Kolitschite Grey I E, Mumme W G, Bordet P The Canadian Mineralogist 46 (2008) 1355-1364 A new crystal-chemical variation of the alunite-type structure in monoclinic PbZn0.5Fe3(AsO4)2(OH)6 Locality: Broken Hill, Australia _database_code_amcsd 0006197 CELL PARAMETERS: 25.8898 14.8753 12.1700 90.000 110.681 90.000 SPACE GROUP: C2/c X-RAY WAVELENGTH: 1.541838 Cell Volume: 4384.875 Density (g/cm3): 4.709 MAX. ABS. INTENSITY / VOLUME**2: 27.09593921 RIR: 1.874 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.30 1.83 12.1107 2 0 0 2 14.22 2.92 6.2268 0 2 1 4 14.63 45.00 6.0554 4 0 0 2 14.67 5.22 6.0380 -2 0 2 2 14.69 89.38 6.0317 -2 2 1 4 15.57 15.12 5.6929 0 0 2 2 16.67 1.26 5.3188 -3 1 2 4 17.22 1.85 5.1481 2 2 1 4 18.26 1.23 4.8577 1 3 0 4 18.36 19.87 4.8327 -4 2 1 4 19.43 5.04 4.5682 2 0 2 2 22.02 12.59 4.0369 6 0 0 2 22.04 5.77 4.0329 -6 0 2 2 22.37 4.36 3.9744 4 2 1 4 22.89 1.01 3.8856 -3 1 3 4 23.84 83.32 3.7323 -6 2 1 4 23.93 58.78 3.7188 0 4 0 2 24.97 6.84 3.5665 4 0 2 2 25.02 19.37 3.5589 -2 2 3 4 25.83 1.47 3.4495 -4 2 3 4 26.45 1.24 3.3702 7 1 0 4 26.52 1.98 3.3609 -5 3 2 4 28.07 10.24 3.1788 -8 0 2 2 28.16 17.46 3.1689 4 4 0 4 28.18 3.88 3.1664 -2 4 2 4 28.58 95.76 3.1232 6 2 1 4 28.62 93.55 3.1195 -6 2 3 4 28.67 100.00 3.1134 0 4 2 4 29.50 7.83 3.0277 8 0 0 2 29.62 30.62 3.0158 -4 4 2 4 30.23 11.04 2.9567 -8 2 1 4 31.01 2.33 2.8840 2 4 2 4 31.37 2.61 2.8519 6 0 2 2 31.41 6.06 2.8477 -6 0 4 2 31.43 60.98 2.8464 0 0 4 2 32.74 6.09 2.7352 6 4 0 4 32.76 6.15 2.7339 -6 4 2 4 32.92 8.67 2.7204 -8 2 3 4 33.50 1.03 2.6750 -7 1 4 4 33.50 1.05 2.6750 5 3 2 4 33.88 1.03 2.6458 -9 1 3 4 34.20 3.93 2.6215 4 2 3 4 34.75 2.64 2.5813 -10 0 2 2 34.81 11.18 2.5772 -8 0 4 2 34.85 36.12 2.5741 4 4 2 4 35.38 7.14 2.5370 8 2 1 4 37.12 6.05 2.4221 10 0 0 2 37.14 2.27 2.4209 -10 2 1 4 37.21 3.03 2.4163 -8 4 2 4 37.30 4.35 2.4105 -2 6 1 4 37.59 1.04 2.3925 -3 5 3 4 38.34 1.21 2.3479 8 4 0 4 38.44 5.95 2.3418 2 6 1 4 38.94 2.57 2.3127 -4 2 5 4 38.99 1.66 2.3098 -4 6 1 4 39.42 5.31 2.2856 -10 0 4 2 39.45 21.17 2.2841 4 0 4 2 39.50 40.52 2.2814 -2 2 5 4 39.80 9.10 2.2648 6 2 3 4 39.83 3.05 2.2630 6 4 2 4 39.85 9.87 2.2619 -6 2 5 4 39.87 3.46 2.2609 -6 4 4 4 39.88 15.29 2.2603 0 4 4 4 42.03 8.70 2.1497 -6 6 1 4 42.15 3.67 2.1439 -8 2 5 4 42.64 4.90 2.1205 -10 4 2 4 42.68 1.84 2.1183 -8 4 4 4 42.76 5.74 2.1149 -2 6 3 4 44.43 4.31 2.0391 -12 2 1 4 44.45 8.99 2.0381 -12 2 3 4 44.65 4.24 2.0296 10 4 0 4 44.91 3.76 2.0185 12 0 0 2 44.95 15.74 2.0165 -12 0 4 2 45.07 40.58 2.0116 6 6 1 4 45.09 11.34 2.0106 -6 6 3 4 45.59 1.62 1.9900 10 0 2 2 46.11 3.60 1.9685 8 2 3 4 46.20 2.22 1.9649 -8 6 1 4 46.64 2.42 1.9472 -10 4 4 4 48.13 2.31 1.8907 -8 6 3 4 48.80 31.00 1.8662 -12 4 2 4 48.99 27.63 1.8594 0 8 0 2 49.35 1.94 1.8467 -14 0 2 2 49.95 2.37 1.8258 8 6 1 4 50.13 4.99 1.8198 12 2 1 4 50.19 3.24 1.8176 -12 2 5 4 51.19 2.02 1.7844 -14 0 4 2 51.35 4.50 1.7794 -4 4 6 4 51.59 1.40 1.7718 6 4 4 4 51.64 1.47 1.7701 -6 4 6 4 52.06 4.51 1.7568 -14 2 1 4 52.13 2.48 1.7546 10 4 2 4 52.21 1.78 1.7521 -10 6 3 4 52.92 1.45 1.7301 14 0 0 2 52.98 4.23 1.7283 10 2 3 4 53.10 4.04 1.7248 -8 4 6 4 53.15 5.25 1.7232 -2 6 5 4 53.39 3.34 1.7160 6 6 3 4 53.43 3.65 1.7148 -6 6 5 4 54.20 7.15 1.6924 6 2 5 4 54.26 6.15 1.6907 -6 2 7 4 54.27 7.17 1.6903 0 4 6 4 54.32 1.24 1.6889 6 8 0 4 55.25 1.86 1.6627 -8 2 7 4 55.28 1.21 1.6616 -8 6 5 4 55.56 4.69 1.6540 -14 4 2 4 55.58 1.15 1.6536 -14 2 5 4 55.64 2.13 1.6520 4 0 6 2 55.67 1.93 1.6512 -10 4 6 4 55.68 5.42 1.6507 -2 2 7 4 57.16 1.47 1.6114 -12 6 1 4 57.17 2.55 1.6111 -16 0 2 2 57.18 3.28 1.6109 -12 6 3 4 57.30 2.39 1.6079 8 4 4 4 57.33 2.80 1.6070 -10 2 7 4 57.41 2.06 1.6050 -8 8 2 4 58.07 1.12 1.5885 10 0 4 2 58.23 3.15 1.5845 8 8 0 4 58.44 1.22 1.5793 -16 2 3 4 59.17 6.67 1.5616 12 4 2 4 59.24 6.94 1.5597 -12 4 6 4 59.36 1.34 1.5569 -6 8 4 4 59.37 15.03 1.5567 0 8 4 4 60.04 2.46 1.5409 -16 2 1 4 60.14 1.18 1.5385 8 2 5 4 60.35 1.45 1.5337 12 2 3 4 60.45 2.00 1.5315 -12 2 7 4 61.25 1.18 1.5133 14 0 2 2 61.41 22.51 1.5097 4 4 6 4 61.42 9.27 1.5095 -8 0 8 2 61.49 4.63 1.5079 -8 8 4 4 61.69 1.67 1.5035 -16 2 5 4 62.02 2.16 1.4964 12 6 1 4 62.08 1.16 1.4952 -12 6 5 4 63.02 1.46 1.4749 10 8 0 4 63.67 3.99 1.4615 -16 4 4 4 63.67 1.62 1.4615 -16 0 6 2 63.71 1.39 1.4608 10 4 4 4 63.71 3.08 1.4608 -14 6 1 4 63.73 2.82 1.4603 -14 4 6 4 63.82 1.45 1.4584 8 8 2 4 64.50 1.80 1.4447 -14 2 7 4 64.52 3.12 1.4443 10 6 3 4 64.62 1.35 1.4424 -10 8 4 4 64.64 3.80 1.4420 4 8 4 4 65.41 1.44 1.4267 -18 0 4 2 65.56 1.98 1.4238 -12 0 8 2 65.59 2.21 1.4232 0 0 8 2 65.60 5.76 1.4232 6 6 5 4 65.65 1.86 1.4221 -6 6 7 4 66.30 1.01 1.4098 16 2 1 4 66.37 1.25 1.4085 -12 8 2 4 66.49 3.11 1.4063 -6 10 1 4 66.73 2.04 1.4017 14 4 2 4 66.79 1.11 1.4007 8 0 6 2 66.91 2.04 1.3985 -4 4 8 4 66.93 1.87 1.3980 -2 6 7 4 68.22 2.09 1.3747 14 2 3 4 68.43 2.35 1.3711 -18 2 1 4 68.48 1.23 1.3702 -18 2 5 4 68.63 2.73 1.3676 12 8 0 4 68.66 4.44 1.3670 -12 8 4 4 68.75 3.55 1.3654 6 10 1 4 68.77 5.55 1.3651 -6 10 3 4 70.70 1.35 1.3325 -18 4 2 4 70.90 1.09 1.3292 0 4 8 4 71.26 1.13 1.3234 -12 6 7 4 73.54 1.76 1.2879 4 0 8 2 73.59 3.23 1.2871 -2 2 9 4 74.05 1.04 1.2803 12 2 5 4 74.85 2.24 1.2685 16 4 2 4 75.01 2.62 1.2662 -14 6 7 4 75.17 3.93 1.2639 -2 10 5 4 76.58 1.01 1.2441 -18 6 3 4 76.63 1.04 1.2434 16 2 3 4 76.91 2.32 1.2396 0 12 0 2 77.25 1.95 1.2350 4 8 6 4 78.43 2.25 1.2193 -20 4 4 4 78.56 1.39 1.2176 -16 8 2 4 78.57 1.03 1.2176 -16 4 8 4 78.76 1.06 1.2151 -18 6 5 4 79.06 2.43 1.2112 0 12 2 4 81.06 1.36 1.1863 -6 6 9 4 82.27 3.97 1.1719 -8 8 8 4 82.36 1.88 1.1709 4 12 2 4 83.48 2.47 1.1580 10 2 7 4 83.63 2.22 1.1563 -8 4 10 4 83.65 2.72 1.1561 -2 6 9 4 84.05 3.41 1.1515 20 4 0 4 84.06 1.73 1.1515 -22 2 5 4 84.28 2.15 1.1490 -16 8 6 4 84.49 1.42 1.1467 -4 12 4 4 86.02 2.15 1.1302 0 8 8 4 86.07 1.12 1.1296 -6 10 7 4 87.05 1.02 1.1195 -16 0 10 2 87.12 1.31 1.1188 8 8 6 4 88.22 1.39 1.1076 20 0 2 2 88.50 1.03 1.1048 -14 4 10 4 88.62 1.02 1.1036 -10 10 7 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.