1.30 1.1591 1 20 8 4 83.43 1.21 1.1585 1 12 9 4 83.51 1.98 1.1576 2 16 7 4 84.17 3.85 1.1502 3 16 3 4 84.43 1.68 1.1474 3 20 0 4 85.88 1.02 1.1316 3 8 5 4 86.45 1.03 1.1256 2 32 2 4 87.24 1.20 1.1174 1 16 9 4 87.70 1.94 1.1128 2 24 6 4 88.32 1.62 1.1065 1 0 10 2 88.60 1.45 1.1038 3 12 5 4 89.37 1.47 1.0963 3 0 6 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.