Na2[(UO2)(MoO4)2](H2O)4 Krivovichev S V, Burns P C The Canadian Mineralogist 41 (2003) 707-719 Crystal chemistry of uranyl molybdates. VIII. Crystal structures of Na3Tl3[(UO2)(MoO4)4], Na13-xTl3+x[(UO2)(MoO4)3]4(H2O)6+x (x=0.1), Na3Tl5[(UO2)(MoO4)2]2(H2O)3 and Na2[(UO2)(MoO4)2](H2O)4 Sample 4 _database_code_amcsd 0005858 CELL PARAMETERS: 8.9023 11.5149 13.8151 90.000 107.743 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 1348.810 Density (g/cm3): 3.508 MAX. ABS. INTENSITY / VOLUME**2: 62.39222825 RIR: 5.792 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.21 1.96 8.6653 0 1 1 4 10.55 100.00 8.3851 -1 0 1 2 12.97 33.79 6.8276 1 1 0 4 13.46 2.03 6.5790 0 0 2 2 14.04 11.54 6.3058 1 0 1 2 15.39 2.56 5.7575 0 2 0 2 15.51 21.23 5.7124 0 1 2 4 16.02 13.68 5.5308 1 1 1 4 16.81 2.08 5.2746 0 2 1 4 18.63 1.41 4.7631 1 2 0 4 18.70 19.67 4.7463 -1 2 1 4 19.75 3.36 4.4945 -1 0 3 2 20.50 2.18 4.3326 0 2 2 4 20.95 8.02 4.2394 2 0 0 2 21.19 11.91 4.1925 -2 0 2 2 21.22 9.93 4.1869 -1 1 3 4 21.41 15.37 4.1512 -2 1 1 4 22.35 2.88 3.9784 2 1 0 4 22.57 3.63 3.9395 -2 1 2 4 24.15 13.75 3.6847 0 3 1 4 24.88 3.58 3.5781 1 2 2 4 25.14 6.30 3.5428 -1 2 3 4 25.17 5.06 3.5381 2 1 1 4 25.52 3.53 3.4900 -1 3 1 4 25.55 7.54 3.4861 1 0 3 2 25.57 8.48 3.4840 -2 1 3 4 26.10 3.79 3.4138 2 2 0 4 26.30 22.94 3.3892 -2 2 2 4 26.72 6.52 3.3366 1 1 3 4 26.89 13.43 3.3153 0 3 2 4 27.05 1.83 3.2966 -1 1 4 4 27.11 16.29 3.2895 0 0 4 2 27.20 16.61 3.2787 1 3 1 4 27.34 14.85 3.2623 -1 3 2 4 28.21 13.53 3.1630 0 1 4 4 28.58 4.95 3.1233 2 2 1 4 29.37 11.48 3.0410 2 1 2 4 29.89 2.51 2.9895 -2 1 4 4 29.96 2.46 2.9821 1 2 3 4 30.42 8.75 2.9384 1 3 2 4 30.63 10.60 2.9188 -1 3 3 4 30.96 7.50 2.8884 0 3 3 4 31.07 1.16 2.8787 0 4 0 2 31.26 1.62 2.8616 -3 1 1 4 31.44 5.16 2.8454 2 3 0 4 31.82 2.36 2.8122 0 4 1 4 32.02 4.29 2.7950 -3 0 3 2 32.37 3.43 2.7654 2 2 2 4 32.40 3.40 2.7630 -1 0 5 2 32.62 3.59 2.7448 3 1 0 4 32.86 2.15 2.7259 1 4 0 4 32.98 2.31 2.7162 -3 1 3 4 33.35 1.88 2.6867 -1 1 5 4 33.56 1.68 2.6705 2 3 1 4 33.99 1.42 2.6373 0 4 2 4 34.11 5.48 2.6285 -3 2 1 4 34.24 2.46 2.6187 1 4 1 4 34.50 2.50 2.5999 2 1 3 4 34.76 1.05 2.5806 1 3 3 4 35.09 2.27 2.5570 -2 1 5 4 35.33 3.46 2.5408 3 1 1 4 35.71 1.43 2.5144 -3 2 3 4 35.73 2.20 2.5130 1 2 4 4 35.87 3.36 2.5032 -3 1 4 4 36.06 3.06 2.4910 -1 2 5 4 36.89 1.07 2.4363 2 3 2 4 37.20 6.49 2.4171 -2 4 1 4 37.32 3.48 2.4096 -2 3 4 4 37.58 3.29 2.3934 0 2 5 4 38.80 1.06 2.3210 1 0 5 2 39.61 1.31 2.2753 1 1 5 4 39.83 1.59 2.2635 -3 1 5 4 39.86 1.16 2.2616 -2 4 3 4 39.90 2.43 2.2595 -3 3 3 4 40.87 1.04 2.2079 -1 4 4 4 40.92 1.04 2.2056 -2 1 6 4 41.20 1.56 2.1912 2 3 3 4 41.69 1.09 2.1663 0 4 4 4 41.76 1.55 2.1632 1 5 1 4 41.94 1.29 2.1543 0 1 6 4 41.97 3.76 2.1527 1 2 5 4 42.32 3.01 2.1357 -1 2 6 4 42.59 1.92 2.1227 2 2 4 4 43.15 3.27 2.0963 -4 0 4 2 43.22 3.00 2.0934 -2 2 6 4 43.41 3.59 2.0847 4 1 0 4 43.61 4.87 2.0756 -4 2 2 4 44.01 3.07 2.0577 -3 4 2 4 44.04 1.23 2.0563 1 5 2 4 44.19 1.42 2.0494 0 2 6 4 44.43 1.19 2.0390 0 5 3 4 44.79 1.38 2.0237 2 5 0 4 45.23 1.40 2.0046 1 4 4 4 45.87 2.06 1.9783 -3 3 5 4 45.96 4.84 1.9745 3 2 3 4 46.38 2.82 1.9578 2 5 1 4 46.40 1.87 1.9571 2 4 3 4 46.61 1.67 1.9485 -2 5 3 4 46.77 1.37 1.9423 0 4 5 4 46.86 1.03 1.9386 -2 4 5 4 47.20 1.09 1.9255 -2 1 7 4 47.21 2.21 1.9251 -4 3 2 4 47.51 2.81 1.9138 -1 5 4 4 47.63 2.10 1.9091 -4 3 1 4 47.90 3.27 1.8991 0 6 1 4 48.59 1.10 1.8739 1 2 6 4 48.59 1.41 1.8737 2 2 5 4 48.64 4.09 1.8718 1 6 0 4 48.95 3.83 1.8606 -1 2 7 4 49.10 1.10 1.8556 4 3 0 4 49.32 1.11 1.8477 -2 5 4 4 49.37 1.60 1.8459 -3 0 7 2 49.55 1.13 1.8398 -4 3 4 4 49.74 1.02 1.8331 -1 6 2 4 50.11 1.34 1.8205 3 4 2 4 50.19 1.08 1.8177 -3 3 6 4 50.51 4.56 1.8069 1 4 5 4 50.81 1.22 1.7968 -1 4 6 4 51.05 1.81 1.7891 2 4 4 4 51.16 1.82 1.7853 3 5 0 4 51.52 1.97 1.7739 -5 0 3 2 51.67 2.85 1.7690 4 2 2 4 51.88 2.74 1.7623 -2 6 1 4 51.93 1.03 1.7609 1 3 6 4 52.01 1.40 1.7582 0 6 3 4 52.03 1.67 1.7578 -3 2 7 4 52.19 1.96 1.7526 -4 3 5 4 52.54 1.19 1.7417 -4 4 3 4 52.83 1.15 1.7331 0 5 5 4 52.89 1.90 1.7310 -5 1 1 4 52.91 2.75 1.7304 -2 5 5 4 53.14 2.79 1.7234 2 1 6 4 53.48 1.23 1.7135 -3 5 4 4 53.66 2.71 1.7082 1 1 7 4 53.88 1.19 1.7014 -2 1 8 4 53.97 1.04 1.6991 -5 2 2 4 54.73 1.28 1.6770 -5 0 5 2 54.77 1.50 1.6761 -1 6 4 4 55.03 2.50 1.6688 3 1 5 4 55.36 1.30 1.6595 -5 1 5 4 55.70 2.06 1.6501 -4 3 6 4 55.90 2.06 1.6448 3 5 2 4 56.03 1.42 1.6412 -3 1 8 4 56.52 2.10 1.6282 0 1 8 4 56.98 1.37 1.6162 -2 4 7 4 57.08 1.83 1.6135 -5 3 2 4 57.32 1.24 1.6074 -3 6 2 4 58.01 1.02 1.5898 -1 7 2 4 58.34 1.54 1.5818 1 6 4 4 59.15 1.18 1.5619 4 1 4 4 59.74 1.28 1.5478 -4 0 8 2 59.75 1.16 1.5477 1 7 2 4 60.07 1.39 1.5402 0 7 3 4 60.22 1.08 1.5367 -5 3 5 4 60.93 1.05 1.5205 4 2 4 4 61.41 2.25 1.5097 4 5 1 4 61.52 1.54 1.5073 -1 1 9 4 63.02 1.39 1.4750 -5 3 6 4 63.49 1.27 1.4651 -6 1 2 4 63.94 1.07 1.4560 3 5 4 4 64.60 1.58 1.4426 -4 6 3 4 66.18 1.20 1.4121 5 4 1 4 68.17 1.19 1.3757 -1 5 8 4 73.50 1.08 1.2884 -5 6 4 4 74.30 1.30 1.2765 -2 5 9 4 77.89 1.06 1.2265 4 5 5 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.