Boscardinite Orlandi P, Biagioni C, Bonaccorsi E, Moelo Y, Paar W H The Canadian Mineralogist 50 (2012) 235-251 Lead-antimony sulfosalts from Tuscany (Italy). XII. Boscardinite, TlPb4(Sb7As2)S9S18, a new mineral species from the Monte Arsiccio mine: Occurrence and crystal structure Locality: Monte Arsiccio, near Sant'Anna di Stazzema, Apuan Alps, Tuscany, Italy _database_code_amcsd 0019212 CELL PARAMETERS: 8.0929 8.7610 22.4970 90.868 97.247 90.793 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 1581.957 Density (g/cm3): 5.355 MAX. ABS. INTENSITY / VOLUME**2: 22.82170314 RIR: 1.388 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 7.92 15.51 11.1570 0 0 2 2 11.90 8.58 7.4380 0 0 3 2 12.18 5.01 7.2665 1 0 1 2 12.75 1.56 6.9454 -1 0 2 2 14.38 2.10 6.1575 1 0 2 2 15.05 1.77 5.8850 -1 1 1 2 15.18 7.87 5.8360 -1 0 3 2 15.50 1.10 5.7178 0 -1 3 2 16.31 6.30 5.4338 -1 -1 2 2 17.25 1.36 5.1415 1 0 3 2 17.43 1.28 5.0892 1 -1 2 2 17.79 2.56 4.9869 1 1 2 2 19.83 1.35 4.4771 1 -1 3 2 19.89 6.59 4.4628 0 0 5 2 20.28 3.27 4.3794 0 2 0 2 20.50 2.08 4.3316 1 0 4 2 20.60 24.49 4.3114 0 -2 1 2 20.74 11.65 4.2837 0 2 1 2 21.52 31.40 4.1284 -1 0 5 2 21.67 11.52 4.1005 0 -2 2 2 22.00 46.54 4.0402 -2 0 1 2 22.20 12.22 4.0041 0 -1 5 2 22.58 9.58 3.9386 -2 0 2 2 23.00 44.61 3.8660 2 0 1 2 23.40 12.60 3.8023 0 -2 3 2 23.51 9.32 3.7844 1 -2 1 2 23.75 14.99 3.7461 0 2 3 2 23.82 25.88 3.7350 -2 0 3 2 23.93 4.14 3.7183 1 2 1 2 23.99 32.42 3.7097 -1 2 2 2 24.01 62.37 3.7067 1 0 5 2 24.06 16.75 3.6993 -1 -2 2 2 24.25 3.79 3.6709 -2 1 0 2 24.50 7.61 3.6333 2 0 2 2 24.69 54.96 3.6058 1 -2 2 2 25.09 100.00 3.5499 -1 0 6 2 25.21 62.54 3.5330 1 2 2 2 25.41 24.54 3.5059 -1 -2 3 2 25.45 32.03 3.4998 -1 2 3 2 25.65 22.05 3.4736 0 -2 4 2 25.65 16.47 3.4727 -2 0 4 2 25.90 6.11 3.4402 1 -1 5 2 26.08 8.06 3.4166 0 2 4 2 26.19 1.81 3.4024 0 1 6 2 26.37 1.99 3.3799 2 -1 2 2 26.44 2.75 3.3707 1 -2 3 2 26.53 15.29 3.3592 2 0 3 2 27.01 1.90 3.3006 -1 -1 6 2 27.03 17.63 3.2984 1 2 3 2 27.29 8.67 3.2676 -1 -2 4 2 27.68 20.74 3.2227 1 0 6 2 27.96 20.39 3.1915 -2 0 5 2 27.99 8.02 3.1877 0 0 7 2 28.31 1.74 3.1528 0 -2 5 2 28.67 15.74 3.1138 1 -2 4 2 28.80 12.25 3.1001 -1 0 7 2 28.80 2.50 3.0995 0 2 5 2 29.00 33.56 3.0787 2 0 4 2 29.31 29.96 3.0467 1 2 4 2 29.33 6.91 3.0454 1 -1 6 2 29.62 10.88 3.0155 -1 -2 5 2 29.66 1.41 3.0120 0 -1 7 2 29.85 30.60 2.9927 -1 2 5 2 29.89 3.90 2.9888 -2 2 1 2 29.96 7.93 2.9826 -2 2 0 2 30.29 13.90 2.9506 -2 -2 1 2 30.38 6.85 2.9425 -2 2 2 2 30.45 2.48 2.9358 2 2 0 2 30.49 2.20 2.9321 -1 -1 7 2 30.56 1.61 2.9249 2 -2 1 2 30.57 1.20 2.9244 2 -1 4 2 30.64 6.48 2.9180 -2 0 6 2 31.14 10.68 2.8724 2 2 1 2 31.28 13.36 2.8598 1 -2 5 2 31.29 2.20 2.8589 0 -2 6 2 31.38 37.78 2.8506 -2 2 3 2 31.48 25.15 2.8420 1 0 7 2 31.58 67.41 2.8331 -2 -2 3 2 31.68 52.46 2.8240 2 -2 2 2 31.81 14.91 2.8127 2 0 5 2 31.83 2.09 2.8113 0 2 6 2 31.97 4.13 2.7998 1 2 5 2 32.32 1.35 2.7703 -1 -2 6 2 32.33 44.56 2.7693 2 2 2 2 32.61 8.77 2.7462 -1 3 1 2 32.63 5.78 2.7445 -1 0 8 2 32.81 3.54 2.7299 1 3 0 2 32.86 45.36 2.7252 -2 2 4 2 32.93 8.74 2.7199 1 -1 7 2 32.97 44.07 2.7169 -2 -2 4 2 33.25 8.04 2.6945 -1 3 2 2 33.27 28.67 2.6928 2 -2 3 2 33.30 3.57 2.6907 1 3 1 2 33.35 1.40 2.6869 1 1 7 2 33.44 10.23 2.6799 -3 0 2 2 33.49 3.01 2.6757 3 0 0 2 33.62 4.45 2.6657 -2 0 7 2 33.97 9.11 2.6388 2 2 3 2 34.12 1.96 2.6274 -1 -1 8 2 34.15 6.27 2.6257 -3 0 3 2 34.25 5.40 2.6179 3 0 1 2 34.27 1.01 2.6163 1 3 2 2 34.35 1.64 2.6105 -1 1 8 2 34.37 4.74 2.6092 -1 3 3 2 34.77 3.08 2.5798 -2 2 5 2 34.90 1.56 2.5712 -3 1 2 2 34.90 2.79 2.5708 2 0 6 2 34.91 1.04 2.5704 -3 1 0 2 34.91 1.42 2.5698 1 2 6 2 35.38 7.04 2.5372 1 0 8 2 35.48 6.95 2.5304 3 0 2 2 35.66 1.51 2.5180 -1 2 7 2 36.56 17.11 2.4581 -1 0 9 2 36.67 1.27 2.4505 1 -1 8 2 36.92 12.30 2.4346 -3 0 5 2 37.36 3.39 2.4070 1 -2 7 2 37.95 40.35 2.3710 0 -2 8 2 38.14 1.11 2.3593 -1 1 9 2 38.32 3.80 2.3488 -3 1 5 2 38.51 13.41 2.3375 -1 -2 8 2 38.56 53.19 2.3347 0 2 8 2 38.77 6.21 2.3227 3 1 3 2 38.90 3.79 2.3151 -3 0 6 2 38.92 11.98 2.3138 -1 2 8 2 39.14 13.58 2.3018 3 0 4 2 39.20 1.45 2.2983 2 -3 2 2 39.20 1.91 2.2980 -3 2 2 2 39.37 7.17 2.2888 1 0 9 2 39.76 2.77 2.2673 3 2 0 2 39.81 5.03 2.2646 3 -2 1 2 39.86 3.02 2.2615 -3 2 3 2 40.27 2.01 2.2397 -2 0 9 2 40.42 1.85 2.2314 0 0 10 2 40.45 5.84 2.2299 3 2 1 2 40.57 2.52 2.2236 -1 0 10 2 40.73 6.11 2.2152 1 -2 8 2 40.93 5.24 2.2049 -3 2 4 2 41.20 1.98 2.1909 -3 -2 4 2 41.22 2.18 2.1903 -3 0 7 2 41.23 63.31 2.1897 0 4 0 2 41.36 4.25 2.1829 0 -4 1 2 41.50 10.45 2.1761 1 2 8 2 41.51 1.99 2.1757 0 4 1 2 42.19 1.35 2.1418 0 4 2 2 42.28 7.24 2.1377 3 -2 3 2 42.58 1.29 2.1232 -3 -2 5 2 42.75 1.15 2.1150 -1 4 1 2 42.79 1.75 2.1132 2 -1 8 2 42.85 1.88 2.1103 0 -4 3 2 43.03 6.49 2.1019 3 2 3 2 43.25 2.62 2.0919 2 1 8 2 43.83 5.25 2.0657 -3 0 8 2 44.00 1.09 2.0580 1 -3 7 2 44.05 1.30 2.0557 2 2 7 2 44.12 8.62 2.0525 3 0 6 2 44.19 4.22 2.0494 -3 2 6 2 44.20 1.68 2.0492 1 4 2 2 44.28 5.12 2.0455 1 -2 9 2 44.51 2.44 2.0357 1 -1 10 2 44.67 2.25 2.0285 0 0 11 2 44.87 4.41 2.0201 -4 0 2 2 45.05 1.52 2.0126 -2 -1 10 2 45.06 1.09 2.0118 1 2 9 2 45.18 4.68 2.0068 4 0 0 2 45.29 4.16 2.0022 -4 0 3 2 45.36 1.16 1.9994 -2 -2 9 2 45.52 4.37 1.9928 -1 -2 10 2 45.61 2.94 1.9888 -2 2 9 2 45.78 1.08 1.9819 -1 -1 11 2 45.85 1.13 1.9792 0 -4 5 2 46.01 1.04 1.9727 -1 2 10 2 46.10 1.03 1.9689 0 1 11 2 46.17 5.34 1.9660 3 -2 5 2 46.20 1.19 1.9650 -2 3 7 2 46.32 8.84 1.9600 -3 2 7 2 46.36 1.29 1.9584 2 -2 8 2 46.37 10.67 1.9579 -3 -2 7 2 46.65 1.90 1.9471 -4 -1 3 2 46.69 5.41 1.9453 -3 0 9 2 46.75 1.31 1.9431 -3 -3 3 2 46.81 6.98 1.9406 -1 -4 5 2 46.90 2.54 1.9373 1 4 4 2 46.94 6.12 1.9356 -2 4 1 2 46.95 2.74 1.9352 -2 4 0 2 47.01 1.90 1.9330 4 0 2 2 47.01 5.98 1.9330 3 2 5 2 47.02 8.80 1.9327 3 0 7 2 47.08 8.70 1.9303 3 -3 2 2 47.26 4.74 1.9235 -4 0 5 2 47.34 3.24 1.9204 2 -4 1 2 47.48 2.47 1.9148 -2 -4 1 2 47.60 11.13 1.9102 -2 0 11 2 47.61 2.93 1.9098 -3 -3 4 2 47.71 2.31 1.9061 -2 -4 2 2 47.79 5.96 1.9033 1 -4 5 2 48.03 5.89 1.8942 -2 4 3 2 48.09 1.34 1.8922 2 -4 2 2 48.13 4.56 1.8906 2 4 1 2 48.34 5.05 1.8827 3 -3 3 2 48.45 1.14 1.8787 4 0 3 2 48.58 1.30 1.8741 3 -2 6 2 48.62 2.85 1.8727 -2 -2 10 2 48.65 6.70 1.8714 -1 -4 6 2 48.73 4.32 1.8686 -3 -2 8 2 48.75 1.12 1.8681 -3 2 8 2 48.75 8.11 1.8678 1 4 5 2 48.76 2.48 1.8675 -4 0 6 2 48.92 2.08 1.8617 -2 2 10 2 48.99 7.98 1.8595 0 0 12 2 49.08 16.66 1.8560 -1 4 6 2 49.16 7.53 1.8533 2 0 10 2 49.18 3.16 1.8528 0 -2 11 2 49.26 1.78 1.8499 -1 -2 11 2 49.27 2.56 1.8496 -2 -4 4 2 49.38 11.03 1.8457 -4 2 1 2 49.44 5.96 1.8434 -4 2 2 2 49.45 6.58 1.8433 3 2 6 2 49.67 1.36 1.8355 -4 2 0 2 49.72 5.13 1.8339 2 -2 9 2 49.78 4.61 1.8316 -1 2 11 2 49.79 1.08 1.8313 -3 0 10 2 49.85 8.80 1.8292 1 -4 6 2 49.86 2.16 1.8288 0 2 11 2 49.94 3.02 1.8261 3 -3 4 2 49.96 6.92 1.8255 -4 -2 1 2 49.96 5.49 1.8254 -4 -2 2 2 50.09 1.34 1.8211 2 -1 10 2 50.22 1.09 1.8168 -3 3 6 2 50.22 4.52 1.8166 4 0 4 2 50.31 8.04 1.8135 4 2 0 2 50.38 3.61 1.8113 -3 -3 6 2 50.54 3.45 1.8060 -2 4 5 2 50.56 2.50 1.8052 -2 -4 5 2 50.59 5.52 1.8042 -4 0 7 2 50.59 9.21 1.8041 2 2 9 2 50.80 2.29 1.7974 -1 -4 7 2 51.00 4.10 1.7907 0 4 7 2 51.02 1.56 1.7901 4 2 1 2 51.25 2.33 1.7827 -2 -3 9 2 51.25 1.61 1.7826 3 -2 7 2 51.32 2.06 1.7805 4 -2 2 2 51.33 2.91 1.7798 -1 -3 10 2 51.36 6.44 1.7790 -3 -2 9 2 51.43 6.93 1.7766 -3 2 9 2 51.49 4.13 1.7750 -2 0 12 2 51.75 8.08 1.7665 2 4 4 2 51.76 2.85 1.7662 -4 2 5 2 51.84 3.44 1.7638 1 -2 11 2 51.85 1.68 1.7632 1 0 12 2 52.02 6.13 1.7579 2 -3 8 2 52.06 1.91 1.7566 4 2 2 2 52.08 1.42 1.7560 -4 -2 5 2 52.20 1.05 1.7523 1 -4 7 2 52.28 1.14 1.7499 -2 4 6 2 52.42 5.79 1.7455 -2 2 11 2 52.65 4.50 1.7383 1 2 11 2 52.72 4.20 1.7363 -4 0 8 2 53.10 5.23 1.7249 -3 0 11 2 53.10 2.69 1.7248 2 0 11 2 53.14 2.47 1.7237 -1 0 13 2 53.14 2.06 1.7235 -1 -2 12 2 53.18 3.99 1.7224 4 -1 5 2 53.20 1.32 1.7217 -4 2 6 2 53.25 2.98 1.7201 2 -2 10 2 53.35 4.55 1.7174 1 4 7 2 53.44 1.02 1.7147 4 2 3 2 53.46 1.40 1.7140 -4 -2 6 2 53.60 3.02 1.7098 2 4 5 2 53.66 1.26 1.7079 -3 4 0 2 53.70 2.27 1.7070 -1 2 12 2 53.71 2.87 1.7065 -1 -5 1 2 53.86 2.93 1.7023 -1 4 8 2 54.03 2.65 1.6973 -1 -5 2 2 54.13 1.28 1.6943 3 -4 1 2 54.15 2.66 1.6938 2 2 10 2 54.16 1.51 1.6934 3 -2 8 2 54.28 1.27 1.6899 4 -2 4 2 54.29 1.86 1.6896 -3 4 3 2 54.42 4.98 1.6859 -3 -4 2 2 54.57 1.09 1.6816 3 4 0 2 54.65 1.61 1.6794 0 -3 11 2 54.66 2.68 1.6790 0 1 13 2 54.76 1.05 1.6762 -1 -3 11 2 54.81 1.86 1.6748 1 -4 8 2 54.93 1.33 1.6715 3 -4 2 2 55.12 1.41 1.6663 4 2 4 2 55.12 2.57 1.6662 -4 0 9 2 55.15 2.59 1.6653 3 4 1 2 55.34 1.74 1.6600 -4 3 3 2 55.70 1.29 1.6503 -2 -2 12 2 55.90 3.72 1.6449 -1 -4 9 2 56.07 1.44 1.6402 0 -5 5 2 56.20 1.24 1.6368 1 0 13 2 56.37 3.84 1.6323 -3 4 5 2 56.63 1.89 1.6254 -1 4 9 2 56.98 2.56 1.6162 3 0 10 2 56.99 1.43 1.6159 -4 2 8 2 57.03 1.04 1.6149 -2 5 0 2 57.25 2.28 1.6091 4 0 7 2 57.32 2.12 1.6074 0 -2 13 2 57.49 3.06 1.6032 3 -4 4 2 57.71 1.11 1.5974 -5 0 4 2 57.72 1.59 1.5971 1 -5 5 2 57.78 1.70 1.5958 -4 0 10 2 57.78 1.51 1.5956 3 -1 10 2 57.85 3.08 1.5939 0 0 14 2 57.87 4.79 1.5934 -5 1 1 2 57.87 1.72 1.5933 2 2 11 2 58.05 2.41 1.5889 0 2 13 2 58.26 1.46 1.5836 -5 1 0 2 58.43 1.15 1.5793 4 -2 6 2 58.59 3.83 1.5754 -5 0 5 2 58.80 1.57 1.5704 3 4 4 2 58.81 2.13 1.5701 -1 -4 10 2 58.96 2.35 1.5665 1 4 9 2 59.17 5.78 1.5615 5 0 2 2 59.21 1.40 1.5604 3 -4 5 2 59.34 1.92 1.5573 4 2 6 2 59.49 1.35 1.5538 -2 -2 13 2 59.53 2.89 1.5529 1 -5 6 2 59.67 1.19 1.5496 -3 4 7 2 60.52 2.06 1.5299 5 0 3 2 61.23 2.05 1.5139 3 -4 6 2 61.32 1.66 1.5117 -1 -2 14 2 61.37 3.36 1.5107 2 0 13 2 61.43 2.28 1.5092 3 -1 11 2 61.61 2.13 1.5053 1 -5 7 2 61.72 2.08 1.5029 -3 -4 8 2 61.94 4.10 1.4982 -1 2 14 2 62.11 2.31 1.4944 -4 4 2 2 62.25 2.20 1.4913 -4 4 0 2 62.28 3.90 1.4908 0 -3 13 2 62.44 1.09 1.4873 4 3 5 2 62.71 1.52 1.4816 3 4 6 2 62.99 1.79 1.4756 0 4 11 2 63.29 1.81 1.4694 -4 -4 3 2 63.45 1.23 1.4660 -2 -2 14 2 63.50 2.23 1.4649 3 -4 7 2 63.63 1.15 1.4623 -5 2 6 2 63.92 1.56 1.4565 -2 2 14 2 63.93 1.60 1.4561 -2 0 15 2 64.00 2.95 1.4548 -5 -2 6 2 64.09 3.92 1.4530 -3 4 9 2 64.20 1.50 1.4508 -4 4 5 2 64.46 2.41 1.4456 -2 -4 11 2 64.76 1.14 1.4395 -4 -4 5 2 65.06 2.46 1.4336 3 4 7 2 65.07 2.42 1.4335 -2 4 11 2 65.10 1.65 1.4329 -5 2 7 2 65.25 1.02 1.4299 2 -4 10 2 65.27 2.80 1.4295 -1 6 2 2 65.27 3.29 1.4295 0 -4 12 2 65.38 1.64 1.4274 1 -6 2 2 65.66 2.08 1.4220 5 -2 4 2 65.86 1.74 1.4182 0 -6 4 2 65.94 1.48 1.4166 -4 -4 6 2 65.99 2.07 1.4156 -1 6 3 2 66.10 2.15 1.4136 1 6 2 2 66.18 1.60 1.4120 4 -4 4 2 66.52 1.57 1.4056 0 4 12 2 66.54 1.96 1.4053 5 2 4 2 66.59 2.46 1.4043 -1 0 16 2 66.79 1.23 1.4006 -1 -6 4 2 66.83 2.58 1.3999 2 4 10 2 66.84 3.00 1.3996 -5 2 8 2 66.88 2.34 1.3991 -3 5 6 2 67.03 2.68 1.3963 1 6 3 2 67.10 2.20 1.3949 -5 -2 8 2 67.41 1.93 1.3893 -4 -4 7 2 68.14 1.70 1.3761 -3 0 15 2 68.24 1.29 1.3743 1 6 4 2 68.32 1.73 1.3730 -1 6 5 2 68.34 1.42 1.3727 -2 4 12 2 68.53 2.24 1.3692 2 -4 11 2 68.62 1.17 1.3677 1 -2 15 2 68.64 1.17 1.3673 -2 -6 1 2 68.83 1.71 1.3640 2 -6 2 2 69.04 1.37 1.3603 1 4 12 2 69.06 1.11 1.3600 2 -2 14 2 69.15 1.11 1.3585 -4 -4 8 2 69.19 1.05 1.3578 -3 -4 11 2 69.25 2.72 1.3568 -2 -6 3 2 69.51 2.75 1.3523 1 2 15 2 69.52 1.18 1.3522 -3 4 11 2 69.61 1.69 1.3507 5 -2 6 2 69.69 2.56 1.3492 2 -6 3 2 69.92 1.71 1.3455 -1 4 13 2 69.92 1.05 1.3453 2 6 2 2 69.99 1.94 1.3442 4 0 11 2 70.04 1.03 1.3435 2 2 14 2 70.25 3.12 1.3400 -6 0 4 2 70.56 1.00 1.3347 5 2 6 2 70.68 2.30 1.3328 -4 0 14 2 70.81 1.52 1.3306 4 2 10 2 70.87 1.45 1.3297 -4 -2 13 2 71.00 1.95 1.3276 -4 2 13 2 71.03 1.28 1.3271 -4 4 9 2 71.13 1.32 1.3255 6 0 1 2 72.59 1.05 1.3023 5 1 8 2 72.92 1.04 1.2973 -5 4 4 2 73.27 1.29 1.2919 -6 2 3 2 73.70 1.19 1.2854 4 0 12 2 73.72 1.18 1.2852 -6 2 0 2 73.77 2.65 1.2844 0 6 8 2 74.00 1.40 1.2810 -6 -2 1 2 74.54 1.20 1.2731 -5 -4 5 2 74.68 1.27 1.2710 -1 -2 17 2 75.08 1.24 1.2653 5 -4 3 2 75.39 3.65 1.2608 5 4 2 2 75.50 1.55 1.2592 2 -1 16 2 75.74 1.01 1.2558 2 -4 13 2 76.10 1.37 1.2508 4 -5 5 2 76.34 1.46 1.2474 5 -3 7 2 76.39 1.42 1.2467 4 4 8 2 76.72 1.03 1.2422 1 -6 9 2 76.73 1.55 1.2421 -3 0 17 2 77.46 1.10 1.2321 -1 7 2 2 77.51 1.49 1.2315 2 4 13 2 78.20 1.15 1.2224 -4 2 15 2 78.84 1.14 1.2140 -3 -6 7 2 80.22 2.01 1.1966 -5 5 1 2 80.28 1.04 1.1959 3 -2 15 2 80.56 1.13 1.1924 -3 -6 8 2 80.57 1.31 1.1923 -3 2 17 2 80.62 1.02 1.1917 -4 6 1 2 80.92 1.20 1.1880 -6 0 11 2 81.37 1.91 1.1825 3 2 15 2 81.78 1.79 1.1777 3 6 6 2 82.05 1.17 1.1745 -1 4 16 2 82.29 1.35 1.1717 4 6 0 2 82.69 1.79 1.1670 2 6 9 2 83.73 1.54 1.1552 -2 6 11 2 84.11 1.38 1.1509 6 0 8 2 84.96 1.39 1.1416 1 0 19 2 85.38 1.65 1.1370 -6 -4 4 2 85.41 1.05 1.1366 -4 4 14 2 85.61 1.44 1.1346 4 4 11 2 86.02 1.38 1.1301 3 -7 2 2 86.99 1.48 1.1200 -6 2 12 2 87.06 1.01 1.1193 -3 -7 4 2 87.16 1.35 1.1183 -6 -2 12 2 89.06 1.30 1.0993 -3 -7 6 2 89.40 1.04 1.0960 -3 -2 19 2 89.63 1.24 1.0938 2 -7 8 2 89.93 1.32 1.0909 -3 2 19 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.