data_global
_amcsd_formula_title 'Pb2(H2O)[(UO2)10UO12(OH)6(H2O)2]'
loop_
_publ_author_name
'Li Y'
'Burns P C'
_journal_name_full 'The Canadian Mineralogist'
_journal_volume 38 
_journal_year 2000
_journal_page_first 1433
_journal_page_last 1441
_publ_section_title
;
 Synthesis and crystal structure of a new Pb uranyl oxide hydrate
 with a framework structure that contains channels
;
_database_code_amcsd 0005702
_chemical_formula_sum 'U11 Pb2 O41 H12'
_cell_length_a 13.281
_cell_length_b 10.223
_cell_length_c 26.10
_cell_angle_alpha 90
_cell_angle_beta 103.202
_cell_angle_gamma 90
_cell_volume 3449.985
_exptl_crystal_density_diffrn      7.125
_symmetry_space_group_name_H-M 'C 1 2/c 1'
loop_
_space_group_symop_operation_xyz
  'x,y,z'
  '1/2+x,1/2+y,z'
  'x,-y,1/2+z'
  '1/2+x,1/2-y,1/2+z'
  '-x,y,1/2-z'
  '1/2-x,1/2+y,1/2-z'
  '-x,-y,-z'
  '1/2-x,1/2-y,-z'
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_U_iso_or_equiv
U(1)   0.23500   0.42220   0.47260   1.00000   0.00840
U(2)   0.00000   0.63900   0.25000   1.00000   0.00720
U(3)   0.50910   0.33900   0.53060   1.00000   0.00810
U(4)  -0.05600   0.45310   0.35670   1.00000   0.00790
U(5)   0.20900   0.72690   0.35590   1.00000   0.00700
U(6)   0.22880   0.91330   0.23400   1.00000   0.00970
Pb   0.17090   0.14340   0.37280   1.00000   0.02080
O(1)   0.11500   0.76700   0.26200   1.00000   0.01000
O(2)   0.26200   0.57900   0.33600   1.00000   0.01000
O(3)   0.03200   0.31600   0.34600   1.00000   0.00390
O(4)   0.21200   0.48800   0.53500   1.00000   0.00620
O(5)   0.60400   0.50200   0.51500   1.00000   0.02530
O(6)   0.34300   0.27300   0.52400   1.00000   0.02250
O(7)   0.15100   0.87400   0.38000   1.00000   0.01720
O(8)   0.04900   0.62000   0.33100   1.00000   0.01460
O(9)   0.25200   0.35700   0.41000   1.00000   0.01110
O(10)   0.49700   0.41300   0.59300   1.00000   0.01650
O(11)   0.28800   0.79000   0.20100   1.00000   0.00410
O(12)  -0.13900   0.58700   0.37100   1.00000   0.01300
O(13)   0.10700   0.50300   0.23700   1.00000   0.01000
O(14)   0.16800   0.03700   0.26200   1.00000   0.01150
O(15)   0.52600   0.25300   0.47300   1.00000   0.02210
O(16)  -0.19500   0.34200   0.31400   1.00000   0.02010
O-H(1)   0.21300   0.64000   0.43600   1.00000   0.01690
O-H(2)   0.05200   0.47200   0.44000   1.00000   0.01190
O-H(3)  -0.13100   0.30900   0.41500   1.00000   0.01170
Wat1   0.08100   0.88000   0.15600   1.00000   0.02560
Wat2  -0.00500   0.08500   0.20300   0.50000   0.08360
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
U(1) 0.00700 0.00760 0.00970 -0.00250 -0.00010 0.00130
U(2) 0.00300 0.00540 0.01320 0.00000 0.00150 0.00000
U(3) 0.00710 0.00880 0.00830 0.00080 0.00150 0.00020
U(4) 0.00670 0.00760 0.00940 -0.00030 0.00210 0.00180
U(5) 0.00560 0.00570 0.00940 0.00020 0.00140 0.00070
U(6) 0.00870 0.00730 0.01310 -0.00310 0.00240 0.00070
Pb 0.01900 0.01340 0.02990 0.00210 0.00550 0.00000