data_global _chemical_name_mineral 'Fizelyite' loop_ _publ_author_name 'Yang H' 'Downs R T' 'Burt J B' 'Costin G' _journal_name_full 'The Canadian Mineralogist' _journal_volume 47 _journal_year 2009 _journal_page_first 1257 _journal_page_last 1264 _publ_section_title ; Structure refinement of an untwinned single crystal of Ag-excess fizelyite, Ag5.94Pb13.74Sb20.84S48 ; _database_code_amcsd 0006307 _chemical_compound_source 'Van Silver mine, Squamish, British Columbia, Canada' _chemical_formula_sum 'Pb3.436 Sb5.215 Ag1.486 S12' _cell_length_a 19.2767 _cell_length_b 13.2345 _cell_length_c 8.7230 _cell_angle_alpha 90 _cell_angle_beta 90.401 _cell_angle_gamma 90 _cell_volume 2225.335 _exptl_crystal_density_diffrn 5.647 _symmetry_space_group_name_H-M 'P 1 21/n 1' loop_ _space_group_symop_operation_xyz 'x,y,z' '1/2+x,1/2-y,1/2+z' '1/2-x,1/2+y,1/2-z' '-x,-y,-z' loop_ _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_occupancy _atom_site_U_iso_or_equiv Pb1 0.25336 0.90335 0.39489 1.00000 0.03218 Pb2 0.25021 0.91738 -0.09877 1.00000 0.03155 PbM1 0.04887 0.88423 0.63069 0.88000 0.02493 SbM1A 0.04887 0.88423 0.63069 0.12000 0.02493 PbM2 0.12809 0.14880 0.11639 0.55600 0.02370 SbM2A 0.12809 0.14880 0.11639 0.09500 0.02370 AgM2B 0.11798 0.15008 0.05462 0.33000 0.09790 Sb1 0.34866 0.12667 0.64208 1.00000 0.02235 Sb2 0.44284 0.88187 0.62540 1.00000 0.02223 Sb3 0.12784 0.64666 0.38066 1.00000 0.02162 Sb4 -0.05363 0.63074 0.63687 1.00000 0.02269 Sb5 0.05207 0.87500 0.14416 1.00000 0.02161 Ag1 0.14372 0.17987 -0.39271 0.75500 0.04637 Ag1B 0.13336 0.16903 -0.34655 0.19200 0.02802 Ag2 0.17332 0.11542 0.33880 0.20900 0.04046 S1 0.39464 0.00414 -0.16482 1.00000 0.02295 S2 -0.00030 0.72559 0.84772 1.00000 0.03224 S3 0.23047 0.04647 -0.35532 1.00000 0.02388 S4 0.33643 0.78508 0.62657 1.00000 0.02409 S5 0.09962 0.96916 0.93084 1.00000 0.03017 S6 0.16607 0.75761 0.58753 1.00000 0.02259 S7 0.39728 0.00309 0.43327 1.00000 0.02244 S8 -0.01999 0.75146 0.43163 1.00000 0.02524 S9 0.25856 0.06015 0.13720 1.00000 0.02554 S10 -0.16860 0.70588 0.64858 1.00000 0.02635 S11 0.08702 0.99048 0.34882 1.00000 0.02929 S12 0.15766 0.76730 0.16853 1.00000 0.02366 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Pb1 0.03363 0.03376 0.02918 -0.00773 0.00202 -0.00293 Pb2 0.03316 0.02741 0.03401 -0.00215 -0.00364 0.00198 PbM1 0.02451 0.02613 0.02414 0.00108 -0.00147 -0.00081 SbM1A 0.02451 0.02613 0.02414 0.00108 -0.00147 -0.00081 PbM2 0.02483 0.01881 0.02749 0.00054 0.00214 -0.00003 SbM2A 0.02483 0.01881 0.02749 0.00054 0.00214 -0.00003 AgM2B 0.10607 0.02085 0.16729 -0.00852 0.03758 0.01501 Sb1 0.02547 0.02153 0.02002 0.00258 -0.00127 0.00073 Sb2 0.01866 0.02095 0.02703 -0.00002 -0.00363 0.00087 Sb3 0.02210 0.02009 0.02266 -0.00015 0.00001 0.00015 Sb4 0.02175 0.02430 0.02198 -0.00106 -0.00151 -0.00148 Sb5 0.02015 0.02221 0.02248 -0.00328 0.00023 0.00136 Ag1 0.03757 0.05093 0.05059 0.02238 -0.00231 0.01009 Ag1B 0.01722 0.02421 0.04261 0.00972 -0.00172 -0.01177 Ag2 0.03250 0.02228 0.06699 -0.01154 0.02738 -0.01545 S1 0.02652 0.02387 0.01844 0.00093 -0.00093 -0.00012 S2 0.03281 0.04091 0.02299 -0.01066 -0.00048 -0.00504 S3 0.02212 0.02285 0.02664 0.00538 -0.00274 -0.00133 S4 0.02311 0.02370 0.02543 -0.00431 -0.00148 0.00414 S5 0.02782 0.03657 0.02607 -0.01035 -0.00319 0.00649 S6 0.02099 0.02423 0.02255 -0.00224 0.00164 -0.00006 S7 0.02552 0.02419 0.01761 -0.00100 -0.00037 0.00214 S8 0.02147 0.03394 0.02032 -0.00031 -0.00022 0.00161 S9 0.02368 0.02174 0.03125 -0.00530 0.00284 -0.00045 S10 0.01687 0.03400 0.02820 -0.00154 0.00070 0.00429 S11 0.03761 0.02633 0.02392 -0.00053 -0.00064 -0.00351 S12 0.02469 0.02470 0.02158 -0.00071 -0.00048 0.00194