Zn0.75K0.5SU2O13H6 Peeters O M, Vochten R, Blaton N The Canadian Mineralogist 46 (2008) 173-182 The crystal structures of synthetic potassium - transition-metal zippeite-group phases Sample: K-Zn _database_code_amcsd 0006166 CELL PARAMETERS: 8.6500 14.1800 17.7090 90.000 104.140 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 2106.321 Density (g/cm3): 4.920 MAX. ABS. INTENSITY / VOLUME**2: 165.2700109 RIR: 10.938 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 10.30 17.91 8.5862 0 0 2 2 12.48 100.00 7.0900 0 2 0 2 14.27 1.10 6.2054 1 1 1 4 16.21 13.69 5.4670 0 2 2 4 20.69 7.40 4.2931 0 0 4 2 21.18 5.18 4.1941 -2 0 2 2 21.18 5.59 4.1940 2 0 0 2 21.58 1.82 4.1179 -1 3 1 4 22.80 7.16 3.8997 1 3 1 4 24.24 5.75 3.6723 0 2 4 4 24.66 3.98 3.6098 -2 2 2 4 24.66 2.98 3.6097 2 2 0 4 25.08 4.04 3.5507 -1 3 3 4 25.12 25.79 3.5450 0 4 0 2 25.82 21.97 3.4509 -2 0 4 2 25.82 22.90 3.4506 2 0 2 2 27.22 3.26 3.2767 0 4 2 4 28.77 28.15 3.1028 -2 2 4 4 28.77 26.56 3.1027 2 2 2 4 31.25 13.53 2.8621 0 0 6 2 31.87 2.00 2.8084 -1 3 5 4 32.76 2.35 2.7335 0 4 4 4 33.09 1.50 2.7074 -2 4 2 4 33.09 1.72 2.7074 2 4 0 4 33.31 1.56 2.6895 2 0 4 2 33.77 15.70 2.6540 0 2 6 4 34.18 3.65 2.6231 1 5 1 4 35.70 1.96 2.5148 -2 2 6 4 35.71 1.21 2.5147 2 2 4 4 36.11 1.19 2.4876 -1 1 7 4 36.33 7.85 2.4727 -2 4 4 4 36.33 8.79 2.4727 2 4 2 4 38.08 2.34 2.3633 0 6 0 2 39.55 2.40 2.2786 0 6 2 4 40.51 8.42 2.2269 0 4 6 4 41.00 1.32 2.2013 -1 5 5 4 41.02 1.17 2.2002 -3 3 5 4 41.77 8.10 2.1625 -4 0 2 2 42.36 2.78 2.1339 -2 0 8 2 42.36 1.97 2.1338 2 0 6 2 43.14 1.37 2.0970 -4 0 4 2 43.14 1.17 2.0970 4 0 0 2 43.76 1.42 2.0685 3 3 3 4 43.77 7.39 2.0684 -4 2 2 4 44.08 2.14 2.0545 0 2 8 4 44.33 1.53 2.0434 -2 2 8 4 44.33 2.17 2.0433 2 2 6 4 45.08 1.97 2.0109 -4 2 4 4 45.09 2.64 2.0109 4 2 0 4 45.24 1.50 2.0045 1 3 7 4 45.56 1.56 1.9911 -3 5 3 4 46.10 1.11 1.9691 -1 7 1 4 46.58 4.21 1.9499 -2 6 4 4 46.58 4.08 1.9499 2 6 2 4 46.73 4.94 1.9437 1 7 1 4 47.05 1.27 1.9314 -4 0 6 2 47.05 1.47 1.9313 4 0 2 2 47.99 2.08 1.8958 -1 7 3 4 48.88 1.21 1.8635 -4 2 6 4 49.36 6.41 1.8461 -4 4 2 4 49.88 2.06 1.8282 -2 4 8 4 49.88 1.30 1.8282 2 4 6 4 50.05 3.81 1.8223 0 6 6 4 51.13 2.16 1.7866 3 5 3 4 51.56 1.95 1.7725 0 8 0 2 52.21 3.13 1.7522 -1 7 5 4 52.41 2.36 1.7458 -2 0 10 2 52.41 2.15 1.7457 2 0 8 2 52.44 1.20 1.7449 1 5 7 4 53.08 3.25 1.7254 -4 0 8 2 53.08 3.06 1.7253 4 0 4 2 54.07 1.01 1.6959 4 4 2 4 54.10 5.88 1.6951 -2 2 10 4 54.10 6.19 1.6950 2 2 8 4 54.75 3.81 1.6765 -4 2 8 4 54.76 4.55 1.6764 4 2 4 4 56.06 2.17 1.6404 -3 7 3 4 57.79 2.56 1.5954 -4 6 2 4 58.54 1.26 1.5767 -2 8 4 4 58.54 1.37 1.5767 2 8 2 4 58.98 2.48 1.5662 -2 4 10 4 58.98 2.40 1.5661 2 4 8 4 59.59 2.82 1.5514 -4 4 8 4 59.60 2.63 1.5513 4 4 4 4 60.25 2.50 1.5360 1 9 1 4 60.94 1.79 1.5203 3 7 3 4 61.54 1.50 1.5069 0 8 6 4 62.11 1.70 1.4943 1 7 7 4 64.93 1.96 1.4361 -1 9 5 4 65.19 1.11 1.4310 0 0 12 2 66.60 2.27 1.4042 -2 6 10 4 66.60 2.52 1.4042 2 6 8 4 66.68 1.76 1.4027 0 2 12 4 66.93 1.42 1.3980 -6 0 6 2 66.93 1.18 1.3980 6 0 0 2 67.17 1.25 1.3936 -4 6 8 4 67.18 1.47 1.3935 4 6 4 4 68.34 1.79 1.3726 -3 9 3 4 68.40 1.58 1.3716 -6 2 6 4 68.40 1.91 1.3716 6 2 0 4 68.44 1.78 1.3709 -4 8 2 4 71.03 1.67 1.3270 0 4 12 4 72.30 1.28 1.3069 -5 7 1 4 72.71 1.53 1.3006 -6 4 6 4 72.71 1.19 1.3005 6 4 0 4 72.75 1.44 1.2999 3 9 3 4 73.83 1.18 1.2836 1 9 7 4 74.94 1.37 1.2672 1 11 1 4 79.21 1.39 1.2093 -1 11 5 4 81.29 1.12 1.1836 -3 9 9 4 81.85 1.39 1.1769 -4 2 14 4 81.85 1.38 1.1768 4 2 10 4 82.38 1.07 1.1707 -3 11 3 4 85.52 1.54 1.1354 -6 2 12 4 85.53 1.48 1.1354 6 2 6 4 89.66 1.14 1.0935 2 2 14 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.