RbBaScSi3O9 Wierzbicka-Wieczorek M, Kolitsch U, Tillmanns E The Canadian Mineralogist 48 (2010) 51-68 The crystal structures of three new complex silicates of scandium Locality: synthetic _database_code_amcsd 0006317 CELL PARAMETERS: 6.9570 10.1990 11.8810 90.000 90.070 90.000 SPACE GROUP: P2_1/n X-RAY WAVELENGTH: 1.541838 Cell Volume: 843.009 Density (g/cm3): 3.907 MAX. ABS. INTENSITY / VOLUME**2: 19.21859855 RIR: 1.601 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 11.43 22.48 7.7387 0 1 1 4 14.75 7.49 6.0067 -1 0 1 2 14.76 10.27 6.0003 1 0 1 2 14.91 8.80 5.9405 0 0 2 2 17.39 17.04 5.0995 0 2 0 2 18.94 2.80 4.6861 0 2 1 4 21.50 2.47 4.1326 -1 1 2 4 21.52 5.46 4.1285 1 1 2 4 21.61 5.41 4.1129 1 2 0 4 24.11 3.33 3.6918 0 1 3 4 25.61 42.02 3.4785 2 0 0 2 25.87 43.85 3.4436 -1 0 3 2 25.90 41.97 3.4399 1 0 3 2 27.08 7.62 3.2923 2 1 0 4 27.29 3.69 3.2685 0 3 1 4 27.34 7.05 3.2626 -1 1 3 4 27.36 8.48 3.2595 1 1 3 4 28.12 3.87 3.1737 -2 1 1 4 28.54 1.49 3.1279 0 2 3 4 29.75 7.45 3.0033 -2 0 2 2 29.78 5.34 3.0001 2 0 2 2 30.09 7.65 2.9702 0 0 4 2 30.21 63.31 2.9587 -1 3 1 4 30.22 61.94 2.9579 1 3 1 4 30.29 63.75 2.9506 0 3 2 4 31.04 27.06 2.8810 -2 1 2 4 31.07 27.89 2.8782 2 1 2 4 31.12 77.85 2.8736 2 2 0 4 31.34 77.12 2.8538 -1 2 3 4 31.37 24.55 2.8518 0 1 4 4 31.37 75.45 2.8518 1 2 3 4 32.05 1.12 2.7924 2 2 1 4 34.66 1.96 2.5879 -2 2 2 4 34.96 2.06 2.5666 0 2 4 4 35.20 4.71 2.5498 0 4 0 2 37.36 5.83 2.4071 1 2 4 4 38.70 3.24 2.3270 -2 2 3 4 38.92 1.06 2.3142 0 1 5 4 39.61 4.43 2.2755 3 0 1 2 39.89 2.79 2.2602 -2 0 4 2 40.06 11.14 2.2508 -2 3 2 4 40.08 11.59 2.2495 2 3 2 4 40.12 2.48 2.2478 1 0 5 2 40.32 8.90 2.2368 0 3 4 4 40.60 12.69 2.2219 -3 1 1 4 40.90 1.13 2.2066 -2 1 4 4 40.95 10.62 2.2041 2 1 4 4 41.09 9.92 2.1967 -1 1 5 4 41.12 1.42 2.1951 1 1 5 4 42.15 1.21 2.1439 0 4 3 4 42.81 2.26 2.1125 3 1 2 4 43.54 3.57 2.0788 -3 2 1 4 43.55 1.21 2.0780 3 2 1 4 43.86 4.99 2.0642 2 2 4 4 44.00 3.85 2.0581 -1 2 5 4 44.03 2.68 2.0565 2 4 0 4 44.20 1.89 2.0492 -1 4 3 4 44.22 1.82 2.0484 1 4 3 4 44.72 1.04 2.0266 -2 4 1 4 44.73 1.74 2.0261 2 4 1 4 45.10 2.55 2.0104 0 5 1 4 45.29 14.78 2.0022 -3 0 3 2 45.34 15.46 2.0001 3 0 3 2 45.82 12.99 1.9802 0 0 6 2 47.05 9.17 1.9315 -1 5 1 4 47.05 8.18 1.9313 1 5 1 4 47.11 7.87 1.9292 0 5 2 4 48.10 10.83 1.8916 -3 3 1 4 48.12 3.50 1.8910 3 3 1 4 48.36 4.76 1.8822 -2 3 4 4 48.40 8.66 1.8806 2 3 4 4 48.53 9.24 1.8760 -1 3 5 4 48.55 5.37 1.8750 1 3 5 4 48.62 1.44 1.8727 -1 1 6 4 48.87 17.49 1.8637 -3 2 3 4 48.87 1.61 1.8636 1 4 4 4 48.92 17.43 1.8620 3 2 3 4 49.37 15.96 1.8459 0 2 6 4 49.99 1.42 1.8245 2 4 3 4 50.71 1.84 1.8002 -3 1 4 4 52.62 9.88 1.7392 4 0 0 2 53.20 9.81 1.7218 -2 0 6 2 53.26 8.79 1.7200 2 0 6 2 53.94 4.93 1.6998 0 6 0 2 54.00 2.55 1.6982 -3 4 1 4 54.03 1.09 1.6972 -4 1 1 4 54.27 2.52 1.6902 2 4 4 4 54.37 13.31 1.6874 -2 5 2 4 54.39 2.14 1.6868 -1 4 5 4 54.39 12.96 1.6868 2 5 2 4 54.58 13.55 1.6815 0 5 4 4 54.83 1.75 1.6743 0 1 7 4 55.32 2.00 1.6606 -3 0 5 2 55.76 1.32 1.6486 -3 4 2 4 55.77 2.11 1.6485 1 0 7 2 55.79 1.33 1.6478 -4 1 2 4 55.85 6.84 1.6461 4 2 0 4 56.19 1.57 1.6371 3 1 5 4 56.24 3.04 1.6356 -1 6 1 4 56.25 2.75 1.6355 1 6 1 4 56.29 1.86 1.6342 0 6 2 4 56.40 6.42 1.6313 -2 2 6 4 56.46 6.24 1.6298 2 2 6 4 56.52 1.53 1.6282 -1 1 7 4 58.13 1.73 1.5868 -4 2 2 4 58.71 1.05 1.5727 4 1 3 4 58.84 1.63 1.5693 -1 2 7 4 60.99 5.27 1.5192 -3 5 1 4 61.00 7.12 1.5189 3 5 1 4 61.21 7.05 1.5143 -2 5 4 4 61.24 4.48 1.5135 2 5 4 4 61.35 5.63 1.5111 -1 5 5 4 61.37 8.90 1.5106 1 5 5 4 61.91 2.60 1.4987 -4 3 2 4 61.95 9.84 1.4979 4 3 2 4 62.22 8.74 1.4921 -3 3 5 4 62.28 3.11 1.4907 3 3 5 4 62.37 1.47 1.4888 3 1 6 4 62.60 3.05 1.4840 -1 3 7 4 62.63 7.32 1.4833 1 3 7 4 62.82 2.33 1.4793 -2 6 2 4 62.83 2.11 1.4789 2 6 2 4 63.01 2.67 1.4753 0 6 4 4 64.90 1.79 1.4368 4 4 0 4 65.40 1.28 1.4269 -2 4 6 4 65.46 1.40 1.4259 2 4 6 4 65.98 2.39 1.4159 -1 7 1 4 65.98 2.73 1.4159 1 7 1 4 66.02 3.07 1.4151 0 7 2 4 67.82 1.50 1.3818 5 0 1 2 68.28 3.59 1.3736 -4 3 4 4 68.35 2.51 1.3724 4 3 4 4 68.96 1.85 1.3618 3 6 1 4 69.01 3.54 1.3609 0 3 8 4 69.31 1.29 1.3558 1 6 5 4 69.39 1.07 1.3543 -2 1 8 4 71.89 2.56 1.3132 -5 0 3 2 71.96 5.26 1.3122 5 0 3 2 72.15 1.31 1.3092 0 1 9 4 72.26 5.19 1.3075 -4 0 6 2 72.36 2.23 1.3060 4 0 6 2 72.92 1.43 1.2973 -1 0 9 2 72.96 5.10 1.2967 1 0 9 2 73.26 3.59 1.2921 -4 5 2 4 73.54 1.14 1.2878 -3 5 5 4 73.61 3.87 1.2869 3 5 5 4 73.89 3.43 1.2826 -1 5 7 4 74.04 1.20 1.2804 -5 3 1 4 74.06 6.03 1.2801 5 3 1 4 74.63 5.52 1.2717 -5 2 3 4 74.68 5.18 1.2710 -3 3 7 4 74.69 1.08 1.2708 5 2 3 4 74.90 1.44 1.2679 -2 3 8 4 74.96 5.56 1.2669 2 3 8 4 75.09 5.03 1.2651 4 2 6 4 75.64 4.68 1.2572 -1 2 9 4 76.37 1.62 1.2471 -1 8 1 4 76.37 2.15 1.2470 1 8 1 4 76.41 2.53 1.2465 0 8 2 4 77.85 1.59 1.2270 3 7 1 4 78.03 1.39 1.2246 -2 7 4 4 79.18 1.09 1.2096 -2 6 6 4 79.21 2.45 1.2093 -4 5 4 4 79.28 1.90 1.2085 4 5 4 4 79.90 1.96 1.2006 0 5 8 4 80.19 2.71 1.1970 2 8 0 4 80.30 3.07 1.1956 -1 8 3 4 80.32 3.01 1.1954 1 8 3 4 80.69 1.06 1.1908 4 6 2 4 80.93 1.75 1.1879 -3 6 5 4 81.30 1.26 1.1834 1 6 7 4 82.71 1.24 1.1668 5 4 3 4 83.00 1.06 1.1635 -4 4 6 4 83.35 1.24 1.1595 6 0 0 2 84.38 1.44 1.1479 -3 0 9 2 84.49 1.16 1.1466 3 0 9 2 84.71 3.34 1.1442 -5 5 1 4 85.41 2.18 1.1366 3 5 7 4 85.54 2.92 1.1353 -2 5 8 4 85.78 1.27 1.1327 -5 3 5 4 85.88 1.46 1.1316 5 3 5 4 85.98 2.62 1.1306 6 2 0 4 86.54 1.17 1.1247 4 6 4 4 87.01 2.18 1.1198 -3 2 9 4 87.12 2.22 1.1187 3 2 9 4 87.75 1.92 1.1123 -3 8 1 4 87.97 2.64 1.1101 2 8 4 4 88.06 1.95 1.1091 -1 8 5 4 89.25 1.91 1.0975 4 7 2 4 89.48 1.48 1.0952 -3 7 5 4 89.85 1.68 1.0917 1 7 7 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.