Cs2[(UO2)6(MoO4)7(H2O)2] Krivovichev S V, Burns P C The Canadian Mineralogist 39 (2001) 207-214 Crystal chemistry of uranyl molybdates. IV. The structures of M2[(UO2)6(MoO4)7(H2O)2] (M=Cs,NH4) _database_code_amcsd 0005716 CELL PARAMETERS: 13.9900 10.8080 25.6710 90.000 90.000 90.000 SPACE GROUP: Pbcm X-RAY WAVELENGTH: 1.541838 Cell Volume: 3881.556 Density (g/cm3): 5.439 MAX. ABS. INTENSITY / VOLUME**2: 74.64310631 RIR: 4.469 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 6.89 9.95 12.8355 0 0 2 2 12.65 2.62 6.9950 2 0 0 2 13.80 1.91 6.4177 0 0 4 2 15.09 2.24 5.8724 2 1 0 4 15.19 1.49 5.8333 1 0 4 4 15.48 7.80 5.7245 2 1 1 8 16.40 11.44 5.4040 0 2 0 2 16.60 2.38 5.3401 2 1 2 8 16.77 4.46 5.2881 0 2 1 4 17.93 4.28 4.9465 1 2 1 8 18.32 100.00 4.8419 2 1 3 8 18.91 6.22 4.6921 1 2 2 8 19.43 18.41 4.5691 0 2 3 4 20.17 1.34 4.4020 1 1 5 8 20.50 4.48 4.3324 2 1 4 8 20.76 31.76 4.2785 0 0 6 2 20.77 3.27 4.2765 2 2 0 4 21.50 1.02 4.1337 0 2 4 4 22.43 1.19 3.9643 1 2 4 8 23.23 1.19 3.8291 3 1 3 8 23.25 1.69 3.8254 2 2 3 8 23.58 4.82 3.7726 3 0 4 4 23.91 1.49 3.7222 0 2 5 4 24.39 1.43 3.6499 2 0 6 4 25.00 2.29 3.5618 3 1 4 8 25.47 2.18 3.4976 3 2 1 8 25.47 67.51 3.4975 4 0 0 2 25.76 81.46 3.4580 2 1 6 8 25.77 2.26 3.4571 1 3 1 8 26.44 1.09 3.3705 1 1 7 8 26.57 64.83 3.3544 0 2 6 4 26.79 3.10 3.3276 4 1 0 4 27.02 2.51 3.3000 4 1 1 8 27.12 1.06 3.2883 3 1 5 8 27.86 96.20 3.2028 2 3 0 4 28.54 2.24 3.1277 1 0 8 4 28.70 10.23 3.1106 2 1 7 8 28.73 4.56 3.1075 2 3 2 8 28.79 2.86 3.1014 4 1 3 8 28.86 1.04 3.0934 3 2 4 8 29.13 4.79 3.0652 1 3 4 8 29.43 1.45 3.0345 0 2 7 4 29.53 1.32 3.0246 2 2 6 8 29.74 2.78 3.0044 1 1 8 8 29.79 5.97 2.9996 2 3 3 8 30.44 5.08 2.9362 4 2 0 4 30.99 1.71 2.8856 1 3 5 8 31.21 3.85 2.8658 2 3 4 8 32.16 2.06 2.7831 3 3 2 8 32.23 8.54 2.7773 4 2 3 8 33.08 11.79 2.7079 4 0 6 4 33.16 1.30 2.7020 0 4 0 2 33.56 1.20 2.6700 4 2 4 8 34.13 1.28 2.6267 4 1 6 8 34.82 6.41 2.5766 0 4 3 4 34.94 1.34 2.5678 3 1 8 8 34.97 14.50 2.5657 2 1 9 8 34.98 1.13 2.5648 5 0 4 4 35.00 11.62 2.5640 2 3 6 8 35.29 1.44 2.5434 3 2 7 8 35.59 4.07 2.5225 0 2 9 4 35.78 2.94 2.5095 4 3 0 4 36.07 1.60 2.4903 0 4 4 4 36.55 1.60 2.4587 1 1 10 8 36.65 4.02 2.4517 1 4 4 8 36.85 2.69 2.4394 5 2 2 8 37.14 28.70 2.4209 4 2 6 8 39.31 1.22 2.2921 4 2 7 8 39.44 2.09 2.2846 0 4 6 4 39.54 1.45 2.2792 6 1 0 4 40.06 3.02 2.2508 3 3 7 8 40.98 16.54 2.2024 6 1 3 8 41.09 1.09 2.1967 3 4 4 8 41.44 1.86 2.1788 5 1 7 8 42.25 12.91 2.1393 0 0 12 2 42.44 1.98 2.1301 2 3 9 8 42.46 2.27 2.1289 1 5 1 8 42.82 1.06 2.1117 6 2 2 8 43.30 3.12 2.0894 5 3 4 8 43.58 2.68 2.0769 6 2 3 8 43.59 2.27 2.0763 3 2 10 8 43.63 9.32 2.0744 4 4 3 8 43.84 3.10 2.0652 2 5 0 4 44.24 1.07 2.0474 6 0 6 4 44.27 5.55 2.0459 4 2 9 8 44.30 2.86 2.0447 1 4 8 8 44.43 1.53 2.0390 2 5 2 8 44.67 1.02 2.0286 4 4 4 8 45.07 7.71 2.0116 6 1 6 8 45.11 1.43 2.0100 2 1 12 8 45.27 2.26 2.0031 2 3 10 8 45.61 2.14 1.9891 0 2 12 4 45.98 1.25 1.9739 4 4 5 8 46.17 1.79 1.9660 2 5 4 8 46.28 3.58 1.9616 0 4 9 4 46.39 14.69 1.9575 6 3 0 4 46.44 1.94 1.9555 3 5 1 8 46.84 1.52 1.9398 1 3 11 8 46.94 1.25 1.9358 6 1 7 8 47.45 1.34 1.9160 2 5 5 8 47.49 1.29 1.9146 6 2 6 8 47.54 2.99 1.9127 4 4 6 8 47.66 1.77 1.9082 6 3 3 8 47.67 1.14 1.9077 3 3 10 8 48.16 1.97 1.8896 3 4 8 8 48.65 3.81 1.8717 2 1 13 8 48.88 2.66 1.8633 5 1 10 8 48.97 3.72 1.8602 5 4 4 8 48.98 19.05 1.8599 2 5 6 8 49.12 1.13 1.8547 0 2 13 4 49.37 1.76 1.8459 1 5 7 8 49.40 1.46 1.8448 1 4 10 8 49.58 1.24 1.8387 1 2 13 8 49.98 9.84 1.8249 4 0 12 4 50.68 4.89 1.8013 0 6 0 2 51.21 1.29 1.7839 0 6 2 4 51.31 6.47 1.7806 6 1 9 8 51.33 8.52 1.7800 6 3 6 8 51.36 16.56 1.7789 2 3 12 8 51.66 1.07 1.7695 1 6 2 8 51.76 1.23 1.7662 0 4 11 4 51.87 1.17 1.7627 0 6 3 4 51.92 1.02 1.7611 6 4 1 8 52.31 4.60 1.7487 8 0 0 2 52.71 1.41 1.7366 2 5 8 8 52.78 1.08 1.7343 0 6 4 4 52.96 1.57 1.7290 4 2 12 8 52.96 1.61 1.7289 6 4 3 8 52.97 2.09 1.7285 3 4 10 8 53.14 1.01 1.7234 3 2 13 8 53.15 1.57 1.7232 1 2 14 8 53.18 1.59 1.7224 8 1 1 8 53.22 1.15 1.7211 1 6 4 8 53.56 4.16 1.7109 4 4 9 8 55.21 2.30 1.6638 8 2 0 4 55.25 1.32 1.6625 5 4 8 8 55.34 1.00 1.6602 0 6 6 4 55.96 5.98 1.6430 2 1 15 8 56.13 1.17 1.6386 4 2 13 8 56.33 2.56 1.6332 8 2 3 8 56.39 1.63 1.6315 0 2 15 4 56.62 1.55 1.6255 3 6 4 8 56.88 4.30 1.6188 8 0 6 4 57.55 5.86 1.6014 4 6 0 4 57.78 1.02 1.5957 5 1 13 8 58.04 1.11 1.5891 4 6 2 8 58.20 1.73 1.5852 6 5 0 4 58.55 1.52 1.5765 4 4 11 8 58.65 1.28 1.5741 4 6 3 8 59.62 3.80 1.5507 8 2 6 8 61.08 1.53 1.5172 3 0 16 4 61.66 1.06 1.5042 5 6 2 8 61.86 2.13 1.4998 4 6 6 8 62.20 1.04 1.4925 6 1 13 8 62.48 4.91 1.4865 6 5 6 8 62.51 1.04 1.4858 2 5 12 8 62.85 2.46 1.4786 4 2 15 8 63.86 2.37 1.4577 1 3 16 8 64.39 1.87 1.4470 8 4 3 8 64.45 1.42 1.4458 0 4 15 4 64.50 1.23 1.4447 7 3 10 8 64.53 5.43 1.4441 6 3 12 8 64.88 1.31 1.4372 8 2 9 8 67.98 1.08 1.3790 0 2 18 4 68.04 2.27 1.3779 0 6 12 4 68.51 1.60 1.3695 10 1 3 8 68.57 2.90 1.3685 6 1 15 8 69.14 1.02 1.3587 4 6 10 8 69.42 1.75 1.3539 8 0 12 4 70.08 1.15 1.3427 8 5 3 8 70.38 1.37 1.3377 10 2 3 8 70.48 1.80 1.3361 4 4 15 8 71.55 1.25 1.3186 9 4 4 8 71.89 1.39 1.3133 8 2 12 8 72.40 1.66 1.3053 8 4 9 8 72.48 1.56 1.3041 10 3 0 4 72.85 2.24 1.2983 5 3 16 8 73.51 1.72 1.2883 0 8 6 4 73.88 1.02 1.2828 4 2 18 8 73.93 2.42 1.2820 4 6 12 8 75.00 1.61 1.2664 2 7 11 8 76.07 1.03 1.2511 7 0 16 4 76.33 1.19 1.2477 10 1 9 8 76.34 3.20 1.2475 10 3 6 8 76.51 1.03 1.2451 0 8 8 4 79.24 1.90 1.2089 4 8 6 8 79.63 1.43 1.2040 8 6 6 8 80.21 1.79 1.1968 2 1 21 8 81.29 1.33 1.1836 2 9 0 4 82.17 1.11 1.1730 4 8 8 8 83.26 1.24 1.1604 3 6 16 8 83.89 1.37 1.1533 2 9 5 8 84.46 1.02 1.1470 8 7 3 8 86.53 1.13 1.1248 12 0 6 4 87.63 1.14 1.1135 10 3 12 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.