Pb2(H2O)[(UO2)10UO12(OH)6(H2O)2] Li Y, Burns P C The Canadian Mineralogist 38 (2000) 1433-1441 Synthesis and crystal structure of a new Pb uranyl oxide hydrate with a framework structure that contains channels _database_code_amcsd 0005702 CELL PARAMETERS: 13.2810 10.2230 26.1000 90.000 103.202 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 3449.985 Density (g/cm3): 7.125 MAX. ABS. INTENSITY / VOLUME**2: 85.28020185 RIR: 3.897 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.03 8.31 8.0193 1 1 0 4 11.09 1.43 7.9787 -1 1 1 4 12.03 3.04 7.3544 1 1 1 4 12.19 16.44 7.2616 -1 1 2 4 13.70 16.03 6.4650 2 0 0 2 13.87 26.76 6.3855 1 1 2 4 14.09 100.00 6.2847 -1 1 3 4 16.26 3.73 5.4506 1 1 3 4 16.53 19.63 5.3629 -1 1 4 4 16.75 9.05 5.2939 2 0 2 2 19.01 1.43 4.6681 1 1 4 4 19.31 2.10 4.5971 -1 1 5 4 20.29 7.99 4.3763 0 2 3 4 20.98 5.08 4.2350 0 0 6 2 21.95 20.18 4.0499 -2 2 1 4 21.99 1.13 4.0416 1 1 5 4 22.28 1.50 3.9894 -2 2 2 4 22.31 27.14 3.9852 -1 1 6 4 22.31 2.41 3.9842 -2 0 6 2 22.32 5.86 3.9824 0 2 4 4 22.39 4.75 3.9715 3 1 0 4 23.16 43.33 3.8406 -2 2 3 4 23.39 2.17 3.8036 3 1 1 4 23.79 7.90 3.7398 -3 1 4 4 24.20 27.73 3.6772 2 2 2 4 24.52 77.97 3.6308 -2 2 4 4 24.70 1.38 3.6039 0 2 5 4 24.86 52.21 3.5820 3 1 2 4 25.13 26.63 3.5434 1 1 6 4 25.39 2.75 3.5079 -3 1 5 4 26.29 56.93 3.3900 -2 2 5 4 26.72 10.07 3.3361 3 1 3 4 26.86 25.26 3.3191 -4 0 2 2 27.06 10.86 3.2952 1 3 0 4 27.08 25.34 3.2923 -1 3 1 4 27.50 6.70 3.2438 1 3 1 4 27.57 7.58 3.2357 -1 3 2 4 27.59 33.99 3.2325 4 0 0 2 27.95 20.68 3.1927 2 2 4 4 27.97 10.15 3.1905 -4 0 4 2 28.09 29.74 3.1763 0 0 8 2 28.34 2.10 3.1497 -2 0 8 2 28.37 7.81 3.1454 1 3 2 4 28.39 15.20 3.1439 1 1 7 4 28.49 2.57 3.1332 -1 3 3 4 28.91 1.16 3.0881 3 1 4 4 29.64 14.81 3.0138 -3 1 7 4 29.66 5.52 3.0123 1 3 3 4 29.81 2.35 2.9972 -1 3 4 4 30.04 10.49 2.9746 4 0 2 2 30.29 69.59 2.9511 2 2 5 4 30.72 6.37 2.9100 -4 0 6 2 30.80 7.45 2.9034 -2 2 7 4 31.37 1.35 2.8516 3 1 5 4 31.74 1.30 2.8195 1 1 8 4 32.08 10.21 2.7898 -1 1 9 4 32.17 13.89 2.7825 -3 1 8 4 32.27 1.27 2.7739 -4 2 1 4 32.43 1.02 2.7604 -4 2 3 4 32.86 9.66 2.7253 2 2 6 4 33.10 1.14 2.7065 -4 2 4 4 33.20 13.09 2.6985 -3 3 1 4 33.25 8.58 2.6942 1 3 5 4 33.26 7.39 2.6938 -3 3 2 4 33.42 3.60 2.6815 -2 2 8 4 33.47 5.74 2.6773 -1 3 6 4 33.87 10.33 2.6470 4 0 4 2 34.04 2.43 2.6336 3 1 6 4 34.22 6.50 2.6201 3 3 1 4 34.78 14.90 2.5791 -4 0 8 2 35.00 7.98 2.5634 -5 1 3 4 35.11 3.52 2.5557 0 4 0 2 35.16 1.22 2.5523 1 1 9 4 35.18 4.10 2.5507 -5 1 1 4 35.28 2.19 2.5442 3 3 2 4 35.30 14.18 2.5429 0 4 1 4 35.32 18.38 2.5410 0 0 10 2 35.48 1.39 2.5303 1 3 6 4 35.52 9.21 2.5276 -1 1 10 4 35.72 2.18 2.5137 -1 3 7 4 35.82 1.07 2.5070 5 1 0 4 36.23 7.42 2.4797 -2 2 9 4 36.28 4.34 2.4764 -5 1 5 4 36.66 1.46 2.4515 3 3 3 4 36.73 1.71 2.4468 0 4 3 4 37.14 1.63 2.4205 -3 3 6 4 37.17 1.28 2.4187 -4 2 7 4 37.42 2.66 2.4032 -5 1 6 4 37.80 1.91 2.3798 -3 1 10 4 37.95 4.17 2.3711 0 4 4 4 38.09 1.02 2.3623 5 1 2 4 38.33 1.20 2.3482 2 4 1 4 38.34 1.35 2.3478 3 3 4 4 38.47 1.07 2.3401 -2 4 3 4 38.71 5.12 2.3261 4 0 6 2 38.91 2.41 2.3147 -3 3 7 4 39.02 3.10 2.3084 -1 1 11 4 40.28 3.15 2.2387 3 3 5 4 40.53 1.49 2.2259 -2 4 5 4 40.86 5.65 2.2084 -1 3 9 4 41.26 2.20 2.1882 0 4 6 4 41.31 1.77 2.1854 -4 2 9 4 41.55 1.22 2.1735 5 1 4 4 41.65 2.12 2.1684 2 2 9 4 42.00 1.97 2.1512 -2 4 6 4 42.22 4.03 2.1406 1 1 11 4 42.47 2.52 2.1285 3 3 6 4 42.70 1.18 2.1175 0 0 12 2 43.04 3.54 2.1017 3 1 9 4 43.18 2.24 2.0949 -3 3 9 4 43.19 18.37 2.0945 -5 3 2 4 43.27 14.71 2.0909 -5 3 3 4 43.70 1.30 2.0714 -1 3 10 4 44.31 1.50 2.0442 4 0 8 2 44.62 2.21 2.0306 -6 2 3 4 44.68 1.81 2.0281 -6 2 2 4 44.81 2.54 2.0225 -5 1 10 4 44.85 2.76 2.0208 2 2 10 4 44.87 4.16 2.0202 -6 2 4 4 44.87 1.82 2.0202 3 3 7 4 44.97 1.60 2.0160 -4 4 3 4 45.04 6.79 2.0129 -6 2 1 4 45.17 1.19 2.0075 1 5 1 4 45.23 2.28 2.0048 4 4 0 4 45.40 1.43 1.9975 -6 2 5 4 45.47 16.42 1.9947 -4 4 4 4 45.52 2.04 1.9926 -2 2 12 4 45.69 5.27 1.9857 6 2 0 4 45.82 1.99 1.9804 -1 5 3 4 45.85 1.01 1.9793 1 1 12 4 45.91 11.52 1.9768 4 4 1 4 45.97 3.83 1.9742 5 1 6 4 46.22 1.36 1.9641 -1 1 13 4 46.23 5.14 1.9638 -6 2 6 4 46.27 6.36 1.9622 -4 4 5 4 46.29 8.35 1.9612 3 1 10 4 46.60 9.70 1.9488 1 5 3 4 46.62 6.63 1.9481 6 2 1 4 46.69 4.27 1.9455 -1 3 11 4 47.23 9.14 1.9244 -5 1 11 4 47.45 3.03 1.9159 3 3 8 4 47.74 1.88 1.9051 1 5 4 4 47.83 5.14 1.9018 6 2 2 4 48.02 19.78 1.8948 0 4 9 4 48.17 4.07 1.8892 2 2 11 4 48.28 6.24 1.8849 -3 3 11 4 48.48 7.27 1.8776 5 1 7 4 48.67 2.25 1.8707 -4 4 7 4 48.86 12.43 1.8641 -2 2 13 4 49.10 1.47 1.8556 -3 5 1 4 49.14 4.86 1.8542 1 5 5 4 49.29 4.83 1.8488 6 2 3 4 49.29 3.51 1.8487 -1 5 6 4 49.30 1.82 1.8483 -7 1 5 4 49.33 1.42 1.8473 3 5 0 4 49.49 5.24 1.8418 1 3 11 4 49.58 2.45 1.8386 4 4 4 4 49.81 6.07 1.8305 -1 3 12 4 49.82 2.02 1.8302 -5 3 9 4 49.84 5.98 1.8295 3 5 1 4 49.96 4.17 1.8257 -7 1 6 4 50.19 1.59 1.8177 7 1 0 4 50.31 13.40 1.8137 -6 2 9 4 50.32 1.34 1.8134 -2 4 10 4 50.50 6.65 1.8072 4 0 10 2 50.71 4.30 1.8002 -3 1 14 4 50.76 6.19 1.7986 5 3 5 4 50.77 3.44 1.7981 1 5 6 4 50.92 6.12 1.7934 -3 5 5 4 50.96 7.08 1.7922 -1 5 7 4 51.18 1.89 1.7848 7 1 1 4 51.30 2.08 1.7808 4 4 5 4 51.59 1.24 1.7717 2 2 12 4 51.80 2.52 1.7650 -5 3 10 4 51.83 2.41 1.7639 -4 0 14 2 52.04 1.85 1.7574 -3 5 6 4 52.07 8.87 1.7563 -4 4 9 4 52.15 1.64 1.7539 -6 2 10 4 52.30 6.10 1.7492 -2 2 14 4 52.43 8.59 1.7452 7 1 2 4 52.84 2.08 1.7326 5 3 6 4 52.92 2.93 1.7302 6 2 5 4 53.13 1.69 1.7240 3 1 12 4 53.25 1.15 1.7203 4 4 6 4 53.30 7.18 1.7186 1 1 14 4 53.40 4.61 1.7156 -3 5 7 4 53.47 1.87 1.7137 -7 1 9 4 53.92 1.69 1.7006 7 1 3 4 54.21 5.88 1.6920 -3 1 15 4 54.49 1.47 1.6840 3 5 5 4 55.11 4.15 1.6665 2 2 13 4 55.12 3.14 1.6662 5 3 7 4 55.12 3.00 1.6662 -7 1 10 4 55.36 7.40 1.6595 -8 0 4 2 55.40 6.51 1.6584 4 4 7 4 55.43 2.46 1.6576 -7 3 3 4 55.63 1.08 1.6521 7 1 4 4 55.70 1.17 1.6503 -2 6 1 4 55.80 6.95 1.6476 2 6 0 4 55.80 1.12 1.6475 6 4 0 4 56.01 1.35 1.6417 -7 3 1 4 56.09 1.93 1.6398 1 3 13 4 56.15 2.12 1.6380 2 6 1 4 56.19 3.09 1.6369 3 3 11 4 56.24 2.04 1.6356 3 5 6 4 56.34 2.51 1.6329 -4 4 11 4 56.36 3.27 1.6324 -5 3 12 4 56.46 1.91 1.6297 -6 2 12 4 56.47 1.63 1.6296 -7 3 6 4 56.91 4.83 1.6179 -2 6 4 4 57.03 1.59 1.6148 5 1 10 4 57.14 1.48 1.6119 1 1 15 4 57.30 1.22 1.6080 0 2 15 4 57.78 1.78 1.5957 -5 5 5 4 57.80 1.44 1.5952 -8 0 8 2 57.81 2.31 1.5949 -3 1 16 4 58.14 1.09 1.5866 5 5 1 4 58.21 2.24 1.5848 3 5 7 4 58.63 1.51 1.5746 -5 1 15 4 58.71 2.86 1.5727 2 6 4 4 58.74 3.74 1.5720 2 2 14 4 58.77 2.58 1.5712 -4 4 12 4 58.91 3.44 1.5677 -6 2 13 4 59.07 1.45 1.5639 5 5 2 4 59.49 1.36 1.5538 -2 2 16 4 59.63 1.42 1.5505 -5 5 7 4 59.70 1.45 1.5489 7 1 6 4 59.72 2.25 1.5484 -7 3 9 4 59.88 1.09 1.5447 -8 2 7 4 59.91 1.45 1.5440 6 2 8 4 60.18 1.39 1.5376 5 1 11 4 60.23 3.87 1.5366 5 5 3 4 60.29 2.20 1.5352 4 4 9 4 61.85 1.02 1.5001 -5 1 16 4 61.92 1.51 1.4986 -2 6 8 4 62.12 3.60 1.4942 1 5 11 4 62.44 2.75 1.4873 8 0 4 2 62.60 4.06 1.4839 6 2 9 4 62.79 2.77 1.4798 0 4 14 4 63.16 2.55 1.4721 1 3 15 4 63.55 2.83 1.4640 7 3 5 4 63.72 2.08 1.4605 -2 6 9 4 63.79 1.71 1.4591 -3 3 16 4 64.15 3.77 1.4517 -4 4 14 4 64.40 1.02 1.4467 1 7 1 4 64.75 3.06 1.4398 -9 1 7 4 64.80 1.19 1.4387 -9 1 1 4 64.85 4.00 1.4377 1 7 2 4 65.29 1.92 1.4291 3 5 10 4 65.42 1.08 1.4266 -6 4 12 4 65.68 1.67 1.4216 -4 6 8 4 65.73 1.59 1.4207 -2 6 10 4 65.87 2.38 1.4179 -4 0 18 2 66.11 1.50 1.4134 -3 5 13 4 66.20 3.80 1.4117 0 0 18 2 66.45 2.15 1.4070 -7 1 15 4 66.67 1.76 1.4029 9 1 1 4 67.27 2.00 1.3918 -8 4 4 4 67.30 1.66 1.3913 -6 2 16 4 67.48 2.61 1.3881 -8 4 5 4 67.59 2.20 1.3860 -3 7 2 4 67.85 1.06 1.3813 -3 7 3 4 68.01 2.17 1.3784 3 5 11 4 68.23 2.48 1.3745 -1 5 14 4 68.33 2.06 1.3728 -8 0 14 2 68.49 1.44 1.3700 6 2 11 4 68.71 1.16 1.3662 -5 1 18 4 68.72 1.26 1.3660 8 4 0 4 69.02 3.74 1.3607 -7 5 7 4 69.26 1.14 1.3565 -7 1 16 4 69.40 1.80 1.3541 -9 3 4 4 69.52 2.07 1.3521 -9 3 3 4 69.83 1.59 1.3469 -6 6 4 4 70.32 1.32 1.3387 7 5 2 4 70.42 1.49 1.3370 -6 2 17 4 70.45 3.44 1.3365 6 6 0 4 71.11 1.34 1.3258 -1 3 18 4 71.25 1.07 1.3235 8 0 8 2 71.39 1.23 1.3213 -1 5 15 4 71.58 2.53 1.3183 7 5 3 4 71.67 2.53 1.3168 6 2 12 4 71.67 1.80 1.3167 5 5 9 4 71.71 1.96 1.3161 -6 6 7 4 71.87 1.24 1.3136 -8 4 10 4 71.99 3.62 1.3118 4 0 16 2 72.36 1.11 1.3059 2 6 11 4 72.78 3.20 1.2995 -6 6 8 4 72.84 1.66 1.2984 -9 1 13 4 72.98 1.45 1.2964 -5 5 14 4 73.46 1.79 1.2890 -4 4 17 4 73.56 1.67 1.2876 3 3 16 4 73.85 1.18 1.2833 -1 1 20 4 74.09 1.33 1.2797 -5 7 2 4 74.24 1.69 1.2774 1 7 9 4 74.36 1.29 1.2757 1 5 15 4 74.45 2.29 1.2743 -1 7 10 4 74.74 1.72 1.2702 -3 3 19 4 75.09 2.70 1.2651 -1 3 19 4 75.13 1.32 1.2644 -8 4 12 4 75.30 1.86 1.2621 3 7 7 4 75.40 1.61 1.2606 -7 1 18 4 75.47 2.81 1.2596 8 4 5 4 75.66 1.34 1.2569 -5 5 15 4 75.87 1.78 1.2541 -3 7 10 4 75.90 1.59 1.2535 10 2 0 4 75.93 2.01 1.2532 -10 2 9 4 76.33 1.14 1.2476 7 1 12 4 76.41 1.24 1.2465 1 7 10 4 76.85 1.66 1.2404 -2 8 4 4 76.93 3.73 1.2393 0 8 5 4 76.99 2.33 1.2386 10 2 1 4 77.07 2.08 1.2374 -8 4 13 4 77.22 2.11 1.2354 3 7 8 4 78.21 1.61 1.2223 -1 1 21 4 79.25 1.02 1.2088 -8 0 18 2 79.53 2.42 1.2053 5 3 15 4 79.62 1.43 1.2042 8 4 7 4 80.45 1.13 1.1937 3 1 19 4 80.95 2.22 1.1877 -11 1 2 4 81.33 1.09 1.1830 1 7 12 4 81.42 2.82 1.1819 5 7 6 4 81.44 2.06 1.1817 -5 3 20 4 81.53 1.88 1.1806 -10 2 13 4 81.64 2.03 1.1793 -4 8 5 4 82.68 1.63 1.1672 9 3 7 4 82.90 1.72 1.1646 2 2 20 4 83.14 1.35 1.1618 5 5 13 4 83.81 1.09 1.1542 -2 2 22 4 84.00 2.11 1.1521 -7 3 19 4 84.11 1.03 1.1509 9 5 2 4 84.32 1.07 1.1486 -5 7 12 4 84.89 1.07 1.1423 3 1 20 4 85.33 1.39 1.1375 -11 1 12 4 85.45 1.91 1.1362 4 8 5 4 85.68 1.47 1.1338 -11 3 3 4 86.13 1.42 1.1290 7 5 10 4 87.82 1.10 1.1115 2 6 16 4 88.45 1.24 1.1053 -5 1 23 4 88.49 1.02 1.1049 9 1 11 4 88.56 1.40 1.1042 -2 6 18 4 89.01 1.91 1.0998 7 5 11 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.