KNa5[(UO2)(SO4)4](H2O) Hayden L A, Burns P C The Canadian Mineralogist 40 (2002) 211-216 The sharing of an edge between a uranyl pentagonal bipyramid and sulfate tetrahedron in the structure of KNa5[(UO2)(SO4)4](H2O) _database_code_amcsd 0005767 CELL PARAMETERS: 16.9170 5.5999 35.3400 90.000 90.437 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 3347.785 Density (g/cm3): 3.287 MAX. ABS. INTENSITY / VOLUME**2: 14.00706030 RIR: 1.387 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 5.00 2.26 17.6695 0 0 2 2 10.01 56.06 8.8347 0 0 4 2 10.46 60.73 8.4583 2 0 0 2 11.56 51.18 7.6520 -2 0 2 2 11.63 54.98 7.6066 2 0 2 2 14.44 32.67 6.1331 -2 0 4 2 14.55 24.13 6.0865 2 0 4 2 15.04 2.54 5.8898 0 0 6 2 16.68 50.26 5.3162 1 1 0 4 16.86 7.55 5.2589 -1 1 1 4 16.87 100.00 5.2552 1 1 1 4 17.43 3.00 5.0874 1 1 2 4 18.29 10.11 4.8508 -2 0 6 2 18.29 74.12 4.8499 -1 1 3 4 18.33 14.46 4.8412 1 1 3 4 18.42 27.70 4.8162 2 0 6 2 19.47 18.76 4.5599 -1 1 4 4 19.51 33.53 4.5503 1 1 4 4 20.10 6.57 4.4174 0 0 8 2 20.88 7.81 4.2534 -1 1 5 4 20.93 18.40 4.2436 1 1 5 4 21.57 13.78 4.1201 -4 0 2 2 21.64 18.09 4.1059 4 0 2 2 22.37 10.80 3.9734 3 1 0 4 22.50 3.10 3.9509 -3 1 1 4 22.53 4.06 3.9462 3 1 1 4 22.56 15.05 3.9417 1 1 6 4 22.64 9.57 3.9279 -2 0 8 2 22.78 4.54 3.9033 2 0 8 2 22.91 8.69 3.8811 -3 1 2 4 22.97 48.77 3.8722 3 1 2 4 23.59 35.82 3.7711 -3 1 3 4 23.67 17.94 3.7589 3 1 3 4 24.28 4.94 3.6652 -1 1 7 4 24.34 2.44 3.6564 1 1 7 4 24.52 1.76 3.6311 -3 1 4 4 25.20 3.00 3.5339 0 0 10 2 25.66 1.24 3.4716 -3 1 5 4 25.78 10.63 3.4557 3 1 5 4 25.84 61.44 3.4478 -4 0 6 2 26.03 73.68 3.4229 4 0 6 2 26.20 12.42 3.4015 -1 1 8 4 26.26 2.90 3.3935 1 1 8 4 27.00 4.14 3.3022 -3 1 6 4 27.14 32.48 3.2858 3 1 6 4 27.43 17.39 3.2519 2 0 10 2 28.22 16.46 3.1621 -1 1 9 4 28.29 12.17 3.1548 1 1 9 4 28.51 60.16 3.1305 -3 1 7 4 28.67 12.68 3.1142 3 1 7 4 29.35 1.85 3.0433 4 0 8 2 30.34 2.21 2.9463 3 1 8 4 30.34 1.15 2.9462 -1 1 10 4 30.35 40.99 2.9449 0 0 12 2 30.88 4.79 2.8958 5 1 0 4 31.00 1.01 2.8846 5 1 1 4 31.27 4.26 2.8607 -5 1 2 4 31.74 2.78 2.8194 6 0 0 2 31.77 17.17 2.8164 -5 1 3 4 31.87 15.38 2.8078 5 1 3 4 32.07 3.11 2.7912 0 2 1 4 32.11 8.47 2.7878 -2 0 12 2 32.11 1.75 2.7875 -6 0 2 2 32.13 30.27 2.7854 3 1 9 4 32.19 1.16 2.7809 6 0 2 2 32.37 9.99 2.7654 0 2 2 4 32.47 2.71 2.7571 -5 1 4 4 32.53 4.23 2.7525 -1 1 11 4 32.88 15.40 2.7241 0 2 3 4 32.90 14.99 2.7220 -4 0 10 2 33.16 6.44 2.7017 4 0 10 2 33.28 3.07 2.6919 -6 0 4 2 33.36 12.69 2.6858 -5 1 5 4 33.43 7.32 2.6800 6 0 4 2 33.82 10.35 2.6501 2 2 1 4 33.86 20.96 2.6477 -3 1 10 4 34.10 5.62 2.6294 -2 2 2 4 34.12 1.05 2.6276 2 2 2 4 34.42 8.63 2.6054 -5 1 6 4 34.45 11.35 2.6031 0 2 5 4 34.57 8.78 2.5942 -2 2 3 4 34.79 11.98 2.5787 -1 1 12 4 35.18 3.63 2.5507 -6 0 6 2 35.57 3.03 2.5242 0 0 14 2 35.85 12.33 2.5049 5 1 7 4 36.13 6.30 2.4860 2 2 5 4 36.70 4.95 2.4486 0 2 7 4 37.07 2.98 2.4250 -2 2 6 4 37.11 9.18 2.4227 -1 1 13 4 37.14 5.70 2.4206 2 2 6 4 37.18 6.92 2.4180 1 1 13 4 37.24 1.70 2.4146 5 1 8 4 37.25 5.10 2.4138 2 0 14 2 37.34 2.08 2.4081 4 0 12 2 37.93 1.48 2.3720 -3 1 12 4 37.99 9.71 2.3684 6 0 8 2 38.23 13.28 2.3543 -2 2 7 4 38.31 2.75 2.3497 2 2 7 4 38.51 5.54 2.3379 -5 1 9 4 38.64 7.85 2.3302 -4 2 1 4 38.66 12.24 2.3289 4 2 1 4 38.76 2.49 2.3233 5 1 9 4 39.31 9.34 2.2919 -4 2 3 4 39.38 5.81 2.2883 4 2 3 4 39.53 2.46 2.2800 -2 2 8 4 39.53 7.95 2.2797 0 2 9 4 39.56 1.28 2.2781 1 1 14 4 39.61 1.76 2.2751 2 2 8 4 40.13 2.37 2.2471 -5 1 10 4 40.65 4.11 2.2196 -4 2 5 4 40.66 6.85 2.2188 7 1 0 4 40.73 6.45 2.2155 -7 1 1 4 40.75 1.78 2.2141 4 2 5 4 40.76 1.12 2.2135 7 1 1 4 40.79 2.99 2.2122 -6 0 10 2 40.86 8.60 2.2087 0 0 16 2 40.96 1.48 2.2036 -2 2 9 4 40.96 1.44 2.2035 -7 1 2 4 41.05 1.84 2.1987 2 2 9 4 41.11 1.17 2.1958 6 0 10 2 41.13 2.38 2.1946 0 2 10 4 41.46 6.00 2.1777 7 1 3 4 41.52 3.96 2.1748 -4 0 14 2 41.82 8.33 2.1602 4 0 14 2 41.86 6.46 2.1580 -5 1 11 4 41.91 2.23 2.1558 -1 1 15 4 41.91 8.63 2.1556 -7 1 4 4 42.06 6.95 2.1485 7 1 4 4 42.15 5.18 2.1440 5 1 11 4 42.21 1.75 2.1410 -2 0 16 2 42.32 1.61 2.1358 -3 1 14 4 42.37 1.11 2.1331 2 0 16 2 42.53 13.59 2.1255 3 1 14 4 42.60 8.68 2.1224 -4 2 7 4 42.62 5.32 2.1212 -7 1 5 4 42.74 4.80 2.1156 4 2 7 4 42.76 8.73 2.1146 8 0 0 2 42.80 3.14 2.1128 7 1 5 4 43.95 5.58 2.0600 -8 0 4 2 44.00 2.66 2.0581 5 1 12 4 44.11 4.31 2.0529 8 0 4 2 44.17 5.21 2.0504 -2 2 11 4 44.31 2.48 2.0444 -6 0 12 2 44.38 2.13 2.0414 -1 1 16 4 44.46 1.66 2.0379 1 1 16 4 44.61 4.38 2.0313 -3 1 15 4 44.67 3.63 2.0288 6 0 12 2 44.73 4.16 2.0261 7 1 7 4 44.83 5.56 2.0217 3 1 15 4 45.10 2.51 2.0104 -4 2 9 4 45.46 1.13 1.9950 -8 0 6 2 45.62 1.81 1.9884 -5 1 13 4 45.62 5.35 1.9884 -7 1 8 4 45.66 3.29 1.9867 6 2 0 4 45.73 13.05 1.9842 -6 2 1 4 45.76 2.31 1.9830 6 2 1 4 45.90 5.78 1.9772 7 1 8 4 45.94 3.65 1.9755 -2 2 12 4 46.23 3.09 1.9639 -4 0 16 2 46.24 1.38 1.9633 0 0 18 2 46.39 2.94 1.9573 6 2 3 4 46.56 8.71 1.9504 0 2 13 4 46.89 4.54 1.9376 -1 1 17 4 46.89 4.64 1.9376 -7 1 9 4 46.96 1.15 1.9349 -3 1 16 4 46.97 1.51 1.9344 1 1 17 4 47.19 4.49 1.9260 7 1 9 4 47.47 5.32 1.9153 -6 2 5 4 47.63 5.29 1.9092 2 0 18 2 47.64 1.74 1.9090 -5 1 14 4 47.92 7.11 1.8982 2 2 13 4 48.08 6.06 1.8924 -4 2 11 4 48.21 3.57 1.8878 -6 0 14 2 48.29 4.78 1.8849 4 2 11 4 49.10 4.09 1.8554 1 3 0 4 49.37 2.22 1.8460 -3 1 17 4 49.39 3.81 1.8453 6 2 7 4 49.53 2.22 1.8403 1 1 18 4 49.73 3.34 1.8334 -5 1 15 4 49.75 1.75 1.8326 -2 2 14 4 50.07 2.96 1.8217 5 1 15 4 50.13 1.85 1.8198 7 1 11 4 50.24 4.74 1.8161 -1 3 4 4 50.26 2.58 1.8155 1 3 4 4 51.15 3.46 1.7860 -4 0 18 2 51.27 1.40 1.7819 9 1 0 4 51.36 4.46 1.7790 9 1 1 4 51.44 3.14 1.7766 -6 2 9 4 51.47 3.25 1.7756 4 0 18 2 51.49 2.42 1.7748 -4 2 13 4 51.59 1.54 1.7716 9 1 2 4 51.64 1.12 1.7701 -1 3 6 4 51.64 1.20 1.7701 -3 3 1 4 51.65 1.59 1.7696 3 3 1 4 51.66 1.79 1.7692 1 3 6 4 51.76 3.54 1.7662 7 1 12 4 51.79 2.05 1.7652 -2 2 15 4 51.84 3.46 1.7638 -9 1 3 4 51.84 5.19 1.7636 -3 3 2 4 51.87 2.51 1.7628 3 3 2 4 51.92 3.65 1.7610 2 2 15 4 51.96 1.52 1.7600 9 1 3 4 52.07 6.75 1.7564 3 1 18 4 52.18 1.04 1.7530 -3 3 3 4 52.53 1.85 1.7420 -1 3 7 4 52.65 2.80 1.7383 -3 3 4 4 52.85 2.81 1.7323 6 0 16 2 52.85 2.00 1.7323 -2 0 20 2 53.09 1.21 1.7249 9 1 5 4 53.10 4.41 1.7249 -7 1 13 4 53.13 5.03 1.7239 -8 0 12 2 53.49 1.58 1.7131 7 1 13 4 53.54 5.48 1.7115 8 0 12 2 53.56 5.15 1.7111 -1 3 8 4 53.59 5.48 1.7101 1 3 8 4 53.86 1.09 1.7022 9 1 6 4 54.00 4.30 1.6980 -3 3 6 4 54.08 3.52 1.6958 3 3 6 4 54.22 1.72 1.6917 10 0 0 2 54.35 6.86 1.6880 -3 1 19 4 54.42 1.46 1.6860 -8 2 1 4 54.43 4.17 1.6857 6 2 11 4 54.45 2.49 1.6850 8 2 1 4 54.48 1.01 1.6841 -9 1 7 4 54.53 3.02 1.6827 10 0 2 2 54.59 3.44 1.6811 3 1 19 4 54.70 2.68 1.6780 -1 1 20 4 54.87 1.05 1.6733 -3 3 7 4 54.90 1.23 1.6723 -7 1 14 4 54.92 1.24 1.6718 -8 2 3 4 55.02 1.98 1.6691 0 2 17 4 55.02 2.57 1.6689 8 2 3 4 55.28 3.06 1.6618 -4 2 15 4 55.38 1.57 1.6591 10 0 4 2 55.46 1.08 1.6567 -9 1 8 4 55.53 3.76 1.6548 4 2 15 4 55.95 1.34 1.6435 -8 2 5 4 55.97 1.54 1.6429 6 2 12 4 56.00 2.25 1.6422 1 3 10 4 56.10 1.25 1.6394 -2 2 17 4 56.11 3.34 1.6390 8 2 5 4 56.24 1.55 1.6356 2 2 17 4 56.29 1.34 1.6344 5 3 0 4 56.36 1.13 1.6324 5 3 1 4 56.45 2.63 1.6300 -5 1 18 4 56.53 4.53 1.6280 -5 3 2 4 56.56 1.59 1.6271 -9 1 9 4 56.57 3.29 1.6269 5 3 2 4 56.61 1.93 1.6260 4 0 20 2 56.90 2.10 1.6182 9 1 9 4 56.96 1.18 1.6166 -3 3 9 4 57.03 2.10 1.6149 8 0 14 2 57.23 2.11 1.6096 7 1 15 4 57.29 2.95 1.6081 -6 2 13 4 57.48 3.65 1.6033 -8 2 7 4 57.48 3.62 1.6032 1 1 21 4 57.61 1.28 1.5999 6 2 13 4 57.71 1.69 1.5975 8 2 7 4 58.18 1.53 1.5856 -3 3 10 4 58.25 1.46 1.5838 -10 0 8 2 58.31 2.98 1.5825 3 3 10 4 58.56 3.31 1.5764 -5 3 6 4 58.57 1.61 1.5759 2 0 22 2 58.68 1.84 1.5734 5 3 6 4 58.78 1.05 1.5709 -7 1 16 4 58.80 3.36 1.5704 -1 3 12 4 58.83 2.30 1.5696 -5 1 19 4 59.10 1.20 1.5631 -9 1 11 4 59.22 2.55 1.5603 5 1 19 4 59.49 4.92 1.5538 -8 2 9 4 59.65 4.38 1.5501 3 3 11 4 59.78 3.55 1.5469 8 2 9 4 59.80 1.09 1.5466 3 1 21 4 60.37 1.97 1.5333 -8 0 16 2 60.47 2.10 1.5310 5 3 8 4 60.70 1.86 1.5256 -2 2 19 4 60.85 1.63 1.5223 -7 1 17 4 60.89 1.20 1.5213 10 0 10 2 60.99 1.73 1.5191 8 2 10 4 61.19 1.26 1.5148 6 2 15 4 61.61 1.54 1.5055 -4 0 22 2 62.11 1.40 1.4944 1 3 14 4 62.22 1.89 1.4921 6 0 20 2 62.53 2.03 1.4855 -5 3 10 4 62.53 1.79 1.4854 9 1 13 4 62.72 1.64 1.4813 5 3 10 4 62.93 3.39 1.4769 11 1 2 4 63.13 3.16 1.4727 -11 1 3 4 63.79 1.45 1.4591 -5 1 21 4 63.84 1.83 1.4581 -7 3 4 4 63.86 4.07 1.4577 -4 2 19 4 63.94 2.27 1.4559 7 3 4 4 64.11 1.13 1.4525 -2 0 24 2 64.14 1.03 1.4520 -3 3 14 4 64.15 1.54 1.4518 4 2 19 4 64.28 1.60 1.4492 11 1 5 4 64.30 2.20 1.4487 3 3 14 4 64.42 2.76 1.4463 10 2 1 4 64.62 3.55 1.4424 0 2 21 4 64.73 2.88 1.4401 -6 2 17 4 64.83 2.14 1.4382 -10 2 3 4 64.86 3.52 1.4376 -8 2 13 4 64.96 1.06 1.4356 11 1 6 4 65.41 1.48 1.4268 5 3 12 4 65.44 1.21 1.4262 -9 1 15 4 65.47 2.19 1.4257 -11 1 7 4 65.59 1.20 1.4234 -2 2 21 4 65.70 1.46 1.4212 -1 3 16 4 65.76 1.03 1.4200 11 1 7 4 65.94 3.25 1.4166 10 2 5 4 66.66 1.11 1.4030 -7 3 8 4 66.81 1.47 1.4003 10 0 14 2 66.81 1.15 1.4003 -6 0 22 2 66.88 2.26 1.3990 7 3 8 4 66.88 1.23 1.3989 0 4 1 4 67.14 1.54 1.3942 -10 2 7 4 67.66 1.14 1.3848 -1 3 17 4 67.70 1.58 1.3840 11 1 9 4 67.77 2.23 1.3827 0 4 4 4 67.92 1.21 1.3801 2 4 1 4 68.08 1.36 1.3771 -2 4 2 4 68.10 1.01 1.3769 2 4 2 4 68.25 1.64 1.3742 -5 3 14 4 68.30 1.21 1.3734 -12 0 6 2 68.43 1.63 1.3710 -11 1 10 4 68.66 3.01 1.3669 -1 1 25 4 68.76 1.08 1.3653 1 1 25 4 68.78 1.15 1.3649 -2 4 4 4 68.98 1.06 1.3614 -6 2 19 4 69.32 1.38 1.3556 10 2 9 4 69.76 1.16 1.3481 9 1 17 4 69.77 1.15 1.3479 1 3 18 4 70.22 1.36 1.3404 2 0 26 2 70.47 1.44 1.3363 7 1 21 4 70.57 2.24 1.3346 0 4 8 4 70.75 1.08 1.3316 -2 2 23 4 71.12 1.58 1.3255 -4 4 2 4 71.15 1.79 1.3251 4 4 2 4 71.26 2.52 1.3233 -10 2 11 4 71.55 1.42 1.3187 -2 4 8 4 72.00 1.21 1.3115 5 3 16 4 72.04 1.13 1.3109 -9 3 4 4 72.16 1.09 1.3091 5 1 24 4 72.18 1.62 1.3088 9 3 4 4 72.34 1.30 1.3062 8 2 17 4 73.02 1.18 1.2958 4 4 6 4 73.67 1.18 1.2860 -4 2 23 4 73.67 1.84 1.2859 2 4 10 4 73.88 1.08 1.2828 -11 1 14 4 74.02 1.12 1.2807 6 2 21 4 74.06 1.78 1.2801 -1 3 20 4 74.13 1.16 1.2790 1 3 20 4 74.29 1.11 1.2767 10 0 18 2 74.44 1.05 1.2745 10 2 13 4 74.71 1.81 1.2706 -9 3 8 4 75.30 1.01 1.2621 0 0 28 2 75.31 1.72 1.2619 0 2 25 4 75.54 1.48 1.2586 -12 2 1 4 75.96 1.18 1.2527 -3 3 20 4 76.08 1.14 1.2511 12 2 3 4 76.21 1.28 1.2493 -2 2 25 4 76.21 1.09 1.2492 -13 1 5 4 76.82 1.38 1.2409 6 4 4 4 77.09 1.26 1.2372 -10 2 15 4 77.78 1.07 1.2279 -9 1 21 4 77.83 1.13 1.2272 13 1 7 4 78.10 1.39 1.2237 -12 2 7 4 79.08 1.17 1.2110 2 4 14 4 79.57 1.25 1.2048 -3 1 28 4 80.14 1.39 1.1976 5 3 20 4 80.33 1.70 1.1952 -8 2 21 4 80.93 1.21 1.1879 8 2 21 4 81.82 1.01 1.1772 -4 4 14 4 82.47 1.30 1.1696 12 2 11 4 83.99 1.02 1.1523 6 4 12 4 84.76 1.72 1.1437 -4 2 27 4 85.14 1.05 1.1396 4 2 27 4 85.23 1.32 1.1386 -9 3 16 4 85.96 1.09 1.1308 7 3 20 4 86.06 1.26 1.1298 -8 4 8 4 86.28 1.23 1.1274 8 4 8 4 86.69 1.19 1.1232 11 3 10 4 87.03 1.20 1.1197 -13 1 15 4 87.62 1.17 1.1136 -12 2 15 4 88.07 1.01 1.1091 -14 2 1 4 88.24 1.11 1.1073 12 2 15 4 88.61 1.41 1.1037 1 5 5 4 89.20 1.32 1.0979 3 5 1 4 89.28 1.21 1.0972 -14 2 5 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.