Cs2[(UO2)(PO4)]2(H2O)5 Locock A J, Burns P C, Duke M J M, Flynn T M The Canadian Mineralogist 42 (2004) 973-996 Monovalent cations in structures of the meta-autunite group Sample: CsUP _database_code_amcsd 0005953 CELL PARAMETERS: 9.8716 9.9550 17.6465 90.000 90.402 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 1734.110 Density (g/cm3): 4.200 MAX. ABS. INTENSITY / VOLUME**2: 36.39782413 RIR: 2.822 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.03 96.51 8.8230 0 0 2 2 10.20 1.19 8.6704 0 1 1 4 10.30 6.08 8.5894 1 0 1 2 12.63 2.64 7.0095 1 1 0 4 13.57 1.15 6.5255 -1 1 1 4 13.62 3.23 6.5033 1 1 1 4 16.11 57.18 5.5017 -1 1 2 4 16.19 18.97 5.4750 1 1 2 4 17.50 1.39 5.0686 -1 0 3 2 17.51 1.28 5.0641 0 1 3 4 17.61 7.00 5.0375 1 0 3 2 17.82 37.04 4.9775 0 2 0 2 17.97 52.25 4.9357 2 0 0 2 18.52 12.29 4.7906 0 2 1 4 19.65 3.83 4.5169 -1 1 3 4 19.75 4.23 4.4948 1 1 3 4 20.08 6.43 4.4220 2 1 0 4 20.13 25.25 4.4115 0 0 4 2 20.49 48.57 4.3352 0 2 2 4 20.56 11.66 4.3204 -2 0 2 2 20.59 3.53 4.3131 -1 2 1 4 20.62 3.82 4.3066 1 2 1 4 20.68 7.40 4.2958 -2 1 1 4 20.68 19.00 4.2947 2 0 2 2 20.74 2.80 4.2830 2 1 1 4 22.37 2.10 3.9743 -1 2 2 4 22.43 2.37 3.9643 1 2 2 4 22.43 10.90 3.9633 -2 1 2 4 23.41 3.42 3.7996 0 2 3 4 23.78 97.75 3.7420 -1 1 4 4 23.89 100.00 3.7253 1 1 4 4 25.12 5.57 3.5453 -2 1 3 4 25.41 75.53 3.5047 2 2 0 4 26.77 1.24 3.3306 -1 0 5 2 26.80 1.64 3.3264 0 1 5 4 26.89 2.27 3.3158 1 0 5 2 27.33 53.97 3.2628 -2 2 2 4 27.43 93.71 3.2516 2 2 2 4 27.54 1.73 3.2388 -3 0 1 2 27.61 5.83 3.2306 3 0 1 2 28.25 3.25 3.1585 -1 1 5 4 28.37 2.08 3.1459 1 1 5 4 28.46 1.87 3.1360 -1 2 4 4 28.49 6.04 3.1330 -2 1 4 4 28.55 4.03 3.1261 1 2 4 4 28.57 1.08 3.1242 3 1 0 4 28.67 1.96 3.1133 2 1 4 4 28.74 5.47 3.1059 0 3 2 4 28.82 2.04 3.0978 -1 3 1 4 28.84 3.86 3.0954 1 3 1 4 28.99 2.55 3.0799 -3 1 1 4 29.06 1.90 3.0729 3 1 1 4 30.14 27.89 2.9648 -1 3 2 4 30.19 11.80 2.9606 1 3 2 4 30.28 21.98 2.9512 -3 1 2 4 30.42 16.32 2.9389 3 1 2 4 31.24 5.05 2.8631 3 0 3 2 32.51 1.29 2.7538 2 3 0 4 32.55 9.97 2.7508 -2 2 4 4 32.62 5.66 2.7449 3 2 0 4 32.71 1.42 2.7375 2 2 4 4 32.90 2.25 2.7225 -2 3 1 4 32.97 9.94 2.7168 -1 1 6 4 33.09 17.57 2.7072 1 1 6 4 33.80 5.05 2.6519 0 3 4 4 34.15 1.51 2.6253 -3 2 2 4 34.27 3.75 2.6166 3 2 2 4 35.00 3.62 2.5638 -1 3 4 4 35.08 3.42 2.5584 1 3 4 4 35.09 5.00 2.5576 -3 1 4 4 35.31 2.57 2.5416 3 1 4 4 35.42 2.11 2.5343 -2 0 6 2 35.45 2.46 2.5320 0 2 6 4 35.65 1.16 2.5187 2 0 6 2 35.95 1.91 2.4978 -2 3 3 4 36.09 7.93 2.4887 0 4 0 2 36.41 8.28 2.4678 4 0 0 2 36.69 1.43 2.4491 1 2 6 4 36.81 2.23 2.4418 2 1 6 4 37.23 1.36 2.4152 -3 0 5 2 37.26 2.52 2.4132 1 4 0 4 37.55 23.29 2.3953 0 4 2 4 37.78 14.23 2.3810 -4 0 2 2 37.87 1.45 2.3759 -1 1 7 4 37.93 7.47 2.3723 4 0 2 2 38.66 3.70 2.3288 -1 4 2 4 38.70 1.22 2.3267 1 4 2 4 39.86 16.40 2.2614 -3 3 2 4 39.92 3.45 2.2584 -2 2 6 4 39.97 4.24 2.2559 3 3 2 4 40.60 25.03 2.2222 2 4 0 4 40.81 15.64 2.2110 4 2 0 4 40.91 19.19 2.2058 0 0 8 2 40.95 1.76 2.2039 2 4 1 4 41.01 3.15 2.2010 0 3 6 4 41.34 1.80 2.1841 2 1 7 4 41.52 1.53 2.1752 -3 3 3 4 41.67 1.97 2.1676 0 4 4 4 41.68 1.23 2.1670 2 3 5 4 41.89 6.45 2.1565 -2 4 2 4 41.96 6.58 2.1533 2 4 2 4 42.01 14.68 2.1506 -1 3 6 4 42.05 13.09 2.1486 -3 1 6 4 42.07 8.51 2.1479 -4 2 2 4 42.08 4.70 2.1473 4 0 4 2 42.11 16.66 2.1458 1 3 6 4 42.20 12.30 2.1415 4 2 2 4 42.35 14.32 2.1344 3 1 6 4 42.92 10.96 2.1070 -1 1 8 4 43.05 7.37 2.1010 1 1 8 4 43.58 1.87 2.0766 2 4 3 4 43.64 1.34 2.0739 -4 2 3 4 43.75 15.56 2.0690 -3 3 4 4 43.83 1.02 2.0653 4 2 3 4 43.94 16.84 2.0605 3 3 4 4 44.89 4.65 2.0191 -2 0 8 2 44.95 7.18 2.0166 0 2 8 4 45.05 1.00 2.0126 -3 2 6 4 45.14 3.45 2.0086 2 0 8 2 45.16 1.62 2.0079 -3 0 7 2 45.78 1.40 1.9821 2 4 4 4 45.82 1.03 1.9802 4 3 0 4 46.10 1.18 1.9689 2 1 8 4 46.92 2.18 1.9366 5 1 0 4 47.09 1.24 1.9299 4 3 2 4 47.18 1.49 1.9264 -5 1 1 4 47.25 1.10 1.9236 5 1 1 4 47.71 1.89 1.9062 -1 5 2 4 47.74 5.64 1.9051 1 5 2 4 48.03 2.84 1.8943 -5 1 2 4 48.18 3.57 1.8888 5 1 2 4 48.26 1.20 1.8859 0 5 3 4 48.45 1.25 1.8790 -4 2 5 4 48.48 1.30 1.8778 2 4 5 4 48.67 2.42 1.8710 -2 2 8 4 48.90 3.52 1.8626 2 2 8 4 49.72 9.33 1.8339 -3 3 6 4 49.97 11.80 1.8250 3 3 6 4 50.48 2.46 1.8078 -1 3 8 4 50.49 1.71 1.8076 -3 1 8 4 50.60 1.13 1.8041 1 3 8 4 50.83 3.60 1.7963 3 1 8 4 51.15 8.53 1.7857 -1 5 4 4 51.21 6.70 1.7839 1 5 4 4 51.40 9.58 1.7777 -5 1 4 4 51.56 2.77 1.7726 -4 2 6 4 51.68 5.55 1.7688 5 1 4 4 51.81 1.47 1.7646 0 0 10 2 52.20 16.38 1.7524 4 4 0 4 53.11 1.38 1.7243 -3 2 8 4 53.24 4.73 1.7204 -4 4 2 4 53.35 7.34 1.7172 4 4 2 4 55.06 4.29 1.6680 -5 3 2 4 55.15 3.09 1.6653 -2 0 10 2 55.23 9.71 1.6632 0 2 10 4 55.37 4.13 1.6592 0 6 0 2 55.42 4.54 1.6579 2 0 10 2 55.70 1.23 1.6503 -4 0 8 2 55.88 5.73 1.6452 6 0 0 2 56.40 1.02 1.6314 -4 4 4 4 56.43 5.16 1.6306 0 6 2 4 56.56 4.69 1.6272 -1 5 6 4 56.61 1.67 1.6258 4 4 4 4 56.64 3.52 1.6252 1 5 6 4 56.74 4.83 1.6225 -5 1 6 4 56.86 1.72 1.6194 -6 0 2 2 57.01 1.47 1.6153 6 0 2 2 57.13 3.69 1.6123 5 1 6 4 57.30 3.04 1.6079 -3 3 8 4 57.61 3.09 1.6000 3 3 8 4 57.96 8.74 1.5910 -3 5 4 4 58.12 5.76 1.5871 3 5 4 4 58.13 3.29 1.5868 -5 3 4 4 58.39 3.44 1.5804 5 3 4 4 58.44 7.46 1.5793 -2 2 10 4 58.70 7.44 1.5730 2 2 10 4 58.71 9.14 1.5727 2 6 0 4 58.90 7.24 1.5680 -2 4 8 4 58.96 4.09 1.5665 -4 2 8 4 59.11 4.98 1.5630 2 4 8 4 59.14 8.99 1.5621 6 2 0 4 59.37 4.01 1.5567 4 2 8 4 59.70 4.09 1.5489 -2 6 2 4 59.75 1.61 1.5477 2 6 2 4 60.08 1.48 1.5399 -6 2 2 4 60.17 1.05 1.5380 6 0 4 2 60.23 3.66 1.5364 6 2 2 4 62.77 2.89 1.4803 2 6 4 4 62.96 1.09 1.4764 -3 5 6 4 63.09 2.14 1.4735 -5 3 6 4 63.24 3.10 1.4705 0 0 12 2 63.29 1.03 1.4694 6 2 4 4 63.46 3.04 1.4658 5 3 6 4 63.61 1.09 1.4627 -1 5 8 4 63.71 4.16 1.4607 1 5 8 4 64.22 4.21 1.4503 5 1 8 4 64.71 1.90 1.4406 -1 1 12 4 64.73 2.10 1.4402 -4 0 10 2 64.76 4.17 1.4395 0 4 10 4 64.85 2.03 1.4377 1 1 12 4 65.21 1.71 1.4307 4 0 10 2 66.18 2.01 1.4120 -2 0 12 2 66.28 2.46 1.4102 0 2 12 4 66.47 1.68 1.4066 2 0 12 2 67.36 1.35 1.3902 -1 7 2 4 67.38 2.25 1.3898 1 7 2 4 67.61 2.24 1.3856 -5 5 2 4 67.70 4.51 1.3840 -2 4 10 4 67.73 1.05 1.3835 5 5 2 4 67.73 6.32 1.3834 -4 2 10 4 67.89 2.18 1.3806 -7 1 2 4 67.93 4.09 1.3798 2 4 10 4 68.10 3.23 1.3769 4 6 0 4 68.18 2.56 1.3754 -4 4 8 4 68.20 4.94 1.3750 4 2 10 4 68.35 1.21 1.3724 6 4 0 4 68.56 1.96 1.3688 4 4 8 4 69.08 1.26 1.3596 4 6 2 4 69.15 1.82 1.3584 -2 2 12 4 69.22 1.42 1.3573 -6 4 2 4 69.36 2.41 1.3549 6 4 2 4 69.72 1.04 1.3488 -5 3 8 4 69.89 2.64 1.3458 3 5 8 4 70.16 1.90 1.3414 -1 7 4 4 70.19 1.34 1.3409 5 3 8 4 70.21 1.61 1.3406 1 7 4 4 70.36 2.01 1.3380 -5 5 4 4 70.60 1.26 1.3341 5 5 4 4 70.62 3.48 1.3338 -7 1 4 4 70.94 2.41 1.3285 7 1 4 4 71.10 2.69 1.3259 0 6 8 4 71.27 3.05 1.3232 -6 0 8 2 71.82 1.22 1.3144 6 0 8 2 73.71 1.41 1.2852 -7 3 2 4 73.94 1.93 1.2819 -2 6 8 4 74.15 1.53 1.2788 -6 2 8 4 74.69 1.21 1.2708 6 2 8 4 74.74 3.47 1.2702 -1 7 6 4 74.81 2.35 1.2692 1 7 6 4 74.89 2.04 1.2679 -5 5 6 4 75.11 1.31 1.2647 -7 1 6 4 75.23 3.05 1.2630 5 5 6 4 75.59 2.27 1.2579 7 1 6 4 75.96 1.44 1.2527 -3 7 4 4 76.10 1.49 1.2508 3 7 4 4 76.35 1.83 1.2473 -7 3 4 4 76.41 1.75 1.2465 -4 4 10 4 76.56 1.05 1.2444 0 8 0 2 76.67 1.46 1.2429 7 3 4 4 76.86 1.87 1.2403 4 4 10 4 76.92 1.19 1.2395 1 1 14 4 77.46 2.45 1.2322 0 8 2 4 77.77 2.15 1.2281 -2 4 12 4 77.77 1.66 1.2280 -4 2 12 4 78.03 2.81 1.2245 2 4 12 4 78.31 2.46 1.2209 4 2 12 4 78.32 1.79 1.2209 8 0 2 2 79.25 3.95 1.2088 0 6 10 4 79.35 1.52 1.2076 -6 0 10 2 79.42 1.37 1.2066 2 8 0 4 80.01 1.40 1.1992 6 0 10 2 80.13 2.24 1.1977 8 2 0 4 80.29 1.35 1.1958 -2 8 2 4 80.33 1.52 1.1952 2 8 2 4 80.40 1.04 1.1944 -3 7 6 4 80.60 1.28 1.1919 3 7 6 4 81.08 1.13 1.1860 1 7 8 4 81.11 1.33 1.1857 8 2 2 4 81.20 1.15 1.1846 7 3 6 4 81.92 1.23 1.1761 7 1 8 4 81.97 1.14 1.1754 -2 6 10 4 82.00 1.42 1.1750 -5 1 12 4 82.13 1.02 1.1735 -6 2 10 4 82.30 1.62 1.1716 -3 1 14 4 82.36 1.79 1.1709 -1 3 14 4 82.43 1.98 1.1701 -4 6 8 4 82.51 1.47 1.1691 1 3 14 4 82.58 2.15 1.1682 6 6 0 4 82.76 1.53 1.1662 3 1 14 4 82.78 1.24 1.1660 4 6 8 4 83.40 2.35 1.1589 -6 6 2 4 83.53 3.08 1.1574 6 6 2 4 84.66 1.58 1.1448 -5 7 2 4 84.92 1.15 1.1420 -7 5 2 4 86.11 1.09 1.1292 -4 4 12 4 86.64 1.16 1.1237 4 4 12 4 87.24 1.44 1.1175 -5 7 4 4 87.46 1.21 1.1153 5 7 4 4 87.47 1.28 1.1151 -3 5 12 4 87.82 1.88 1.1116 -3 3 14 4 87.87 2.16 1.1111 4 8 0 4 88.28 1.11 1.1070 3 3 14 4 88.43 2.22 1.1055 8 4 0 4 88.79 2.13 1.1020 4 8 2 4 88.94 1.87 1.1005 0 6 12 4 89.22 1.08 1.0978 -8 4 2 4 89.39 1.48 1.0961 8 4 2 4 89.75 1.23 1.0926 6 0 12 2 89.99 1.89 1.0903 -1 1 16 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.