Co0.75K0.5SU2O13H6 Peeters O M, Vochten R, Blaton N The Canadian Mineralogist 46 (2008) 173-182 The crystal structures of synthetic potassium - transition-metal zippeite-group phases Sample: K-Co _database_code_amcsd 0006163 CELL PARAMETERS: 8.6510 14.1880 17.7130 90.000 104.140 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 2108.229 Density (g/cm3): 4.914 MAX. ABS. INTENSITY / VOLUME**2: 143.1801574 RIR: 9.488 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.30 21.89 8.5882 0 0 2 2 12.48 100.00 7.0940 0 2 0 2 14.27 1.70 6.2068 1 1 1 4 16.21 16.80 5.4694 0 2 2 4 20.68 8.53 4.2941 0 0 4 2 21.18 5.67 4.1946 -2 0 2 2 21.18 6.60 4.1944 2 0 0 2 21.57 2.87 4.1198 -1 3 1 4 22.79 7.56 3.9014 1 3 1 4 24.23 5.02 3.6735 0 2 4 4 24.66 6.39 3.6107 -2 2 2 4 24.66 5.03 3.6105 2 2 0 4 25.07 4.22 3.5522 -1 3 3 4 25.11 29.48 3.5470 0 4 0 2 25.81 25.20 3.4514 -2 0 4 2 25.82 26.66 3.4511 2 0 2 2 27.20 3.86 3.2784 0 4 2 4 28.77 33.66 3.1036 -2 2 4 4 28.77 32.31 3.1034 2 2 2 4 31.24 15.72 2.8627 0 0 6 2 31.85 2.74 2.8093 -1 3 5 4 32.75 2.67 2.7347 0 4 4 4 33.07 1.62 2.7085 -2 4 2 4 33.07 2.01 2.7084 2 4 0 4 33.30 1.08 2.6902 -2 0 6 2 33.31 1.98 2.6900 2 0 4 2 33.76 19.88 2.6547 0 2 6 4 34.16 4.47 2.6245 1 5 1 4 35.69 1.48 2.5154 -2 2 6 4 36.10 1.55 2.4881 -1 1 7 4 36.32 8.85 2.4736 -2 4 4 4 36.32 9.93 2.4735 2 4 2 4 38.05 2.23 2.3647 0 6 0 2 39.53 2.82 2.2798 0 6 2 4 40.49 9.63 2.2277 0 4 6 4 40.98 1.29 2.2023 -1 5 5 4 41.01 1.22 2.2007 -3 3 5 4 41.77 9.19 2.1628 -4 0 2 2 42.09 1.03 2.1470 0 0 8 2 42.16 1.07 2.1433 2 4 4 4 42.35 3.20 2.1344 -2 0 8 2 42.35 2.33 2.1342 2 0 6 2 43.13 1.52 2.0973 -4 0 4 2 43.13 1.41 2.0972 4 0 0 2 43.75 1.87 2.0689 3 3 3 4 43.76 7.67 2.0687 -4 2 2 4 43.96 1.08 2.0599 -2 6 2 4 44.07 2.53 2.0550 0 2 8 4 44.32 1.61 2.0439 -2 2 8 4 44.32 2.50 2.0437 2 2 6 4 45.08 2.34 2.0113 -4 2 4 4 45.08 3.09 2.0112 4 2 0 4 45.22 1.63 2.0051 1 3 7 4 45.54 1.98 1.9918 -3 5 3 4 46.07 1.45 1.9702 -1 7 1 4 46.56 5.09 1.9507 -2 6 4 4 46.56 4.89 1.9507 2 6 2 4 46.71 5.57 1.9447 1 7 1 4 47.04 1.45 1.9317 -4 0 6 2 47.05 1.76 1.9315 4 0 2 2 47.96 2.35 1.8967 -1 7 3 4 48.22 1.06 1.8873 -1 5 7 4 48.87 1.22 1.8638 -4 2 6 4 49.35 6.99 1.8466 -4 4 2 4 49.86 2.24 1.8288 -2 4 8 4 49.87 1.46 1.8287 2 4 6 4 50.03 4.77 1.8231 0 6 6 4 51.11 2.17 1.7871 3 5 3 4 51.53 2.19 1.7735 0 8 0 2 52.18 3.84 1.7530 -1 7 5 4 52.40 2.78 1.7461 -2 0 10 2 52.40 2.58 1.7460 2 0 8 2 52.42 1.40 1.7455 1 5 7 4 53.07 3.87 1.7257 -4 0 8 2 53.07 3.51 1.7256 4 0 4 2 54.06 1.10 1.6963 4 4 2 4 54.09 6.04 1.6955 -2 2 10 4 54.09 6.42 1.6954 2 2 8 4 54.74 4.97 1.6768 -4 2 8 4 54.75 5.26 1.6767 4 2 4 4 55.01 1.39 1.6694 0 2 10 4 56.04 2.38 1.6411 -3 7 3 4 57.77 2.66 1.5959 -4 6 2 4 58.51 1.48 1.5774 -2 8 4 4 58.51 1.57 1.5774 2 8 2 4 58.96 2.95 1.5666 -2 4 10 4 58.96 2.79 1.5665 2 4 8 4 59.58 3.19 1.5518 -4 4 8 4 59.58 2.97 1.5517 4 4 4 4 60.21 2.86 1.5369 1 9 1 4 60.91 2.27 1.5209 3 7 3 4 61.51 1.75 1.5076 0 8 6 4 62.09 1.95 1.4950 1 7 7 4 64.90 2.10 1.4368 -1 9 5 4 65.18 1.29 1.4314 0 0 12 2 66.57 2.37 1.4047 -2 6 10 4 66.58 2.56 1.4046 2 6 8 4 66.66 1.89 1.4031 0 2 12 4 66.92 1.66 1.3982 -6 0 6 2 66.92 1.42 1.3981 6 0 0 2 67.15 1.59 1.3940 -4 6 8 4 67.16 1.72 1.3939 4 6 4 4 68.30 2.19 1.3733 -3 9 3 4 68.38 1.79 1.3718 -6 2 6 4 68.39 2.35 1.3718 6 2 0 4 68.41 1.99 1.3714 -4 8 2 4 70.05 1.02 1.3432 -3 7 9 4 71.01 1.96 1.3274 0 4 12 4 72.27 1.46 1.3073 -5 7 1 4 72.69 1.68 1.3008 -6 4 6 4 72.69 1.38 1.3007 6 4 0 4 72.71 1.55 1.3005 3 9 3 4 73.79 1.34 1.2841 1 9 7 4 74.90 1.44 1.2679 1 11 1 4 76.58 1.22 1.2441 -5 7 7 4 78.04 1.06 1.2245 0 6 12 4 79.16 1.61 1.2099 -1 11 5 4 79.67 1.08 1.2035 6 6 0 4 81.25 1.23 1.1841 -3 9 9 4 81.83 1.53 1.1771 -4 2 14 4 81.83 1.52 1.1770 4 2 10 4 82.33 1.17 1.1712 -3 11 3 4 85.51 1.63 1.1356 -6 2 12 4 85.52 1.53 1.1355 6 2 6 4 85.91 1.04 1.1313 -4 4 14 4 85.92 1.02 1.1312 4 4 10 4 86.47 1.05 1.1255 -1 9 11 4 87.54 1.03 1.1145 1 11 7 4 89.58 1.06 1.0943 6 4 6 4 89.64 1.39 1.0937 2 2 14 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.