Ni0.75K0.5SU2O13H6 Peeters O M, Vochten R, Blaton N The Canadian Mineralogist 46 (2008) 173-182 The crystal structures of synthetic potassium - transition-metal zippeite-group phases Sample: K-Ni _database_code_amcsd 0006165 CELL PARAMETERS: 8.6620 14.0950 17.7700 90.000 104.180 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 2103.451 Density (g/cm3): 4.881 MAX. ABS. INTENSITY / VOLUME**2: 152.8791721 RIR: 10.199 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.27 21.09 8.6143 0 0 2 2 12.56 100.00 7.0475 0 2 0 2 14.27 1.12 6.2056 1 1 1 4 16.25 15.20 5.4546 0 2 2 4 20.62 6.66 4.3071 0 0 4 2 21.15 5.99 4.2016 -2 0 2 2 21.16 6.59 4.1990 2 0 0 2 21.67 1.79 4.1009 -1 3 1 4 22.89 7.27 3.8856 1 3 1 4 24.22 6.06 3.6751 0 2 4 4 24.67 5.18 3.6089 -2 2 2 4 24.68 4.02 3.6073 2 2 0 4 25.13 3.80 3.5435 -1 3 3 4 25.27 24.92 3.5238 0 4 0 2 25.75 24.53 3.4600 -2 0 4 2 25.78 25.41 3.4558 2 0 2 2 27.35 3.66 3.2614 0 4 2 4 28.74 29.69 3.1059 -2 2 4 4 28.77 28.23 3.1028 2 2 2 4 31.15 15.79 2.8714 0 0 6 2 31.86 1.79 2.8086 -1 3 5 4 32.84 1.97 2.7273 0 4 4 4 33.18 1.83 2.6999 -2 4 2 4 33.19 1.94 2.6992 2 4 0 4 33.25 1.48 2.6948 2 0 4 2 33.70 16.19 2.6592 0 2 6 4 34.36 3.72 2.6102 1 5 1 4 35.63 1.76 2.5198 -2 2 6 4 35.99 1.09 2.4954 -1 1 7 4 36.39 8.80 2.4688 -2 4 4 4 36.41 9.27 2.4673 2 4 2 4 38.32 2.33 2.3492 0 6 0 2 39.77 2.53 2.2664 0 6 2 4 40.53 9.78 2.2260 0 4 6 4 41.00 1.37 2.2014 -3 3 5 4 41.10 1.46 2.1963 -1 5 5 4 41.71 7.94 2.1655 -4 0 2 2 41.95 1.03 2.1536 0 0 8 2 42.21 2.63 2.1410 -2 0 8 2 42.26 2.15 2.1387 2 0 6 2 43.06 1.48 2.1008 -4 0 4 2 43.08 1.37 2.0995 4 0 0 2 43.73 7.35 2.0700 -4 2 2 4 43.76 1.51 2.0685 3 3 3 4 43.96 2.06 2.0596 0 2 8 4 44.21 1.80 2.0486 -2 2 8 4 44.26 2.18 2.0465 2 2 6 4 45.03 1.99 2.0132 -4 2 4 4 45.06 2.53 2.0121 4 2 0 4 45.18 1.53 2.0070 1 3 7 4 45.66 1.62 1.9870 -3 5 3 4 46.37 1.12 1.9581 -1 7 1 4 46.74 4.38 1.9435 -2 6 4 4 46.76 4.25 1.9428 2 6 2 4 46.94 1.08 1.9357 -4 0 6 2 46.99 1.44 1.9337 4 0 2 2 47.00 4.74 1.9332 1 7 1 4 48.24 2.05 1.8865 -1 7 3 4 48.79 1.24 1.8666 -4 2 6 4 49.40 5.96 1.8450 -4 4 2 4 49.84 1.79 1.8297 -2 4 8 4 49.88 1.34 1.8283 2 4 6 4 50.17 3.84 1.8182 0 6 6 4 51.21 1.97 1.7839 3 5 3 4 51.90 1.80 1.7619 0 8 0 2 52.22 2.34 1.7517 -2 0 10 2 52.27 2.18 1.7501 2 0 8 2 52.41 2.97 1.7458 -1 7 5 4 52.47 1.14 1.7439 1 5 7 4 52.93 3.63 1.7300 -4 0 8 2 53.00 3.32 1.7279 4 0 4 2 53.94 5.51 1.7000 -2 2 10 4 53.99 5.85 1.6985 2 2 8 4 54.63 3.94 1.6801 -4 2 8 4 54.69 4.38 1.6782 4 2 4 4 56.27 2.08 1.6350 -3 7 3 4 57.92 2.50 1.5922 -4 6 2 4 58.81 1.41 1.5700 -2 8 4 4 58.83 1.46 1.5696 2 8 2 4 58.88 2.51 1.5686 -2 4 10 4 58.92 2.33 1.5674 2 4 8 4 59.53 3.08 1.5529 -4 4 8 4 59.59 2.75 1.5514 4 4 4 4 60.63 2.23 1.5274 1 9 1 4 61.13 1.79 1.5161 3 7 3 4 61.78 1.70 1.5017 0 8 6 4 62.25 1.69 1.4914 1 7 7 4 64.95 1.00 1.4357 0 0 12 2 65.26 1.81 1.4298 -1 9 5 4 66.46 1.75 1.4068 0 2 12 4 66.59 2.10 1.4043 -2 6 10 4 66.64 2.25 1.4034 2 6 8 4 66.80 1.36 1.4005 -6 0 6 2 66.84 1.21 1.3997 6 0 0 2 67.20 1.22 1.3930 -4 6 8 4 67.26 1.40 1.3919 4 6 4 4 68.28 1.54 1.3737 -6 2 6 4 68.32 1.86 1.3729 6 2 0 4 68.66 1.69 1.3670 -3 9 3 4 68.68 1.64 1.3667 -4 8 2 4 70.88 1.53 1.3296 0 4 12 4 72.45 1.21 1.3046 -5 7 1 4 72.65 1.40 1.3015 -6 4 6 4 72.69 1.17 1.3008 6 4 0 4 73.06 1.24 1.2952 3 9 3 4 74.09 1.04 1.2797 1 9 7 4 75.45 1.13 1.2599 1 11 1 4 79.68 1.18 1.2034 -1 11 5 4 81.55 1.27 1.1804 -4 2 14 4 81.66 1.24 1.1790 4 2 10 4 85.27 1.31 1.1382 -6 2 12 4 85.40 1.26 1.1368 6 2 6 4 89.37 1.09 1.0963 2 2 14 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.