Gladiusite Sokolova E V, Hawthorne F C, McCammon C A, Liferovich R P The Canadian Mineralogist 39 (2001) 1121-1130 The crystal structure of gladiusite, (Fe,Mg)4Fe2(PO4)(OH)11(H2O) _database_code_amcsd 0005729 CELL PARAMETERS: 16.9500 11.6500 6.2660 90.000 90.000 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 1237.331 Density (g/cm3): 3.027 MAX. ABS. INTENSITY / VOLUME**2: 7.875361892 RIR: 0.847 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.21 69.35 9.6009 1 1 0 4 12.92 100.00 6.8534 2 1 0 4 15.07 22.65 5.8773 -1 0 1 2 15.07 6.54 5.8773 1 0 1 2 15.21 48.98 5.8250 0 2 0 2 16.06 1.81 5.5184 0 1 1 4 16.09 4.41 5.5088 1 2 0 4 16.90 2.04 5.2473 -1 1 1 4 16.90 9.80 5.2473 1 1 1 4 17.44 45.59 5.0837 3 1 0 4 18.48 76.24 4.8005 2 2 0 4 19.19 2.47 4.6245 2 1 1 4 19.19 2.57 4.6245 -2 1 1 4 20.82 2.69 4.2663 0 2 1 4 21.17 3.98 4.1961 3 0 1 2 21.17 8.42 4.1961 -3 0 1 2 21.92 1.74 4.0556 3 2 0 4 22.52 11.07 3.9478 3 1 1 4 22.52 1.15 3.9478 -3 1 1 4 23.34 2.78 3.8107 -2 2 1 4 23.50 26.42 3.7853 1 3 0 4 25.23 42.86 3.5304 2 3 0 4 26.00 32.29 3.4267 4 2 0 4 26.17 2.09 3.4047 3 2 1 4 26.17 8.15 3.4047 -3 2 1 4 26.52 1.26 3.3609 -4 1 1 4 26.52 4.66 3.3609 4 1 1 4 27.01 7.14 3.3008 0 3 1 4 27.40 10.94 3.2550 5 1 0 4 27.53 5.42 3.2400 1 3 1 4 29.03 1.48 3.0758 2 3 1 4 29.52 4.49 3.0255 0 1 2 4 29.97 2.38 2.9816 5 0 1 2 30.00 1.09 2.9784 -1 1 2 4 30.00 1.13 2.9784 1 1 2 4 30.42 1.33 2.9386 -2 0 2 2 30.51 12.83 2.9299 5 2 0 4 30.70 2.38 2.9125 0 4 0 2 31.16 11.66 2.8704 1 4 0 4 31.24 32.17 2.8630 4 3 0 4 31.39 1.79 2.8501 3 3 1 4 31.39 4.77 2.8494 2 1 2 4 31.39 2.73 2.8494 -2 1 2 4 31.67 37.94 2.8250 6 0 0 2 32.51 9.06 2.7544 2 4 0 4 32.62 15.87 2.7454 6 1 0 4 32.89 16.21 2.7234 -1 2 2 4 32.89 23.79 2.7234 1 2 2 4 33.60 31.85 2.6672 3 1 2 4 33.60 25.03 2.6672 -3 1 2 4 33.94 3.09 2.6411 0 4 1 4 34.18 9.08 2.6237 2 2 2 4 34.18 5.84 2.6237 -2 2 2 4 34.36 2.00 2.6096 -1 4 1 4 34.65 18.28 2.5888 3 4 0 4 35.14 3.47 2.5538 5 3 0 4 35.31 11.79 2.5418 6 2 0 4 35.60 1.64 2.5215 2 4 1 4 35.64 8.92 2.5192 -4 0 2 2 35.64 6.86 2.5192 4 0 2 2 36.23 1.03 2.4794 3 2 2 4 36.49 3.41 2.4623 4 1 2 4 36.49 4.08 2.4623 -4 1 2 4 36.86 1.08 2.4384 0 3 2 4 37.26 45.45 2.4135 -1 3 2 4 37.26 52.34 2.4135 1 3 2 4 37.47 2.27 2.4002 4 4 0 4 38.41 2.45 2.3433 2 3 2 4 38.41 2.79 2.3433 -2 3 2 4 38.95 2.93 2.3122 -4 2 2 4 39.02 2.14 2.3083 1 5 0 4 39.91 2.49 2.2586 -7 0 1 2 39.94 2.89 2.2573 5 1 2 4 40.28 3.32 2.2388 -3 3 2 4 40.34 4.69 2.2359 7 2 0 4 40.85 5.79 2.2091 5 4 0 4 41.70 1.30 2.1660 -1 5 1 4 41.94 2.84 2.1540 3 5 0 4 42.23 9.30 2.1400 -5 2 2 4 42.23 6.82 2.1400 5 2 2 4 42.67 15.32 2.1188 8 0 0 2 43.12 7.98 2.0980 -6 0 2 2 43.12 6.49 2.0980 6 0 2 2 43.41 1.81 2.0846 8 1 0 4 43.43 1.83 2.0835 5 4 1 4 43.76 5.32 2.0686 2 4 2 4 43.76 2.93 2.0686 -2 4 2 4 43.85 1.24 2.0648 -6 1 2 4 44.07 2.47 2.0547 7 3 0 4 44.37 1.34 2.0417 4 5 0 4 44.69 2.50 2.0278 6 4 0 4 45.45 1.24 1.9956 3 4 2 4 45.45 1.10 1.9956 -3 4 2 4 46.35 1.23 1.9591 3 0 3 2 46.79 1.03 1.9417 0 6 0 2 48.07 7.07 1.8926 2 6 0 4 48.70 21.74 1.8696 0 5 2 4 48.92 1.49 1.8620 7 4 0 4 48.97 2.48 1.8599 8 3 0 4 48.99 22.43 1.8592 9 1 0 4 49.02 11.04 1.8584 -1 5 2 4 49.02 11.82 1.8584 1 5 2 4 49.37 4.20 1.8459 -6 3 2 4 49.37 5.08 1.8459 6 3 2 4 49.44 1.56 1.8437 1 6 1 4 49.56 1.17 1.8395 0 3 3 4 49.95 4.45 1.8257 2 5 2 4 49.95 4.45 1.8257 -2 5 2 4 50.79 1.37 1.7975 6 5 0 4 50.96 1.73 1.7920 9 2 0 4 51.24 1.22 1.7830 -8 3 1 4 51.26 2.02 1.7824 -9 1 1 4 51.48 4.58 1.7750 3 5 2 4 51.48 3.40 1.7750 -3 5 2 4 52.74 1.59 1.7355 -8 1 2 4 52.74 1.32 1.7355 8 1 2 4 53.32 13.26 1.7182 -7 3 2 4 53.32 10.99 1.7182 7 3 2 4 53.58 6.78 1.7105 -4 5 2 4 53.58 6.46 1.7105 4 5 2 4 54.61 8.92 1.6805 -8 2 2 4 54.61 6.52 1.6805 8 2 2 4 55.48 11.59 1.6563 1 7 0 4 56.18 6.35 1.6372 -5 5 2 4 56.18 4.57 1.6372 5 5 2 4 56.34 3.15 1.6331 2 7 0 4 56.55 2.93 1.6275 10 2 0 4 56.83 6.39 1.6200 2 6 2 4 56.83 5.80 1.6200 -2 6 2 4 57.58 8.39 1.6006 -7 4 2 4 57.58 9.79 1.6006 7 4 2 4 57.64 7.65 1.5993 -8 3 2 4 57.64 6.56 1.5993 8 3 2 4 57.65 4.92 1.5989 -9 1 2 4 57.65 4.58 1.5989 9 1 2 4 58.35 1.97 1.5815 9 4 0 4 58.96 27.30 1.5665 0 0 4 2 59.27 1.42 1.5591 -6 5 2 4 59.27 1.05 1.5591 6 5 2 4 59.51 3.10 1.5535 10 3 0 4 59.69 1.27 1.5491 4 7 0 4 60.17 2.92 1.5379 -4 6 2 4 60.17 5.01 1.5379 4 6 2 4 60.62 3.11 1.5276 11 1 0 4 60.64 2.89 1.5271 2 1 4 4 60.64 1.25 1.5271 -2 1 4 4 61.28 2.52 1.5128 0 2 4 4 61.71 3.76 1.5032 -8 4 2 4 61.71 4.73 1.5032 8 4 2 4 61.99 1.67 1.4970 3 1 4 4 62.29 3.99 1.4905 -9 3 2 4 62.29 3.98 1.4905 9 3 2 4 62.33 4.07 1.4897 11 2 0 4 62.35 1.85 1.4892 2 2 4 4 62.35 1.44 1.4892 -2 2 4 4 62.79 1.71 1.4799 -7 5 2 4 62.79 1.25 1.4799 7 5 2 4 63.50 2.72 1.4650 10 4 0 4 63.54 2.34 1.4643 -1 7 2 4 63.54 1.45 1.4643 1 7 2 4 64.36 1.15 1.4474 -1 3 4 4 64.36 1.15 1.4474 1 3 4 4 64.98 5.65 1.4352 2 8 0 4 65.15 1.30 1.4319 -2 3 4 4 65.15 1.74 1.4319 2 3 4 4 65.17 7.40 1.4315 8 6 0 4 65.50 1.76 1.4250 -6 6 2 4 65.50 1.55 1.4250 6 6 2 4 65.52 1.60 1.4247 -4 2 4 4 65.52 1.25 1.4247 4 2 4 4 66.19 5.32 1.4118 -9 4 2 4 66.19 5.20 1.4118 9 4 2 4 66.28 1.58 1.4102 3 8 0 4 68.08 2.34 1.3772 4 8 0 4 68.20 1.14 1.3751 1 4 4 4 68.25 2.93 1.3742 -4 3 4 4 68.25 1.54 1.3742 4 3 4 4 68.33 1.99 1.3727 12 2 0 4 68.40 2.89 1.3716 7 7 0 4 68.45 1.41 1.3707 10 5 0 4 68.49 2.60 1.3700 6 0 4 2 68.49 3.36 1.3700 -6 0 4 2 69.03 1.91 1.3606 -6 1 4 4 69.03 1.04 1.3606 6 1 4 4 69.74 3.30 1.3485 -5 7 2 4 69.74 3.18 1.3485 5 7 2 4 70.23 2.05 1.3402 3 4 4 4 70.23 1.44 1.3402 -3 4 4 4 70.36 1.23 1.3380 5 8 0 4 70.63 1.70 1.3336 -6 2 4 4 70.63 1.10 1.3336 6 2 4 4 71.03 2.84 1.3271 10 4 2 4 71.03 2.28 1.3271 -10 4 2 4 73.55 1.24 1.2877 -12 0 2 2 73.55 1.29 1.2877 12 0 2 2 74.21 1.06 1.2778 5 4 4 4 75.47 1.24 1.2596 -8 0 4 2 75.47 1.01 1.2596 8 0 4 2 75.74 1.11 1.2558 -10 5 2 4 75.74 1.01 1.2558 10 5 2 4 76.36 1.17 1.2471 9 7 0 4 79.41 1.29 1.2068 2 6 4 4 79.41 1.38 1.2068 -2 6 4 4 79.94 2.24 1.2001 8 8 0 4 80.11 3.12 1.1980 -9 1 4 4 80.11 3.92 1.1980 9 1 4 4 80.48 1.25 1.1934 1 9 2 4 83.82 1.82 1.1541 2 10 0 4 84.96 3.59 1.1416 7 9 0 4 85.28 1.88 1.1381 -1 7 4 4 85.28 2.53 1.1381 1 7 4 4 86.54 3.25 1.1247 15 1 0 4 86.67 2.07 1.1233 4 10 0 4 87.73 1.67 1.1125 13 4 2 4 87.73 1.76 1.1125 -13 4 2 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.