Na[(UO2)4O2(OH)5](H2O)2 Burns P C, Deely K M The Canadian Mineralogist 40 (2002) 1579-1586 A topologically novel sheet of uranyl pentagonal bipyramids in the structure of Na[(UO2)4O2(OH)5](H2O)2 _database_code_amcsd 0005795 CELL PARAMETERS: 8.0746 8.4633 11.2191 80.398 87.492 71.308 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 716.036 Density (g/cm3): 5.822 MAX. ABS. INTENSITY / VOLUME**2: 168.4946527 RIR: 9.423 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.99 3.51 11.0613 0 0 1 2 11.18 2.04 7.9117 0 1 0 2 11.57 12.00 7.6483 1 0 0 2 14.01 3.39 6.3217 -1 0 1 2 14.15 100.00 6.2606 1 0 1 2 14.63 1.25 6.0532 1 1 1 2 16.03 3.03 5.5307 0 0 2 2 16.39 1.28 5.4090 -1 -1 1 2 19.52 1.20 4.5470 1 1 2 2 19.91 15.63 4.4597 1 0 2 2 22.37 1.37 3.9734 2 1 0 2 22.48 1.23 3.9559 0 2 0 2 23.26 1.01 3.8241 2 0 0 2 24.14 10.45 3.6871 0 0 3 2 24.42 35.89 3.6445 -1 -2 1 2 24.55 10.16 3.6259 -2 0 1 2 24.71 13.58 3.6027 2 0 1 2 24.93 3.30 3.5713 1 2 2 2 25.10 7.86 3.5477 0 -2 1 2 25.48 34.29 3.4956 0 2 2 2 26.73 26.49 3.3349 -1 0 3 2 26.78 22.81 3.3287 2 2 0 2 26.98 6.84 3.3053 2 2 1 2 28.23 21.40 3.1608 -2 0 2 2 28.51 5.66 3.1309 -1 2 0 2 28.51 3.84 3.1303 2 0 2 2 28.59 18.22 3.1225 -1 2 1 2 29.81 12.06 2.9967 0 -2 2 2 29.92 13.80 2.9862 1 2 3 2 30.91 1.25 2.8933 -1 2 2 2 31.85 2.04 2.8094 1 3 1 2 32.37 9.11 2.7653 0 0 4 2 33.12 3.47 2.7045 -2 -2 2 2 33.92 3.67 2.6431 2 2 3 2 33.95 5.44 2.6406 2 0 3 2 34.61 8.25 2.5920 1 0 4 2 34.74 6.21 2.5824 1 -2 2 2 35.20 7.80 2.5494 3 0 0 2 35.26 1.55 2.5455 0 3 2 2 35.48 1.88 2.5299 3 2 1 2 36.00 1.44 2.4950 2 3 2 2 36.07 3.51 2.4900 -3 0 1 2 37.53 4.63 2.3965 3 2 2 2 37.55 1.48 2.3951 -2 2 0 2 37.59 2.59 2.3931 -2 2 1 2 39.06 3.35 2.3062 3 0 2 2 39.31 3.22 2.2920 2 -2 1 2 40.04 2.59 2.2520 -2 0 4 2 40.41 2.16 2.2322 -3 -2 2 2 40.65 2.16 2.2197 -2 -3 2 2 41.90 1.14 2.1562 3 3 2 2 42.32 4.34 2.1355 -1 -2 4 2 42.42 2.08 2.1311 -1 0 5 2 42.55 1.05 2.1245 -3 -3 1 2 42.83 2.54 2.1116 -2 2 3 2 42.83 10.14 2.1113 1 4 1 2 42.92 1.05 2.1072 -3 0 3 2 43.53 2.60 2.0791 0 2 5 2 44.37 1.12 2.0416 2 4 0 2 44.78 4.44 2.0241 2 4 2 2 45.17 5.30 2.0073 -3 -2 3 2 45.21 5.04 2.0057 -2 -2 4 2 45.83 1.36 1.9798 4 2 1 2 45.88 3.27 1.9779 0 4 0 2 46.19 3.30 1.9653 3 2 4 2 46.31 2.52 1.9606 2 2 5 2 46.60 1.24 1.9489 1 -2 4 2 47.04 5.08 1.9319 -4 -2 1 2 47.06 5.90 1.9309 -1 2 5 2 47.29 1.14 1.9221 2 4 3 2 47.37 5.09 1.9192 2 -2 3 2 47.56 5.42 1.9118 -2 2 4 2 47.71 5.53 1.9064 2 0 5 2 48.22 2.73 1.8871 -3 2 0 2 48.30 1.64 1.8842 -3 0 4 2 48.39 4.77 1.8809 4 0 1 2 48.46 1.07 1.8786 3 4 0 2 48.84 1.83 1.8648 3 0 4 2 49.27 2.13 1.8494 -1 -4 2 2 49.71 4.32 1.8341 -3 2 2 2 49.85 1.70 1.8293 -4 -2 2 2 49.95 1.84 1.8258 -1 -2 5 2 50.00 1.44 1.8241 2 3 5 2 50.06 3.08 1.8223 -2 -4 2 2 50.41 4.81 1.8103 0 -2 5 2 50.45 2.92 1.8091 -3 -4 1 2 50.64 2.87 1.8027 4 2 3 2 50.82 2.24 1.7965 -1 0 6 2 50.96 3.25 1.7920 1 2 6 2 51.18 2.28 1.7850 0 2 6 2 51.25 2.59 1.7825 -1 4 0 2 51.26 1.03 1.7821 3 4 3 2 52.35 3.31 1.7478 0 4 4 2 52.55 2.05 1.7415 3 -2 2 2 52.57 1.24 1.7407 -3 2 3 2 52.96 1.41 1.7290 4 3 3 2 53.70 2.88 1.7068 -1 4 3 2 53.78 3.30 1.7047 -4 0 3 2 54.08 1.16 1.6957 -1 -4 3 2 54.27 1.60 1.6902 4 0 3 2 54.65 1.83 1.6795 -3 0 5 2 54.72 1.89 1.6774 4 4 1 2 54.94 1.48 1.6712 3 4 4 2 55.08 2.14 1.6674 -2 0 6 2 55.31 1.83 1.6611 1 4 5 2 55.33 1.23 1.6605 2 5 0 2 56.21 2.54 1.6364 0 -4 3 2 57.24 1.24 1.6094 3 5 1 2 57.25 2.59 1.6091 5 2 0 2 57.74 1.53 1.5967 -3 -2 5 2 58.28 1.01 1.5831 -3 -4 3 2 58.40 3.47 1.5802 0 0 7 2 58.44 1.28 1.5792 -2 4 1 2 59.02 1.69 1.5651 4 0 4 2 60.05 2.10 1.5406 -4 2 1 2 60.85 1.45 1.5224 2 -4 1 2 61.66 2.38 1.5042 1 -2 6 2 61.70 1.76 1.5033 2 2 7 2 61.82 1.24 1.5007 3 -2 4 2 62.47 1.22 1.4866 3 0 6 2 62.87 2.41 1.4783 -5 0 2 2 63.88 1.51 1.4572 4 -2 2 2 64.45 1.34 1.4457 5 4 2 2 66.48 1.81 1.4065 1 -4 4 2 66.75 1.19 1.4014 4 2 6 2 67.97 1.45 1.3792 3 -2 5 2 68.80 1.07 1.3646 1 6 3 2 68.94 1.27 1.3622 -2 -2 7 2 69.13 1.32 1.3589 -5 -2 4 2 69.17 1.43 1.3581 1 0 8 2 72.19 1.38 1.3085 -4 2 5 2 74.18 1.45 1.2783 -1 -4 6 2 76.00 1.12 1.2521 5 0 5 2 76.17 1.49 1.2499 -1 -2 8 2 76.47 1.29 1.2456 -6 -2 3 2 76.93 1.11 1.2393 6 0 2 2 77.52 1.11 1.2314 0 2 9 2 79.83 1.34 1.2015 -5 2 4 2 80.04 1.30 1.1989 5 -2 3 2 88.03 1.12 1.1095 -6 0 5 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.