Ag2.25Pb2.5Bi4.25S10 Topa D, Makovicky E, Schimper H J, Dittrich H The Canadian Mineralogist 48 (2010) 1127-1135 The crystal structure of a synthetic orthorhombic N = 8 member of the lillianite homologous series Locality: synthetic _database_code_amcsd 0017871 CELL PARAMETERS: 4.0840 13.4530 33.9320 90.000 90.000 90.000 SPACE GROUP: Cmcm X-RAY WAVELENGTH: 1.541838 Cell Volume: 1864.294 Density (g/cm3): 6.990 MAX. ABS. INTENSITY / VOLUME**2: 78.44424698 RIR: 3.654 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 5.21 4.77 16.9660 0 0 2 2 10.43 1.80 8.4830 0 0 4 2 13.16 2.26 6.7265 0 2 0 2 13.42 1.88 6.5981 0 2 1 4 15.33 1.42 5.7814 0 2 3 4 15.67 1.38 5.6553 0 0 6 2 18.57 1.02 4.7774 0 2 5 4 20.52 5.10 4.3287 0 2 6 4 20.94 1.30 4.2415 0 0 8 2 22.75 2.20 3.9079 1 1 0 4 23.36 3.96 3.8082 1 1 2 8 24.09 1.20 3.6936 1 1 3 8 24.82 61.21 3.5878 0 2 8 4 25.09 34.58 3.5494 1 1 4 8 26.26 1.35 3.3932 0 0 10 2 26.32 99.56 3.3865 1 1 5 8 26.50 3.34 3.3633 0 4 0 2 26.63 38.70 3.3469 0 4 1 4 27.03 29.23 3.2991 0 4 2 4 27.11 88.47 3.2888 0 2 9 4 27.67 6.13 3.2237 0 4 3 4 27.75 31.83 3.2150 1 1 6 8 29.48 35.98 3.0296 0 2 10 4 29.58 7.23 3.0195 1 3 0 4 29.64 1.29 3.0135 0 4 5 4 29.70 5.16 3.0076 1 3 1 8 30.06 24.36 2.9727 1 3 2 8 30.65 98.32 2.9173 1 3 3 8 31.12 2.24 2.8740 1 1 8 8 31.45 100.00 2.8446 1 3 4 8 31.92 32.88 2.8039 0 2 11 4 32.45 6.59 2.7587 1 3 5 8 33.65 3.47 2.6636 1 3 6 8 34.40 4.06 2.6067 0 2 12 4 35.78 1.24 2.5098 0 4 9 4 37.09 1.20 2.4237 0 0 14 2 37.13 3.01 2.4213 1 1 11 8 41.58 2.97 2.1719 1 5 4 8 41.61 36.55 2.1705 1 1 13 8 41.66 1.52 2.1677 0 6 4 4 41.87 1.02 2.1578 1 3 11 8 42.63 2.52 2.1207 0 0 16 2 43.33 16.50 2.0881 1 5 6 8 43.41 9.81 2.0843 0 6 6 4 43.87 1.36 2.0639 1 3 12 8 43.96 36.20 2.0597 1 1 14 8 44.36 37.81 2.0420 2 0 0 2 44.44 42.09 2.0385 1 5 7 8 44.52 22.54 2.0350 0 6 7 4 45.70 15.63 1.9855 1 5 8 8 45.77 5.95 1.9822 0 6 8 4 45.96 1.77 1.9746 1 3 13 8 46.17 1.63 1.9663 0 4 14 4 46.38 4.95 1.9578 1 1 15 8 47.08 1.42 1.9301 1 5 9 8 48.14 3.59 1.8901 1 3 14 8 48.28 10.13 1.8851 0 0 18 2 48.60 1.28 1.8734 1 5 10 8 50.24 5.49 1.8161 1 5 11 8 50.31 2.76 1.8137 0 6 11 4 50.41 13.84 1.8104 1 3 15 8 50.90 3.57 1.7939 0 4 16 4 51.49 12.95 1.7747 2 2 8 8 51.98 8.74 1.7591 1 5 12 8 52.05 4.47 1.7569 0 6 12 4 52.50 9.59 1.7432 2 4 1 8 52.63 1.20 1.7389 1 7 0 4 52.71 10.47 1.7367 1 7 1 8 52.72 7.21 1.7363 2 4 2 8 52.75 6.71 1.7355 1 3 16 8 52.77 21.99 1.7348 2 2 9 8 52.93 5.41 1.7299 1 7 2 8 53.09 1.79 1.7250 2 4 3 8 53.30 2.22 1.7187 1 7 3 8 53.38 11.59 1.7165 0 4 17 4 53.84 4.70 1.7028 1 5 13 8 53.91 2.06 1.7008 0 6 13 4 54.05 1.93 1.6966 0 0 20 2 54.17 8.77 1.6933 2 2 10 8 54.86 1.36 1.6734 0 8 2 4 55.22 7.12 1.6633 0 8 3 4 55.68 9.73 1.6507 2 2 11 8 55.73 6.67 1.6495 0 8 4 4 55.91 2.33 1.6444 0 4 18 4 57.32 1.49 1.6075 2 2 12 8 61.19 2.82 1.5148 0 4 20 4 62.17 2.07 1.4932 1 1 21 8 63.21 1.14 1.4710 2 0 16 4 63.81 4.46 1.4586 2 6 6 8 63.92 4.27 1.4564 0 4 21 4 64.66 10.54 1.4414 2 6 7 8 65.52 1.78 1.4246 1 3 21 8 65.64 3.10 1.4223 2 6 8 8 67.64 5.48 1.3851 2 0 18 4 67.91 4.06 1.3802 1 1 23 8 68.29 5.68 1.3735 1 3 22 8 69.29 1.52 1.3560 2 6 11 8 69.67 2.29 1.3496 0 8 15 4 69.78 1.97 1.3477 2 4 16 8 69.96 1.91 1.3447 1 7 16 8 70.40 1.18 1.3375 3 1 4 8 70.69 3.67 1.3326 1 9 8 8 70.74 2.68 1.3318 2 6 12 8 70.88 3.77 1.3295 1 1 24 8 70.96 3.63 1.3282 3 1 5 8 71.49 2.00 1.3196 0 10 5 4 71.65 1.27 1.3172 3 1 6 8 71.75 6.68 1.3155 1 9 9 8 71.85 7.02 1.3139 2 4 17 8 72.03 7.01 1.3111 1 7 17 8 72.30 1.36 1.3069 2 6 13 8 72.42 1.28 1.3050 2 0 20 4 72.82 1.07 1.2988 3 3 2 8 72.93 2.38 1.2971 1 9 10 8 73.13 4.03 1.2941 3 3 3 8 73.42 4.38 1.2896 2 8 3 8 73.56 4.72 1.2875 3 3 4 8 73.85 4.30 1.2832 2 8 4 8 73.92 1.48 1.2821 1 1 25 8 74.02 1.54 1.2808 2 4 18 8 74.19 1.29 1.2782 1 7 18 8 74.23 3.04 1.2776 1 9 11 8 77.22 1.21 1.2354 0 2 27 4 78.64 1.97 1.2166 2 4 20 8 78.81 1.97 1.2144 1 7 20 8 79.77 3.00 1.2022 3 1 13 8 80.28 1.24 1.1958 0 10 13 4 80.95 1.38 1.1876 3 5 6 8 81.11 3.33 1.1857 2 4 21 8 81.28 3.68 1.1837 1 7 21 8 81.39 3.19 1.1823 3 1 14 8 81.73 3.73 1.1783 3 5 7 8 81.90 1.40 1.1763 0 10 14 4 82.30 6.43 1.1716 1 11 0 4 82.63 1.64 1.1678 3 5 8 8 83.15 1.78 1.1618 1 5 25 8 83.94 2.07 1.1528 0 2 29 4 86.15 1.56 1.1288 3 3 15 8 86.43 1.89 1.1259 2 8 15 8 87.38 1.14 1.1161 3 5 12 8 87.95 1.40 1.1103 3 7 1 8 88.15 1.77 1.1083 2 10 5 8 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.