Sanmartinite Redfern S A T, Bell A M T, Henderson M B, Schofield P F European Journal of Mineralogy 7 (1995) 1019-1028 Rietveld study of the structural phase transition in the sanmartinite (ZnWO4)- cuproscheelite (CuWO4) solid solution Sample: x=0.55 _database_code_amcsd 0006599 CELL PARAMETERS: 4.6890 5.7700 4.8990 90.840 91.520 85.870 SPACE GROUP: P-1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 132.144 Density (g/cm3): 7.850 MAX. ABS. INTENSITY / VOLUME**2: 86.41185414 RIR: 3.584 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 15.40 26.03 5.7545 0 1 0 2 18.98 77.30 4.6753 1 0 0 2 23.64 34.81 3.7630 1 1 0 2 23.71 34.03 3.7531 0 -1 1 2 24.01 37.69 3.7060 0 1 1 2 25.39 44.99 3.5077 -1 1 0 2 29.52 100.00 3.0264 -1 -1 1 2 30.37 90.23 2.9430 1 1 1 2 31.08 42.39 2.8773 0 2 0 2 31.20 78.24 2.8671 -1 1 1 2 31.54 71.28 2.8364 1 -1 1 2 35.44 6.54 2.5328 1 2 0 2 36.00 32.98 2.4947 0 -2 1 2 36.42 26.29 2.4670 0 2 1 2 36.70 47.43 2.4484 0 0 2 2 37.87 3.32 2.3756 -1 2 0 2 38.51 32.77 2.3376 2 0 0 2 39.83 2.17 2.2634 0 -1 2 2 40.51 13.05 2.2270 1 2 1 2 40.60 1.02 2.2220 2 1 0 2 41.18 19.03 2.1921 -1 0 2 2 42.09 2.52 2.1466 1 0 2 2 42.24 1.31 2.1394 -1 2 1 2 42.33 16.60 2.1353 1 -2 1 2 42.78 2.78 2.1136 -2 1 0 2 43.51 5.33 2.0799 -1 -1 2 2 44.27 5.00 2.0461 -2 -1 1 2 44.74 5.24 2.0257 1 1 2 2 44.91 7.04 2.0185 -1 1 2 2 45.31 7.76 2.0016 2 1 1 2 45.41 7.47 1.9971 1 -1 2 2 46.48 3.51 1.9537 -2 1 1 2 47.15 4.74 1.9277 2 -1 1 2 47.39 5.51 1.9182 0 3 0 2 48.38 12.96 1.8815 2 2 0 2 48.51 11.09 1.8766 0 -2 2 2 49.17 11.31 1.8530 0 2 2 2 50.09 23.96 1.8210 1 3 0 2 51.24 2.33 1.7829 -1 -2 2 2 51.53 12.74 1.7736 -2 -2 1 2 52.15 7.15 1.7539 -2 2 0 2 52.61 17.35 1.7396 2 2 1 2 52.64 2.37 1.7387 1 2 2 2 52.87 23.12 1.7316 -1 3 0 2 53.28 2.36 1.7193 -1 -3 1 2 53.50 27.81 1.7128 -2 0 2 2 53.69 1.93 1.7070 -1 2 2 2 53.83 1.06 1.7029 1 -2 2 2 54.12 1.25 1.6947 1 3 1 2 54.99 1.09 1.6699 -2 -1 2 2 55.00 22.26 1.6696 2 0 2 2 55.45 15.49 1.6571 -2 2 1 2 55.88 16.71 1.6452 2 -2 1 2 56.40 1.15 1.6315 -1 3 1 2 57.04 1.69 1.6147 -2 1 2 2 58.18 1.51 1.5856 2 -1 2 2 58.59 2.34 1.5756 0 -1 3 2 59.02 3.15 1.5651 0 1 3 2 59.30 2.55 1.5584 3 0 0 2 60.17 3.75 1.5379 2 3 0 2 60.98 3.64 1.5194 0 -3 2 2 61.24 13.20 1.5135 -1 -1 3 2 61.26 7.02 1.5132 -2 -2 2 2 61.82 2.67 1.5007 0 3 2 2 62.48 11.61 1.4864 -1 1 3 2 62.69 10.17 1.4819 1 1 3 2 62.89 2.91 1.4778 -3 1 0 2 62.93 10.30 1.4769 -1 -3 2 2 63.05 11.35 1.4743 -3 -1 1 2 63.09 9.12 1.4735 1 -1 3 2 63.19 6.31 1.4715 2 2 2 2 64.21 11.83 1.4506 3 1 1 2 64.44 11.57 1.4460 1 3 2 2 64.81 1.74 1.4386 0 4 0 2 65.06 3.19 1.4335 -2 2 2 2 65.07 3.38 1.4333 -2 3 0 2 65.37 10.40 1.4276 0 -2 3 2 65.61 7.48 1.4230 -3 1 1 2 65.86 3.24 1.4182 2 -2 2 2 66.02 11.07 1.4151 1 -3 2 2 66.11 1.48 1.4134 3 2 0 2 66.16 9.04 1.4124 -1 3 2 2 66.18 9.81 1.4120 0 2 3 2 66.47 8.09 1.4066 3 -1 1 2 67.48 2.41 1.3880 -1 -2 3 2 67.64 9.44 1.3851 0 -4 1 2 68.17 8.85 1.3756 0 4 1 2 68.56 2.51 1.3688 -3 -2 1 2 69.26 1.23 1.3566 1 2 3 2 69.27 1.99 1.3565 -1 -4 1 2 69.83 1.49 1.3468 -1 2 3 2 70.01 1.68 1.3438 1 -2 3 2 70.12 2.34 1.3421 1 4 1 2 70.59 2.25 1.3342 -2 -1 3 2 70.84 1.51 1.3302 -3 0 2 2 71.56 2.09 1.3185 -2 -3 2 2 71.73 1.03 1.3158 -3 -1 2 2 72.51 1.91 1.3035 -2 1 3 2 72.66 1.94 1.3013 1 -4 1 2 72.76 3.64 1.2998 3 0 2 2 72.86 1.96 1.2982 -1 4 1 2 72.90 2.05 1.2975 2 1 3 2 73.43 2.80 1.2896 -3 2 1 2 73.62 1.67 1.2867 2 3 2 2 74.03 1.30 1.2805 2 -1 3 2 74.27 2.90 1.2771 -3 1 2 2 75.85 5.57 1.2543 3 3 0 2 75.90 2.45 1.2536 3 -1 2 2 76.08 2.36 1.2510 -2 -2 3 2 76.86 2.02 1.2403 -2 3 2 2 77.35 1.54 1.2337 2 -3 2 2 77.36 6.72 1.2336 -2 -4 1 2 78.06 5.63 1.2242 0 0 4 2 78.48 6.58 1.2187 2 4 1 2 78.71 1.71 1.2157 2 2 3 2 79.25 1.28 1.2088 3 2 2 2 79.81 2.87 1.2017 -2 2 3 2 80.91 2.50 1.1882 2 -2 3 2 81.84 2.60 1.1769 1 0 4 2 82.50 4.88 1.1692 -3 3 0 2 82.53 6.77 1.1688 4 0 0 2 83.75 5.14 1.1550 -2 4 1 2 83.86 4.52 1.1537 2 -4 1 2 84.03 1.40 1.1518 1 -1 4 2 85.33 1.92 1.1376 -4 -1 1 2 85.42 3.12 1.1366 1 5 0 2 85.72 3.77 1.1334 -3 -1 3 2 85.87 1.76 1.1317 0 -2 4 2 86.06 5.09 1.1297 -3 -3 2 2 86.67 1.21 1.1234 4 1 1 2 86.86 1.89 1.1213 0 2 4 2 87.80 1.82 1.1118 -1 -5 1 2 87.88 3.06 1.1110 4 2 0 2 88.27 2.75 1.1071 -3 1 3 2 88.36 1.08 1.1062 -4 1 1 2 88.63 3.75 1.1035 3 3 2 2 88.72 1.40 1.1026 1 5 1 2 88.83 4.07 1.1016 3 1 3 2 89.05 2.53 1.0994 -1 5 0 2 89.39 4.60 1.0961 -2 0 4 2 89.99 2.00 1.0904 -4 -2 1 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.