(NH4)2[(UO2)6(MoO4)7(H2O)2] Krivovichev S V, Burns P C The Canadian Mineralogist 39 (2001) 207-214 Crystal chemistry of uranyl molybdates. IV. The structures of M2[(UO2)6(MoO4)7(H2O)2] (M=Cs,NH4) _database_code_amcsd 0005717 CELL PARAMETERS: 13.9700 10.7470 25.6070 90.000 90.000 90.000 SPACE GROUP: Pbcm X-RAY WAVELENGTH: 1.541838 Cell Volume: 3844.522 Density (g/cm3): 4.875 MAX. ABS. INTENSITY / VOLUME**2: 77.98884411 RIR: 5.209 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 6.33 4.00 13.9700 1 0 0 2 6.90 14.20 12.8035 0 0 2 2 9.37 5.29 9.4389 1 0 2 4 10.39 4.96 8.5181 1 1 0 4 12.48 15.66 7.0920 1 1 2 8 12.67 1.24 6.9850 2 0 0 2 13.83 4.19 6.4018 0 0 4 2 15.13 20.31 5.8567 2 1 0 4 15.22 3.77 5.8198 1 0 4 4 15.52 8.80 5.7092 2 1 1 8 16.50 30.65 5.3735 0 2 0 2 16.65 1.16 5.3259 2 1 2 8 16.86 3.14 5.2590 0 2 1 4 17.33 2.73 5.1176 1 1 4 8 18.02 2.40 4.9218 1 2 1 8 18.37 100.00 4.8292 2 1 3 8 19.52 15.29 4.5474 0 2 3 4 20.23 1.09 4.3892 1 1 5 8 20.29 1.05 4.3762 3 0 2 4 20.55 1.27 4.3212 2 1 4 8 20.81 48.36 4.2678 0 0 6 2 20.86 2.23 4.2590 2 2 0 4 22.52 3.76 3.9480 1 2 4 8 23.28 1.35 3.8208 3 1 3 8 23.34 1.78 3.8110 2 2 3 8 23.63 7.27 3.7658 3 0 4 4 25.50 47.35 3.4925 4 0 0 2 25.55 1.52 3.4863 3 2 1 8 25.83 45.46 3.4492 2 1 6 8 25.91 2.49 3.4386 1 3 1 8 26.67 44.08 3.3420 0 2 6 4 26.84 1.76 3.3215 4 1 0 4 27.07 2.45 3.2939 4 1 1 8 27.18 1.11 3.2809 3 1 5 8 27.44 1.32 3.2503 1 2 6 8 27.99 65.40 3.1876 2 3 0 4 28.77 8.79 3.1026 2 1 7 8 28.84 2.93 3.0954 4 1 3 8 28.86 4.18 3.0932 2 3 2 8 28.95 2.32 3.0839 3 2 4 8 29.13 1.17 3.0659 4 0 4 4 29.27 6.99 3.0507 1 3 4 8 29.54 2.04 3.0239 0 2 7 4 29.92 7.02 2.9861 2 3 3 8 30.53 11.67 2.9283 4 2 0 4 31.13 1.06 2.8727 1 3 5 8 31.35 5.53 2.8534 2 3 4 8 32.32 7.27 2.7699 4 2 3 8 33.14 18.02 2.7028 4 0 6 4 33.20 1.53 2.6982 1 2 8 8 34.71 1.85 2.5841 1 4 2 8 35.01 6.95 2.5628 0 4 3 4 35.06 13.81 2.5592 2 1 9 8 35.14 21.37 2.5539 2 3 6 8 35.39 1.70 2.5361 3 2 7 8 35.71 4.12 2.5145 0 2 9 4 35.91 2.06 2.5007 4 3 0 4 36.65 1.24 2.4523 1 1 10 8 36.85 2.20 2.4393 1 4 4 8 36.93 1.10 2.4337 5 2 2 8 37.24 17.74 2.4146 4 2 6 8 39.35 2.00 2.2897 3 4 2 8 39.42 1.53 2.2861 4 2 7 8 39.61 3.21 2.2755 6 1 0 4 40.20 2.31 2.2430 3 3 7 8 41.05 15.35 2.1987 6 1 3 8 41.53 1.63 2.1745 5 1 7 8 42.36 10.14 2.1339 0 0 12 2 42.59 2.99 2.1226 2 3 9 8 42.71 1.30 2.1171 1 5 1 8 43.44 3.85 2.0832 5 3 4 8 43.68 2.73 2.0725 6 2 3 8 43.72 1.99 2.0706 3 2 10 8 43.82 9.82 2.0662 4 4 3 8 44.08 5.90 2.0543 2 5 0 4 44.39 5.51 2.0406 4 2 9 8 44.68 1.27 2.0284 2 5 2 8 45.15 3.82 2.0080 6 1 6 8 45.23 2.64 2.0050 2 1 12 8 45.75 3.52 1.9833 0 2 12 4 46.17 1.27 1.9663 4 4 5 8 46.49 3.40 1.9534 0 4 9 4 46.52 9.80 1.9522 6 3 0 4 46.68 1.27 1.9459 3 5 1 8 47.00 1.18 1.9332 1 3 11 8 47.79 1.88 1.9031 6 3 3 8 48.77 1.02 1.8673 6 3 4 8 48.78 3.65 1.8670 2 1 13 8 48.99 2.17 1.8593 5 1 10 8 49.15 2.39 1.8537 5 4 4 8 49.22 14.51 1.8511 2 5 6 8 49.27 1.01 1.8494 0 2 13 4 49.61 1.46 1.8375 1 4 10 8 49.62 1.85 1.8371 1 5 7 8 50.09 7.41 1.8209 4 0 12 4 50.99 3.03 1.7912 0 6 0 2 51.42 5.84 1.7771 6 1 9 8 51.42 1.26 1.7770 6 2 8 8 51.47 10.81 1.7753 6 3 6 8 51.54 12.67 1.7732 2 3 12 8 51.98 1.17 1.7594 0 4 11 4 52.18 1.48 1.7530 0 6 3 4 52.40 3.05 1.7463 8 0 0 2 52.96 1.47 1.7289 2 5 8 8 53.09 1.18 1.7249 0 6 4 4 53.10 2.64 1.7246 4 2 12 8 53.15 1.67 1.7233 6 4 3 8 53.18 1.64 1.7222 3 4 10 8 53.27 1.49 1.7198 8 1 1 8 53.53 1.47 1.7119 1 6 4 8 53.77 3.96 1.7049 4 4 9 8 55.32 3.01 1.6608 8 2 0 4 55.65 1.60 1.6516 0 6 6 4 56.12 5.97 1.6389 2 1 15 8 56.29 1.03 1.6344 4 2 13 8 56.45 2.08 1.6302 8 2 3 8 56.57 1.38 1.6270 0 2 15 4 56.93 1.76 1.6175 3 6 4 8 56.98 4.78 1.6162 8 0 6 4 57.86 3.69 1.5938 4 6 0 4 58.44 2.55 1.5793 6 5 0 4 58.76 1.38 1.5713 4 4 11 8 58.95 1.67 1.5667 4 6 3 8 59.37 1.21 1.5566 6 1 12 8 59.75 2.29 1.5477 8 2 6 8 59.80 1.01 1.5466 4 6 4 8 61.24 1.11 1.5135 3 0 16 4 62.17 2.87 1.4931 4 6 6 8 62.73 3.67 1.4812 6 5 6 8 62.79 1.93 1.4800 2 5 12 8 63.03 2.08 1.4748 4 2 15 8 63.80 1.02 1.4588 2 1 17 8 64.07 1.76 1.4533 1 3 16 8 64.58 1.83 1.4431 8 4 3 8 64.69 1.61 1.4409 0 4 15 4 64.72 3.92 1.4404 6 3 12 8 65.03 1.16 1.4343 8 2 9 8 68.19 1.01 1.3752 0 2 18 4 68.38 1.56 1.3719 0 6 12 4 68.63 1.28 1.3675 10 1 3 8 68.74 2.71 1.3656 6 1 15 8 69.56 1.23 1.3514 8 0 12 4 70.33 1.11 1.3386 8 5 3 8 70.52 1.29 1.3354 10 2 3 8 70.73 2.02 1.3320 4 4 15 8 71.63 1.04 1.3175 4 0 18 4 72.06 1.61 1.3106 8 2 12 8 72.62 1.50 1.3019 8 4 9 8 73.08 1.56 1.2948 5 3 16 8 73.97 1.33 1.2814 0 8 6 4 74.27 1.61 1.2769 4 6 12 8 74.79 1.42 1.2695 6 5 12 8 75.40 1.33 1.2606 2 7 11 8 76.52 3.14 1.2449 10 3 6 8 79.71 1.48 1.2030 4 8 6 8 79.95 1.59 1.1999 8 6 6 8 80.45 1.71 1.1938 2 1 21 8 84.45 1.01 1.1471 2 9 5 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.