Na13-xTl3+x[(UO2)(MoO4)3]4(H2O)6+x (x=0.1) Krivovichev S V, Burns P C The Canadian Mineralogist 41 (2003) 707-719 Crystal chemistry of uranyl molybdates. VIII. Crystal structures of Na3Tl3[(UO2)(MoO4)4], Na13-xTl3+x[(UO2)(MoO4)3]4(H2O)6+x (x=0.1), Na3Tl5[(UO2)(MoO4)2]2(H2O)3 and Na2[(UO2)(MoO4)2](H2O)4 Sample 2 _database_code_amcsd 0005856 19.7942 7.1913 22.8835 90 97.828 90 P2/c atom x y z occ Uiso U(1,1) U(2,2) U(3,3) U(1,2) U(1,3) U(2,3) U(1) .30498 .32356 .14435 .0119 .0121 .0133 .0103 .00111 .0020 .0001 U(2) -.18434 -.34747 .13618 .0134 .0116 .0173 .0114 -.00128 .0021 .0007 Tl(1) .48894 .52392 .09434 .0282 .0269 .0255 .0314 -.0022 .0008 -.0053 Tl(2) 0 -.67522 .25 .70 .0255 .0247 .0343 .0201 0 .0122 0 Tl(3) -.21575 .1447 .07311 .20 .0164 .0186 .0156 .0159 .0048 .006 .003 Mo(1) .14674 .31323 .02706 .0134 .0150 .0150 .0105 .0013 .0025 .0006 Mo(2) .67240 .34437 .18297 .0130 .0150 .0122 .0113 -.0023 -.0002 .0000 Mo(3) .44974 .02633 .11037 .0153 .0145 .0174 .0147 .0034 .0048 .0001 Mo(4) .65040 .62143 .02228 .0126 .0131 .0142 .0104 -.0005 .0017 .0003 Mo(5) -.14739 -.42124 .31123 .0151 .0177 .0153 .0119 -.0028 .0000 .0013 Mo(6) -.03768 -.02770 .11189 .0183 .0192 .0162 .0208 -.0042 .0078 -.0014 Na(1) .0978 -.1927 .0406 .0285 .032 .020 .033 -.002 .003 -.002 Na(2) .4007 -.1270 -.0321 .0243 .028 .019 .026 .006 .002 .004 Na(3) .6297 .8592 .1612 .0213 .029 .020 .015 -.005 .002 -.004 Na(4) -.0131 .4540 .0761 .0237 .024 .029 .019 -.009 .006 .003 Na(5) -.1410 -.9132 .3305 .0281 .035 .025 .025 -.001 .005 .003 Na(6) .5 -.2392 .25 .90 .029 .040 .040 .006 0 .002 0 Na(7) .2700 -.2046 .0867 .069 .096 .045 .075 -.009 .040 -.003 O(1) .5876 .4527 .0203 .026 .017 .023 .038 -.008 -.005 -.004 O(2) .1189 .1294 .0654 .027 .043 .016 .024 -.016 .017 -.004 O(3) .2716 .0931 .1360 .015 .017 .013 .014 -.002 .005 -.002 O(4) -.1194 -.5088 .1212 .025 .024 .026 .028 -.002 .008 .009 O(5) .2167 .4258 .0714 .022 .022 .027 .017 -.001 .000 -.003 O(6) .0821 .4792 .0153 .017 .014 .026 .011 .006 .000 .001 O(7) .4144 .1953 .1577 .021 .015 .030 .017 .012 .000 -.007 O(8) .6438 .1692 .1350 .025 .032 .014 .025 -.007 -.004 -.006 O(9) .3894 -.1198 .0737 .026 .027 .027 .024 -.006 .004 -.013 O(10) .1700 .2251 -.0383 .022 .030 .030 .006 -.010 .001 .000 O(11) .7585 .4047 .1769 .020 .025 .016 .018 -.001 .000 .003 O(12) .3382 .5570 .1529 .022 .032 .023 .011 -.003 -.002 .004 O(13) .7281 .5315 .0596 .023 .028 .025 .017 .002 .005 .006 O(14) -.1074 -.1107 .1471 .022 .021 .024 .023 -.011 .006 .005 O(15) .6192 .5394 .1687 .028 .021 .013 .046 .000 -.010 .004 O(16) .6558 .6810 -.0549 .026 .015 .047 .016 .004 .004 .002 O(17) .6231 .8149 .0579 .026 .034 .025 .015 .003 -.008 .000 O(18) -.2476 -.1854 .1518 .024 .018 .023 .032 -.001 .008 .003 O(19) -.0022 -.2106 .0750 .023 .021 .019 .029 .007 .001 -.004 O(20) -.2108 -.5942 .3118 .029 .032 .039 .022 -.012 .022 -.004 O(21) .5076 -.1155 .1560 .028 .026 .026 .031 .009 .007 .003 O(22) .6631 .2655 .2563 .022 .020 .035 .011 -.011 .005 .000 O(23) -.1409 -.3551 .2393 .033 .031 .044 .023 -.026 -.001 .005 O(24) .4917 .1393 .0618 .031 .029 .036 .030 .007 .016 .003 O(25) -.0717 -.5190 .3427 .034 .029 .038 .027 .008 -.019 -.002 O(26) -.0623 .1481 .0601 .039 .062 .012 .046 .010 .019 .009 Wat(27) .6198 .8621 .2644 .034 .043 .040 .020 .004 .005 -.005 Wat(28) -.1408 -.8512 .2334 .038 .045 .039 .025 .014 -.008 -.011 O(29) -.1650 -.2333 .3554 .034 .037 .027 .037 .005 -.003 -.007 O(30) .0228 .0648 .1631 .048 .030 .061 .052 -.031 .002 -.016 Wat(31) .5 -.572 .25 .80 .050 .039 .063 .043 0 -.013 0 Wat(32) -.2158 .176 .0042 .058