Pb2FeCl3(OH)4.H2O Pasero M, Perchiazzi N, Bigi S, Franzini M, Merlino S European Journal of Mineralogy 9 (1997) 43-51 Pb2FeCl3(OH)4.H2O, a newly discovered natural phase from Tuscany, Italy: physio-chemical data, crystal structure, and OD character Locality: Tuscany, Italy _database_code_amcsd 0006643 CELL PARAMETERS: 8.0330 6.2530 9.2210 90.000 102.980 90.000 SPACE GROUP: P2_1 X-RAY WAVELENGTH: 1.541838 Cell Volume: 451.339 Density (g/cm3): 4.862 MAX. ABS. INTENSITY / VOLUME**2: 119.2050713 RIR: 7.984 RIR based on corundum from Acta Crystallographica A38 (1982) 733-739 2-THETA INTENSITY D-SPACING H K L Multiplicity 9.84 9.84 8.9854 0 0 1 2 11.30 8.38 7.8277 1 0 0 2 13.23 2.85 6.6936 -1 0 1 2 17.28 100.00 5.1325 0 1 1 2 18.16 1.89 4.8856 1 1 0 2 19.43 1.12 4.5694 -1 1 1 2 19.76 12.15 4.4927 0 0 2 2 22.65 3.43 3.9256 -2 0 1 2 22.72 2.19 3.9139 2 0 0 2 24.40 17.41 3.6486 0 1 2 2 24.97 1.52 3.5654 -1 1 2 2 26.63 28.89 3.3468 -2 0 2 2 26.81 28.81 3.3252 2 0 1 2 26.82 15.38 3.3247 -2 1 1 2 26.87 19.03 3.3176 2 1 0 2 28.55 14.46 3.1265 0 2 0 1 29.44 1.69 3.0340 -1 0 3 2 29.83 14.08 2.9951 0 0 3 2 30.27 14.71 2.9529 0 2 1 2 30.29 5.57 2.9507 -2 1 2 2 30.45 2.95 2.9359 2 1 1 2 31.58 1.66 2.8327 -1 2 1 2 33.16 9.07 2.7012 0 1 3 2 33.21 1.25 2.6978 1 2 1 2 33.34 1.22 2.6877 -2 0 3 2 33.58 2.38 2.6691 2 0 2 2 34.38 1.01 2.6086 1 0 3 2 34.96 5.92 2.5663 0 2 2 2 36.38 21.75 2.4693 -2 1 3 2 36.61 20.37 2.4548 2 1 2 2 36.75 17.90 2.4456 -2 2 1 2 36.79 14.39 2.4428 2 2 0 2 37.34 1.04 2.4080 3 1 0 2 38.29 1.36 2.3509 1 2 2 2 39.44 10.85 2.2847 -2 2 2 2 39.57 12.30 2.2778 2 2 1 2 41.62 3.04 2.1700 -2 0 4 2 41.76 9.96 2.1628 0 2 3 2 41.90 2.46 2.1563 2 0 3 2 42.77 16.20 2.1141 0 1 4 2 44.18 2.85 2.0501 -2 1 4 2 44.44 3.96 2.0385 2 1 3 2 44.61 2.00 2.0311 -3 2 1 2 44.63 6.19 2.0304 0 3 1 2 44.64 1.46 2.0300 2 2 2 2 45.01 1.38 2.0142 1 3 0 2 45.15 9.77 2.0082 -4 0 1 2 48.12 2.12 1.8908 0 3 2 2 48.62 5.74 1.8727 -4 1 2 2 48.76 4.56 1.8676 4 1 0 2 49.51 2.60 1.8409 -2 3 1 2 49.55 3.20 1.8397 2 3 0 2 49.59 1.46 1.8382 -4 0 3 2 50.81 1.28 1.7971 0 0 5 2 50.93 1.86 1.7930 -2 0 5 2 51.24 2.31 1.7830 2 0 4 2 51.25 4.00 1.7827 -2 2 4 2 51.48 3.77 1.7751 2 2 3 2 51.66 1.14 1.7693 -2 3 2 2 51.84 1.36 1.7636 -4 1 3 2 52.11 2.34 1.7551 4 1 1 2 53.02 1.14 1.7272 0 1 5 2 53.14 2.60 1.7235 -2 1 5 2 53.17 1.09 1.7225 3 2 2 2 53.44 2.02 1.7147 2 1 4 2 53.57 1.28 1.7108 0 3 3 2 54.29 2.73 1.6897 -4 2 1 2 54.86 1.20 1.6734 -4 0 4 2 55.25 1.83 1.6626 4 0 2 2 55.26 2.09 1.6623 -4 2 2 2 55.39 3.22 1.6588 4 2 0 2 55.82 5.18 1.6471 -2 3 3 2 55.98 5.01 1.6428 2 3 2 2 55.99 1.49 1.6424 -3 2 4 2 56.97 1.93 1.6165 -4 1 4 2 58.22 2.04 1.5846 -4 2 3 2 58.47 1.27 1.5785 4 2 1 2 59.10 3.74 1.5632 0 4 0 1 59.31 4.00 1.5580 0 2 5 2 60.60 4.52 1.5279 0 3 4 2 60.85 1.06 1.5223 -1 4 1 2 63.00 1.32 1.4754 -4 2 4 2 63.06 3.29 1.4743 -2 1 6 2 63.36 1.80 1.4679 4 2 2 2 63.38 3.55 1.4675 2 1 5 2 63.70 3.29 1.4608 -4 1 5 2 63.92 1.17 1.4564 0 1 6 2 64.18 3.52 1.4512 4 1 3 2 65.30 1.63 1.4289 -4 3 2 2 65.42 1.30 1.4267 4 3 0 2 65.95 2.70 1.4164 -2 4 2 2 66.04 2.77 1.4147 2 4 1 2 67.60 1.66 1.3858 0 4 3 2 72.19 1.08 1.3085 -6 0 3 2 72.44 1.17 1.3046 6 0 0 2 75.63 1.13 1.2574 0 1 7 2 77.28 1.66 1.2346 -4 2 6 2 77.36 2.14 1.2336 -4 4 1 2 77.41 1.33 1.2328 -6 1 4 2 77.75 1.01 1.2284 -6 2 2 2 77.82 1.45 1.2274 4 2 4 2 77.82 1.17 1.2274 6 1 1 2 77.88 1.13 1.2265 -2 3 6 2 78.18 1.24 1.2226 2 3 5 2 78.47 1.44 1.2188 -4 3 5 2 78.91 1.53 1.2132 4 3 3 2 79.30 1.98 1.2082 -2 2 7 2 79.63 1.12 1.2040 6 2 0 2 79.65 1.97 1.2038 2 2 6 2 ================================================================================ XPOW Copyright 1993 Bob Downs, Ranjini Swaminathan and Kurt Bartelmehs For reference, see Downs et al. (1993) American Mineralogist 78, 1104-1107.