SnSb4S7 Topa D, Makovicky E, Schimper H J, Stadler A, Basch A, Dittrich H, Amthauer G The Canadian Mineralogist 48 (2010) 1119-1126 The crystal structure of SnSb4S7, a new member of the meneghinite homologous series Locality: synthetic _database_code_amcsd 0017824 CELL PARAMETERS: 11.3310 3.8650 13.9400 90.000 105.281 90.000 SPACE GROUP: P2_1/m X-RAY WAVELENGTH: 1.541838 Cell Volume: 588.909 Density (g/cm3): 4.681 MAX. ABS. INTENSITY / VOLUME**2: 25.35593078 RIR: 1.764 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 6.57 5.38 13.4471 0 0 1 2 11.70 4.84 7.5622 1 0 1 2 13.17 31.39 6.7236 0 0 2 2 13.52 20.80 6.5486 -1 0 2 2 15.81 3.36 5.6044 -2 0 1 2 16.22 4.16 5.4652 2 0 0 2 17.21 30.88 5.1528 1 0 2 2 18.02 2.20 4.9233 -2 0 2 2 19.07 10.52 4.6533 2 0 1 2 19.32 21.39 4.5940 -1 0 3 2 19.81 6.02 4.4824 0 0 3 2 22.09 19.94 4.0247 -2 0 3 2 23.35 30.10 3.8097 1 0 3 2 23.53 18.92 3.7811 2 0 2 2 23.56 4.15 3.7769 -3 0 1 2 24.43 15.10 3.6439 1 1 0 4 24.43 50.22 3.6435 3 0 0 2 24.53 43.06 3.6290 -3 0 2 2 24.75 25.67 3.5978 -1 1 1 4 25.59 54.04 3.4814 -1 0 4 2 25.89 34.83 3.4416 1 1 1 4 26.60 5.34 3.3508 0 1 2 4 26.78 7.55 3.3285 -1 1 2 4 27.17 13.33 3.2822 -3 0 3 2 27.24 12.90 3.2743 -2 0 4 2 28.28 9.42 3.1556 2 1 0 4 28.88 25.01 3.0919 1 1 2 4 28.90 36.44 3.0895 2 0 3 2 29.38 68.29 3.0401 -2 1 2 4 29.79 8.26 2.9988 1 0 4 2 30.06 59.69 2.9732 2 1 1 4 30.22 10.55 2.9575 -1 1 3 4 30.54 8.29 2.9271 0 1 3 4 30.84 1.72 2.8992 3 0 2 2 31.08 1.61 2.8774 -3 0 4 2 31.94 2.42 2.8022 -4 0 2 2 32.11 99.47 2.7877 -2 1 3 4 32.77 2.91 2.7326 4 0 0 2 33.01 2.66 2.7132 1 1 3 4 33.02 16.09 2.7129 -2 0 5 2 33.14 42.27 2.7028 2 1 2 4 33.16 65.50 2.7013 -3 1 1 4 33.81 10.50 2.6512 3 1 0 4 33.88 11.36 2.6456 -3 1 2 4 34.82 39.24 2.5764 2 0 4 2 35.20 3.67 2.5499 4 0 1 2 35.39 3.02 2.5365 0 1 4 4 35.75 5.25 2.5113 3 1 1 4 35.95 10.10 2.4983 -2 1 4 4 36.50 3.24 2.4616 -4 0 4 2 37.26 8.30 2.4132 2 1 3 4 37.98 5.05 2.3693 1 1 4 4 38.70 5.48 2.3266 4 0 2 2 38.83 2.39 2.3193 3 1 2 4 39.03 2.23 2.3080 -3 1 4 4 39.22 18.32 2.2970 -2 0 6 2 39.87 18.52 2.2609 -1 1 5 4 40.00 1.41 2.2539 -5 0 1 2 40.38 8.47 2.2335 -4 0 5 2 40.43 15.91 2.2313 4 1 0 4 40.63 2.17 2.2205 -2 1 5 4 40.88 35.16 2.2076 0 1 5 4 40.88 3.19 2.2074 -5 0 3 2 41.05 3.78 2.1987 3 0 4 2 41.13 3.10 2.1948 2 0 5 2 41.13 11.08 2.1948 -4 1 3 4 41.30 2.73 2.1861 5 0 0 2 41.36 3.33 2.1829 -3 0 6 2 42.15 1.13 2.1438 2 1 4 4 42.47 21.30 2.1284 4 1 1 4 42.83 3.58 2.1114 3 1 3 4 43.00 9.46 2.1035 -5 0 4 2 43.07 1.72 2.1001 4 0 3 2 43.54 10.65 2.0784 1 1 5 4 43.59 6.67 2.0763 -4 1 4 4 43.66 3.22 2.0730 5 0 1 2 45.05 6.05 2.0124 -4 0 6 2 45.50 16.94 1.9933 4 1 2 4 45.75 3.16 1.9832 -2 0 7 2 46.09 9.23 1.9693 -5 0 5 2 46.52 15.29 1.9520 -5 1 2 4 46.65 12.66 1.9470 -5 1 1 4 46.86 2.58 1.9388 0 1 6 4 46.97 15.21 1.9344 5 0 2 2 46.99 25.34 1.9339 -4 1 5 4 47.02 47.35 1.9325 0 2 0 2 47.32 5.33 1.9210 0 0 7 2 47.32 2.08 1.9209 -3 0 7 2 47.43 4.74 1.9168 -5 1 3 4 47.75 2.88 1.9048 2 0 6 2 47.86 2.42 1.9007 -3 1 6 4 48.13 1.81 1.8906 4 0 4 2 48.19 9.56 1.8884 -6 0 2 2 48.64 2.80 1.8721 -6 0 1 2 48.75 1.32 1.8681 -6 0 3 2 49.05 1.90 1.8573 0 2 2 4 49.16 1.25 1.8535 -1 2 2 4 49.32 1.33 1.8476 -5 1 4 4 49.39 3.91 1.8453 4 1 3 4 49.59 2.19 1.8383 1 1 6 4 50.02 3.75 1.8235 -5 0 6 2 50.29 1.75 1.8145 -6 0 4 2 50.35 4.21 1.8123 1 0 7 2 50.44 2.87 1.8094 1 2 2 4 51.08 2.96 1.7880 5 0 3 2 51.18 1.23 1.7847 2 2 1 4 51.29 2.16 1.7813 -1 2 3 4 51.81 1.05 1.7645 -1 1 7 4 51.81 1.64 1.7645 -2 1 7 4 52.13 5.43 1.7547 -5 1 5 4 52.53 3.11 1.7421 -2 2 3 4 52.58 1.99 1.7407 -2 0 8 2 52.88 1.28 1.7313 -1 0 8 2 52.93 9.28 1.7299 5 1 2 4 52.94 16.82 1.7295 3 1 5 4 53.14 4.85 1.7234 1 2 3 4 53.23 3.36 1.7208 2 2 2 4 53.25 35.11 1.7203 0 1 7 4 53.25 13.34 1.7202 -3 1 7 4 53.34 3.64 1.7176 3 0 6 2 53.64 1.09 1.7086 2 1 6 4 53.69 9.16 1.7072 3 2 0 4 53.70 3.90 1.7070 -3 0 8 2 53.74 8.47 1.7057 -3 2 2 4 54.29 10.43 1.6896 -1 2 4 4 54.46 2.68 1.6848 -6 1 1 4 54.56 1.96 1.6820 -6 1 3 4 55.15 2.85 1.6653 -3 2 3 4 55.19 2.92 1.6643 -2 2 4 4 55.74 2.50 1.6491 -5 1 6 4 55.99 1.50 1.6425 -6 1 4 4 56.14 7.82 1.6384 2 2 3 4 56.66 2.48 1.6244 1 2 4 4 56.73 1.55 1.6227 5 1 3 4 57.60 1.04 1.6001 -7 0 1 2 57.64 1.12 1.5993 1 0 8 2 58.22 2.33 1.5847 -7 0 4 2 58.41 1.04 1.5800 -1 1 8 4 58.65 4.53 1.5740 -2 2 5 4 58.83 1.14 1.5696 3 1 6 4 59.17 7.15 1.5615 7 0 0 2 59.70 2.22 1.5488 -2 0 9 2 59.82 12.02 1.5459 2 2 4 4 59.88 1.71 1.5447 4 0 6 2 60.07 1.18 1.5402 4 2 1 4 60.08 1.68 1.5401 3 0 7 2 60.08 1.45 1.5400 -6 0 7 2 60.17 3.60 1.5378 -7 0 5 2 61.00 1.13 1.5190 6 1 2 4 62.47 2.29 1.4866 4 2 2 4 62.84 7.32 1.4788 -2 2 6 4 62.89 1.92 1.4777 1 1 8 4 63.68 3.24 1.4614 -4 2 5 4 64.04 1.35 1.4540 -5 2 3 4 64.16 1.43 1.4515 3 2 4 4 64.22 1.28 1.4504 2 2 5 4 64.26 1.25 1.4496 6 0 4 2 64.34 1.20 1.4479 5 2 0 4 64.35 7.00 1.4478 7 1 0 4 64.39 1.45 1.4469 -3 2 6 4 64.76 2.31 1.4395 6 1 3 4 64.80 1.72 1.4387 -6 0 8 2 64.85 1.37 1.4377 -2 1 9 4 65.22 1.34 1.4306 -6 1 7 4 65.30 3.85 1.4288 -7 1 5 4 65.39 2.45 1.4271 -1 1 9 4 65.60 3.81 1.4231 -5 2 4 4 65.75 2.37 1.4202 -5 0 9 2 66.02 1.56 1.4151 -8 0 3 2 66.10 1.44 1.4135 5 2 1 4 66.46 4.35 1.4068 4 0 7 2 66.77 1.32 1.4011 -8 0 4 2 67.16 2.82 1.3939 -4 2 6 4 67.60 1.24 1.3857 -3 0 10 2 67.70 1.49 1.3841 -2 2 7 4 67.95 1.05 1.3794 -1 0 10 2 67.96 4.32 1.3793 -5 2 5 4 68.65 7.56 1.3672 5 2 2 4 68.92 2.53 1.3624 0 2 7 4 69.22 1.33 1.3573 6 1 4 4 69.26 1.46 1.3566 2 2 6 4 69.27 2.46 1.3564 -4 0 10 2 69.61 4.91 1.3506 -6 2 2 4 69.70 2.20 1.3491 7 1 2 4 69.97 1.31 1.3446 -6 2 1 4 70.67 2.91 1.3330 -5 1 9 4 71.08 2.14 1.3263 -5 2 6 4 71.30 1.05 1.3228 -6 2 4 4 71.35 2.23 1.3220 1 2 7 4 71.35 9.10 1.3218 -7 1 7 4 71.64 2.60 1.3172 -8 1 4 4 71.95 1.52 1.3124 5 2 3 4 72.03 1.50 1.3111 -2 1 10 4 72.11 2.42 1.3098 5 1 6 4 73.18 1.04 1.2934 -2 2 8 4 73.49 3.24 1.2887 7 1 3 4 73.81 2.36 1.2838 3 2 6 4 74.11 2.22 1.2794 -3 2 8 4 74.25 5.27 1.2773 2 1 9 4 74.33 2.09 1.2761 6 1 5 4 74.93 1.96 1.2674 -6 1 9 4 75.93 1.16 1.2531 8 1 1 4 76.42 2.47 1.2464 -2 3 2 4 76.76 2.77 1.2416 2 3 1 4 76.85 2.11 1.2404 -5 1 10 4 77.85 4.32 1.2270 -2 3 3 4 77.97 1.67 1.2254 -7 2 4 4 78.22 1.01 1.2221 4 1 8 4 78.42 1.94 1.2195 2 3 2 4 78.43 3.15 1.2193 -3 3 1 4 78.44 2.50 1.2192 5 1 7 4 78.52 1.15 1.2182 7 0 5 2 78.80 4.86 1.2146 7 2 0 4 79.27 1.54 1.2086 -2 2 9 4 79.42 1.13 1.2066 4 2 6 4 79.60 1.13 1.2044 3 2 7 4 79.60 1.05 1.2043 -6 2 7 4 79.68 2.46 1.2033 -7 2 5 4 79.69 2.54 1.2033 -2 1 11 4 80.18 6.45 1.1971 -9 1 3 4 80.68 1.60 1.1910 -1 1 11 4 80.75 1.42 1.1900 -6 1 10 4 81.17 1.99 1.1849 -4 1 11 4 82.07 1.83 1.1743 2 1 10 4 82.48 1.27 1.1695 -1 3 5 4 82.84 1.24 1.1653 4 3 0 4 83.13 2.68 1.1619 0 3 5 4 83.30 1.03 1.1600 -4 3 3 4 83.83 1.21 1.1540 -6 2 8 4 84.20 1.59 1.1499 4 3 1 4 84.33 1.48 1.1485 -4 0 12 2 84.70 1.84 1.1444 -5 2 9 4 84.77 1.02 1.1436 9 0 2 2 84.94 1.06 1.1418 1 3 5 4 84.94 1.33 1.1417 -8 2 3 4 85.35 3.46 1.1373 4 2 7 4 85.63 1.02 1.1343 -8 2 4 4 86.31 1.59 1.1271 4 3 2 4 86.40 1.06 1.1261 -3 2 10 4 86.94 1.46 1.1206 0 0 12 2 87.05 1.51 1.1194 -5 3 2 4 87.14 1.41 1.1185 -5 3 1 4 87.39 2.69 1.1160 -4 3 5 4 87.59 1.46 1.1140 8 1 4 4 87.95 2.20 1.1102 -4 2 10 4 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.