Ca[(UO2)4O3(OH)4](H2O)2 Glatz R E, Li Y, Hughes K-A, Cahill C L, Burns P C The Canadian Mineralogist 40 (2002) 217-224 Synthesis and structure of a new Ca uranyl oxide hydrate, Ca[(UO2)4O3(OH)4](H2O)2, and its relationship to becquerelite _database_code_amcsd 0005768 CELL PARAMETERS: 8.0556 8.4212 10.9580 78.878 87.922 72.277 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 694.587 Density (g/cm3): 6.084 MAX. ABS. INTENSITY / VOLUME**2: 165.5691034 RIR: 8.862 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 8.23 6.31 10.7491 0 0 1 2 11.24 1.84 7.8738 0 1 0 2 11.54 8.96 7.6711 1 0 0 2 12.60 1.16 7.0238 0 1 1 2 14.02 100.00 6.3163 -1 0 1 2 14.35 7.11 6.1743 1 0 1 2 16.49 2.40 5.3745 0 0 2 2 19.94 18.80 4.4523 -1 0 2 2 23.19 2.31 3.8355 2 0 0 2 23.42 1.69 3.7980 2 1 1 2 24.45 13.79 3.6402 -2 0 1 2 24.83 8.77 3.5853 2 0 1 2 24.85 16.11 3.5830 0 0 3 2 24.95 4.94 3.5685 -1 -2 1 2 25.05 35.35 3.5544 1 2 2 2 25.36 8.09 3.5119 0 2 2 2 25.54 36.00 3.4878 0 -2 1 2 27.09 9.23 3.2912 2 2 0 2 27.21 24.48 3.2771 2 2 1 2 27.73 21.98 3.2169 1 0 3 2 28.26 3.10 3.1581 -2 0 2 2 28.31 8.04 3.1522 -1 2 1 2 28.45 21.58 3.1373 -1 2 0 2 28.92 22.46 3.0872 2 0 2 2 30.03 13.20 2.9756 -1 -2 2 2 30.35 12.02 2.9447 0 2 3 2 30.61 1.35 2.9211 0 -2 2 2 33.34 6.38 2.6873 0 0 4 2 33.82 7.06 2.6503 -2 0 3 2 33.86 4.32 2.6475 -2 -2 2 2 34.34 4.13 2.6115 2 2 3 2 34.82 5.93 2.5763 -1 2 3 2 35.09 1.31 2.5575 2 3 0 2 35.09 9.56 2.5570 3 0 0 2 35.12 10.33 2.5554 -1 0 4 2 35.39 2.03 2.5364 1 -2 2 2 35.60 2.07 2.5221 3 2 0 2 36.31 4.03 2.4743 3 0 1 2 36.46 1.07 2.4644 -1 -2 3 2 37.19 1.86 2.4173 -2 2 1 2 37.37 1.45 2.4065 -2 2 0 2 37.42 5.38 2.4033 -3 -2 1 2 38.63 2.50 2.3308 -3 0 2 2 38.94 4.44 2.3131 -2 2 2 2 41.49 3.07 2.1764 2 0 4 2 41.71 1.32 2.1655 3 2 3 2 43.01 12.31 2.1031 1 4 1 2 43.17 1.81 2.0958 2 -2 2 2 43.22 1.22 2.0935 -3 -3 1 2 43.95 5.10 2.0604 1 2 5 2 44.00 2.65 2.0581 3 0 3 2 44.02 2.01 2.0573 1 0 5 2 44.29 3.78 2.0450 0 -2 4 2 44.93 5.13 2.0174 2 4 0 2 45.01 1.06 2.0140 2 4 2 2 45.97 4.21 1.9742 0 4 2 2 46.00 3.63 1.9728 -3 -2 3 2 46.51 2.26 1.9527 -2 -2 4 2 46.91 4.29 1.9369 3 2 4 2 47.17 4.45 1.9267 2 2 5 2 47.22 1.52 1.9248 -1 2 5 2 47.26 4.80 1.9232 -2 2 4 2 47.35 1.48 1.9200 -2 -4 1 2 47.75 1.64 1.9048 -3 2 1 2 47.90 5.27 1.8990 4 2 2 2 47.99 6.35 1.8958 -4 0 1 2 48.01 5.11 1.8949 -2 0 5 2 48.02 5.00 1.8948 1 -2 4 2 48.25 4.81 1.8860 2 -2 3 2 48.55 2.02 1.8751 -3 0 4 2 49.07 1.08 1.8564 2 0 5 2 49.28 1.14 1.8490 3 4 2 2 49.70 4.94 1.8345 3 -2 1 2 50.26 2.71 1.8153 1 4 4 2 50.32 2.98 1.8134 -4 -2 2 2 50.35 1.23 1.8123 -1 -4 2 2 50.73 1.04 1.7997 4 3 2 2 51.06 2.06 1.7886 -1 4 2 2 51.18 1.90 1.7849 4 2 3 2 51.30 1.27 1.7810 -1 4 0 2 51.42 2.86 1.7772 2 4 4 2 51.66 3.77 1.7692 3 4 3 2 51.71 4.62 1.7677 -1 -2 5 2 51.88 5.49 1.7625 0 2 6 2 51.99 2.82 1.7588 -3 2 3 2 52.47 3.16 1.7439 0 -4 2 2 52.75 3.53 1.7354 1 0 6 2 52.91 1.79 1.7306 3 -2 2 2 53.64 4.25 1.7086 1 -4 1 2 54.84 2.65 1.6742 4 0 3 2 54.92 1.98 1.6719 -3 -4 2 2 55.29 2.40 1.6616 4 4 1 2 55.54 1.19 1.6547 -1 -4 3 2 56.14 1.63 1.6383 -2 0 6 2 56.28 1.45 1.6346 -2 -4 3 2 56.59 1.25 1.6264 3 0 5 2 56.68 1.43 1.6240 -1 4 4 2 57.09 2.73 1.6134 0 4 5 2 57.28 1.07 1.6084 2 0 6 2 57.68 2.82 1.5983 5 2 1 2 58.03 2.19 1.5894 -2 4 1 2 58.45 2.34 1.5791 -4 0 4 2 59.69 2.79 1.5490 -4 2 0 2 60.27 3.58 1.5356 0 0 7 2 60.35 1.55 1.5338 3 2 6 2 60.47 1.19 1.5310 -2 4 3 2 61.18 1.15 1.5148 -5 -2 2 2 61.43 1.55 1.5094 4 2 5 2 61.51 1.07 1.5075 2 -2 5 2 62.36 1.44 1.4889 -2 -2 6 2 62.93 1.64 1.4770 -1 2 7 2 63.00 1.29 1.4755 3 -2 4 2 63.09 1.70 1.4735 -4 2 3 2 63.45 2.54 1.4660 5 0 2 2 64.72 1.54 1.4403 5 4 0 2 65.63 1.19 1.4225 -3 -4 4 2 66.51 1.62 1.4059 -4 -2 5 2 67.18 1.72 1.3935 -1 4 6 2 67.89 1.91 1.3806 -3 2 6 2 68.03 1.47 1.3781 -3 4 2 2 68.16 1.07 1.3759 2 6 3 2 68.78 1.02 1.3649 3 6 2 2 68.83 1.51 1.3641 1 6 0 2 69.85 1.33 1.3465 2 4 7 2 70.16 1.01 1.3414 6 2 0 2 70.81 1.35 1.3306 -3 0 7 2 70.92 1.04 1.3289 -1 0 8 2 72.14 1.90 1.3093 2 2 8 2 72.83 1.52 1.2986 1 -2 7 2 73.74 1.05 1.2848 3 -4 2 2 75.22 1.18 1.2633 -5 0 5 2 76.78 1.25 1.2414 -3 4 5 2 76.79 1.59 1.2413 1 4 8 2 76.95 1.15 1.2391 -1 -4 6 2 78.40 1.19 1.2198 6 2 4 2 78.98 1.24 1.2122 -5 2 4 2 79.39 1.29 1.2070 1 2 9 2 79.69 1.14 1.2033 0 -2 8 2 80.57 1.40 1.1922 5 -2 3 2 81.69 1.05 1.1787 4 -4 1 2 85.55 1.01 1.1352 1 6 7 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.